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HomeMy WebLinkAboutSESFortunato Binder Report final 1-30-2017SOIL & ENVIRONMENTAL SERVICES, INC. 61 Plants Dam Road, East Lyme, CT 06333 860-739-6691 Fax 739-4150 soilinc@gmail.com SOIL REMEDIAL ACTION REPORT FOR NORWICH PUBLIC UTILITIES, STONY BROOK LOCATION CHERRY LANE, OAKDALE, CT FOR: NORWICH PUBLIC UTILITIES & COMMERCIAL CONSTRUCTION GROUP Prepared by: Martina Castanho Environmental Scientist CT LEP # 236 Donald Fortunato Environmental Scientist CT LEP # 235 December 12, 2016. Rev. December 21, 2016. Rev. January 16, 2017. Rev. January 30, 2017. SOIL & ENVIRONMENTAL SERVICES, INC. 61 Plants Dam Road, East Lyme, CT 06333 860-739-6691 Fax 739-4150 soilinc@gmail.com 1 – NPU, Stony Brook Site, Oakdale, CT 1.0 INTRODUCTION Soil and Environmental Services, Inc. (SES, Inc.) was authorized by Ron Swaney, Commercial Construction Group (CCG), to conduct soil sampling and soil remediation supervision at a leaking generator at the Norwich Public Utilities (NPU) Stony Brook reservoir and water treatment plant (WPT) on Cherry Lane, Oakdale, CT. Soil remediation was conducted to the south of the existing building and at an adjacent wetlands area to the north of the building. Early on October 1, 2016, an older diesel generator used for temporary power released approximately 600 gallons of motor fuel (diesel) to the ground surface. This spill was noted by the NPU crew at about 7 am on Saturday morning, October 1. Generators on Demand (GoD) and CCG was notified and immediately summoned the Connecticut Department of Energy and Environmental Protection (CTDEEP) Oil & Spills Unit. Spills personnel were onsite on Saturday October 1 and Sunday October 2, 2016 to direct CCG personnel and their consultants on proper methods to remediate the spill. Soil removal and Stony Brook tributary remedial efforts took place over that weekend. The leaking generator was connected to a 1,000-gallon diesel fuel underground storage tank (UST) and was an unregistered tank. NPU has since rectified this situation. Our firm conducted soil sampling, test pit examinations, and remediation supervision at the two areas of concern (AOCs) at the southern and northern sections to the existing building. Our work schedule is presented in the section 3.0. SOIL & ENVIRONMENTAL SERVICES, INC. 2 – NPU, Stony Brook Site, Oakdale, CT 2.0 RELATED INFORMATION The site is within a Connecticut Department of Energy and Environmental Protection (CTDEEP) GA groundwater classification area. GA areas are higher quality groundwater areas and water quality is assumed to be suitable for human consumption without treatment. Ground water is assumed to follow surface topography and is towards the north and northeast to the Stony Brook tributary. The site is a public water supply system. The CTDEEP “Remediation Standard Regulations” (RSRs) dated January 1996; revised 2013, state that polluted soil must be remediated to a concentration that is consistent with the Residential Direct Exposure Criteria (RDEC), unless the site is used exclusively for industrial or commercial purposes. In such a case, the less stringent Industrial/Commercial Direct Exposure Criteria may be used, provided an Environmental Land Use Restriction (ELUR) is recorded to ensure that the site is not used for residential purposes in the future. Soils must also meet the “GA pollutant mobility criteria” (PMC). As outlined by the CTDEEP, the RSRs apply to any action taken to remediate polluted soil, surface water or a groundwater plume at or emanating from a release area, provided the remedial action is required pursuant to Chapter 445 or 446k of the Connecticut General Statutes (CGS), or Section 22a-208a(c)(2) of the CGS. The NOV issued to NPU by the CTDEEP on November 22, 2016 required SES, Inc. & CCG to provide certain soil remediation and soil sampling documentation. The NOV stated: “The Compliance Statement should include, but not necessarily be limited to (1) initial analytical results for samples taken from the site; (2) analytical results for samples showing that contamination at the site has been corrected; (3) analytical results evaluating the migration or lack thereof of contamination at the site, (4) documentation confirming that the alleged violations have been remedied, and (5) measures taken to prevent future such violations at this site or other sites or (6) a schedule for providing (1) through (5).” Regulation: CT state regulation CGS 22a-430 Violation Reason: An unpermitted discharge of regulated substance from a UST system has occurred. Required Action: Report the spill to CT DEEP at (860) 424-3338 and hire a spill clean-up contractor and/or an environmental consultant to remediate contaminated soils and/or groundwater to applicable standards. SOIL & ENVIRONMENTAL SERVICES, INC. 3 – NPU, Stony Brook Site, Oakdale, CT Soil sample results were compared to the CTDEEP “residential direct exposure criteria” (DEC) and “GA pollutant mobility criteria” (PMC) as outlined in the CTDEEP RSRs, January 1996, Rev. 2013. As part of the soil remediation process, post-excavation soil samples were collected to determine when all contaminated soil had been removed. Selected samples were analyzed for Extractable Total Petroleum Hydrocarbons (ETPH), Aromatic & Halogenated Volatile Organics (VOCs and AVOCs), and Polynuclear Aromatic Hydrocarbons (PNAs). All soil samples were inspected for visual stains and odor. For disposal authorization, soil samples were analyzed additionally for full VOCs, PCBs, flashpoint, pH, total solids, RCRA Metals, and cyanide/sulfide reactivity. The material was approved for disposal at the Soil Reclamation Facility at Ted Ondrick Company in Chicopee, MA. Soil & waste profile sheets were submitted to the disposal facility personnel prior to shipment. 3.0 ENVIRONMENTAL SUMMARY A summary of environmental work performed on the site related to the surface spill of motor fuel, event dates, and related information is as follows. Saturday, October 1, 2016 to Sunday October 2, 2016 - This spill was noted by the NPU crew at about 7 am on Saturday morning, October 1. GoD and CCG personnel were notified and immediately summoned the CTDEEP Oil & Spills Unit. Spills personnel were onsite both days to direct CCG personnel and their consultants on proper methods to remediate the spill. Soil removal and Stony Brook tributary remedial efforts took place over that weekend. CTDEEP Oils & Spills Unit was the lead agency directing all remedial efforts on the site. Monday, October 3, 2016 to Monday October 10, 2016 - Field work was conducted by SES, Inc. Additional contaminated soil removal was coordinated with the CTDEEP Spills Unit and with Paul Burgess, LEP Consultant to NPU. Soil removal, post-excavation soil sampling, preliminary surface water sampling, and continuing Stony Brook tributary remedial efforts took place. A meeting was conducted with all parties and Liz Burdick, Montville WEO to discuss wetland remediation issues. October 5, 2016 – Montville WEO Burdick sent an email to Robert Shuler (DEEP): “This email is to confirm, pursuant to my conversation yesterday with Matt Williamson of your office, that the State of CT Emergency Response Unit, led by you, will oversee the wetlands restoration in its entirety at 260 Cherry Lane, SOIL & ENVIRONMENTAL SERVICES, INC. 4 – NPU, Stony Brook Site, Oakdale, CT (cont.) Oakdale, CT as part of the emergency remediation of the oil spill that occurred at the site on Saturday, October 1, 2016 and that your office will provide updates and/or relevant reports to this office until such time as you determine the project is complete. Thank you for your assistance with this matter and please contact me should you require any support from the Town of Montville Planning Department”. Liz Burdick, Zoning & Wetlands Officer Town of Montville. October 16 to October 19, 2016 - SES Inc. reviews lab data from post-excavation samples, compiles maps, prepares tables and charts, etc. A meeting was set up with Matt Williamson and Robert Shuler, DEEP to discuss lab results and further action. CTDEEP Oils & Spills Unit, again, is the lead agency directing all remedial efforts on the site. October 19 & 20, 2016 - An email report from SES, Inc. to Liz Burdick regarding wetland issues stating, “the soil removal area within the wetlands covered approximately 150 ft. long by 20-30 feet wide and depths varied from 8-15 inches. Total excavation was ~140 cubic yards or 175 tons. Disposal is currently being arranged. The area has been covered with 4-5 inches of fine sandy loam topsoil and was placed over original sapric muck and very fine sandy loam (Scarboro and Timakwa series). Lab results are satisfactory and the area is to be hydro seeded with a combination of 2 pounds Wetmix, 4 pounds Conservation mix, and 18 pounds of Contractor mix.” Monday, October 24, 2016 – After meeting onsite with Matt Williamson, the DEEP states that we are at the “limits of excavation” and all contaminated soil that can be practically removed has been accomplished. SES issues the following email report. To: Mark Decker; Thomas Cutler; Shuler, Robert; Liz Burdick; Ron Swaney; Williamson, Matthew; Paul Burgess, SES. Subject: NPU Stony Brook “All: Attached are two rough site sketches showing approximate sample locations and ETPH lab results. Complete lab data is attached. We did not want to release this information until all lab results were received with QA/QC data.” 1) All sample results at the wetlands area were non-detectable (ND) or well within the CTDEEP RSRs for ETPH, AVOCs, and PNAs. 2) No additional work has taken place at the site for some time now and Ron will keep NPU apprised. Hydro seeding of the wetlands area will take place shortly and Liz has been notified of this. SOIL & ENVIRONMENTAL SERVICES, INC. 5 – NPU, Stony Brook Site, Oakdale, CT October 24, 2016 (continued) 3) The poly propylene (PP) oil booms will be removed shortly since they are not collecting any oil. Ron will inspect the spill pads periodically and will keep NPU informed. 4) No further remediation work has been conducted at the generator area. Bottom samples at 4-6 feet showed mostly ND levels of ETPH. However, sidewall samples at approximately 0.5 to 6 feet at the generator area were elevated and were over RSR levels. If ETPH levels were elevated, then most AVOC and PNA levels were also elevated above RSR levels. 5) Water sample GW #1 was taken during pumping of waste water from the generator pit. Septic tank overflow moved oil through the crushed stone layers during the spill. ~1200 gallons of oily water were evacuated. Water results were 33 ppm and are above the GWPC of 0.25 ppm. 6) All soil sample locations that are still above RSRs face the sidewalls into electric lines, under asphalt, and under the building. We feel we are at the "limits of excavation" and no further soil removal is warranted. Final grading and seeding at the generator area has not taken place yet and Ron will wait for NPU comments before planning this future work. Please provide any comments you have.” thanks Don Fortunato, SES Inc. November 9, 2016 – NPU responds to Ron Swaney of CCG that they want CCG to excavate under the asphalt and near the electric vault again to remove more soil. An email is sent to DEEP regarding this NPU request. November 10, 2016 – email from DEEP…”Good morning Gentlemen, I received the message that Ron will return on Monday to continue Remediation at NPU Stony Brook. That sounds good. At this time my Supervisor requested that I close this Emergency Spill Case at NPU Stony Brook. My report should be complete in a few weeks. Great job on the work done so far. Continue working with the Town of Montville and property owner to satisfy their needs. Don, once your report is complete please send me a copy to add to CT DEEP ERU file.” Thanks, Robert Shuler November 17, 2016 – NPU requested a meeting onsite with DEEP, NPU, CCG and SES. SOIL & ENVIRONMENTAL SERVICES, INC. 6 – NPU, Stony Brook Site, Oakdale, CT November 21, 2016. Receipt of DEEP email: “Good Morning All: Today I will request that Robert refer this case to Remediation. I am disappointed that progress has slowed and the focus has become the "RSRs" and sign off months and possibly years from now. I have also referred this case to the UST program as the current tank is not registered and may be a source of ongoing contamination. Thank you all.” Williamson, Matthew November 22, 2016 – Notice of Violation; email from CTDEEP, Lori Saliby: “Thank you, Matt & George- Please be aware that we will be expecting the cleanup to proceed on an emergency schedule until we are satisfied pursuant to RCSA 22a-449(d)- 106(b)(2). The UST Program will be issuing an NOV when George stops by tomorrow which will give 30 days to resolve the contamination. Lori Reference: 106 b (2) Corrective action. The owner or operator of an UST system which discharges regulated substances without a permit issued pursuant to section 22a-430 of the general statutes, as amended, shall immediately cease such discharge and reclaim, recover and properly dispose of the discharged liquid and any other substance contaminated by it, restore the environment to a condition and quality acceptable to the commissioner, and repair damage caused by the discharge, and comply with the requirements in subdivision 22a-449 (d)-106 (d) (1) and (b) (3) of these regulations, all to the satisfaction of the commissioner.” November 18 to 22, 2016 – Second remedial effort at generator area at NPU request. Additional contaminated soil removal was coordinated with the CTDEEP Spills Unit and with Paul Burgess, LEP Consultant to NPU. Additional soil removal, post-excavation soil sampling, parking lot test pits, and surface water sampling are completed. As directed by DEEP, remedial efforts at Stony Brook tributary are deemed completed. All PP booms and spill pads are to be removed. 4.0 REMEDIATION SUMMARY As discussed, our firm performed soil sampling and soil remediation supervision at a leaking generator at the Norwich Public Utilities (NPU) site located at the Stony Brook Reservoir, Cherry Lane, Oakdale, CT. Soil remediation areas were located to the south of the existing building and at an adjacent wetlands area to the north of the building. SOIL & ENVIRONMENTAL SERVICES, INC. 7 – NPU, Stony Brook Site, Oakdale, CT Soil samples were collected with stainless steel trowels and knives and all sampling followed proper sampling procedures and chain-of-custody protocol. All soil samples were inspected for visual stains and odor. Selected soil samples were then submitted to CET, a Connecticut certified lab for analysis. Paul Burgess, CTLEP for NPU was onsite and provided his RAE PID to scan soil samples for organic vapors in the field on certain occasions. The first remediation effort for ETPH contaminated soil was conducted from October 1 to October 10, 2016. Contaminated soil from the wetlands area and at the generator/electric vault area was removed. Soil removal in the wetlands was about 8-15 inches deep. The soils here were mostly virgin Timakwa and Whitman soil series (see profile sheets). Soils in the generator/vault area were dug down to about 5-6 feet below grade. The soils here to about 3-4 feet deep were loamy sand to sandy loam fill. The underlying material from 4-7 feet deep was a virgin C horizon and had a massive structure and very firm consistence. Permeability was in NRCS classes slow (0.06 - 0.2 in/hr.) and very slow (0.01 - 0.06 in/hr.). Bedrock was encountered at about 6-7 feet deep. No groundwater was encountered in the generator area. After reviewing post-excavation soil samples results and meeting with the CTDEEP on October 24, DEEP thought that we were at the “limits of excavation” and that all contaminated soil that could be practically removed had been accomplished. CTDEEP Oils & Spills Unit was the lead agency directing all remedial efforts on the site. Our first initial email report of October 24, 2016, showed that all sample results at the wetlands area were non-detectable (ND) or well within the CTDEEP RSRs for ETPH, AVOCs, and/or PNAs. As coordinated with Liz Burdick, Town WEO, hydro seeding of the wetlands area was scheduled and Ms. Burdick was notified. No further remediation work was planned at the generator release area at that time (after October 24). Bottom samples at 4-6 feet showed mostly non-detectable levels of ETPH. However, sidewall samples were over RSR levels at 1-6 feet at sidewalls facing into electric lines and the vault area (west), underneath the asphalt, and under the building. Final grading and seeding at the generator area had not taken place yet and Ron Swaney (CCG) was waiting for NPU comments. On November 9, 2016, NPU responded to Ron Swaney that they wanted CCG to excavate under the asphalt and near the electric vault again to remove more soil. At this point, lead agency DEEP Oil & Spills was ready to “close out” the site. Robert Shuler stated that, “I received the message that Ron will return on Monday to continue Remediation at NPU Stony Brook. That sounds good. At this time my Supervisor SOIL & ENVIRONMENTAL SERVICES, INC. 8 – NPU, Stony Brook Site, Oakdale, CT requested that I close this Emergency Spill Case at NPU Stony Brook. My report should be complete in a few weeks. Great job on the work done so far. Continue working with the Town of Montville and property owner to satisfy their needs. Don, once your report is complete please send me a copy to add to CT DEEP ERU file.” On November 17, 2016, a NPU requested meeting was held onsite with DEEP, NPU, CCG and SES, Inc. During the period of November 18 to 22, 2016, CCG began a second remedial effort at the generator area at the request of NPU. Additional contaminated soil removal was coordinated with the CTDEEP Spills Unit and with Paul Burgess, LEP NPU Consultant. Additional soil removal, post-excavation soil sampling, parking lot test pits, and surface water sampling were completed. As directed by DEEP, remedial efforts at Stony Brook tributary were deemed complete and all PP booms and spill pads were to be removed. Additional soil removal in the generator area took place at initial sample locations: 20-1, 20-2, 20-3, 26, and at sample points #29, 30, 31, and 32 where ETPH levels were above the RDEC. Please refer to Table #1 and site maps for locations. All post-excavation samples after the second round of remediation were found to be either ND or within RSRs at the following locations: at the electric vault area and underneath electric lines, underneath the asphalt parking lot, at the sidewalls facing beneath the building, and septic tank area. No contaminated soils were found at two test pits dug in the parking lot in front of the building. One sample was over the RDEC of 510 ppm at #55 sidewall. The CTDEEP 95% UCL protocol was employed. Results are attached and the mean result from the sample population was ~80 ppm. The 510 ppm #55 is therefore not significant. Please note that samples at #43 and #43/44 composite were taken from sidewalls and the bottom area of the vault for reference purposes. These soil areas have been removed. Samples #12A and 12B were analyzed near wetland sample #12 that initially had an ETPH level of 150 ppm. Samples 12A and B were both ND for ETPH and 12B was also ND for AVOCs. Total disposal is complete and amounted to 227.93 tons. Soil and waste profile sheets, weight tickets, and receipts are on file and general statements are included in the Appendix. Disposal was arranged at Ondricks Soil Reclamation facility in Chicopee, MA. SOIL & ENVIRONMENTAL SERVICES, INC. 9 – NPU, Stony Brook Site, Oakdale, CT The excavated soil was classified as a CT non-hazardous, regulated waste (CR05). As mentioned previously, for disposal authorization, soil samples were analyzed additionally for Aromatic & Halogenated Volatile Organics (VOCs), PCBs, ETPH, flashpoint, pH, total solids, RCRA Metals, cyanide/sulfide reactivity, etc. Again, please note that soils have since been excavated and removed at sample locations #20-1 bottom, #20-2 bottom, #20-3 sidewall, #26 bottom, #29 sidewall, and at #30, 31, and 32 bottoms and sidewalls. Soils were also excavated and removed at sample locations #43 sidewall, at composite #43/44 sidewall, and at all soils surrounding #1 Root in C horizon. All contaminated soil above RSRs has now been removed from the two AOCs and no further remedial work is required. 5.0 OTHER DATA Initial surface water sampling was completed. As directed by the CTDEEP Spills Unit, remedial efforts at Stony Brook tributary were deemed complete as of October 24, 2016, Water sample SW #2 from the tributary was non-detectable (ND) for ETPH and for AVOCs. No groundwater was encountered down to bedrock at 6-7 feet below grade in the generator area. Reasonable Confidence Protocols (RCPs) were used on the last series of soil samples. The Reasonable Confidence Protocols are analytical methods that include specific laboratory quality assurance and quality control (QA/QC) criteria that produce analytical data of known and documented quality. The Reasonable Confidence Protocols methods are published on the DEEP website. For reference CR05, by CTDEEP, is a Waste Chemical Solid (any chemical solid or semi-solid from a commercial, industrial, agricultural or community activity. These wastes may include, but are not limited to, grinding dusts, tumbling sludges, scrap plastic and rubber flash, and other ground or chipped waste solid). 6.0 SUMMARY & CONCLUSIONS Soil and Environmental Services, Inc. (SES, Inc.) was authorized by Ron Swaney, Commercial Construction Group (CCG), to conduct soil sampling and soil remediation SOIL & ENVIRONMENTAL SERVICES, INC. 10 – NPU, Stony Brook Site, Oakdale, CT supervision at a leaking generator to the south of the existing building at the NPU site. Soil remediation also took place at an adjacent wetlands area to the north of the building. The Norwich Public Utilities (NPU) site is located at the Stony Brook Reservoir, Cherry Lane, Oakdale, CT. Early on Saturday, October 1, 2016, an older diesel generator used for temporary power to the facility released approximately 600 gallons of motor fuel (diesel). This spill was noted by the NPU crew at about 7 am that morning and they contacted GoD and CCG who subsequently summoned the Connecticut Department of Energy and Environmental Protection (CTDEEP) Oil & Spills Unit. Spills personnel were onsite on Saturday October 1 and Sunday October 2, 2016 to direct CCG personnel and their consultants on proper methods to remediate the spill. Soil removal and Stony Brook tributary remedial efforts took place over that weekend. The leaking generator was connected to a 1,000-gallon diesel fuel UST and was an unregistered tank. NPU has since rectified this situation. The first remediation effort for ETPH contaminated soil was conducted from October 1 to October 10, 2016. Contaminated soil from the wetlands area and at the generator/electric vault area was removed. Soil removal in the wetlands was about 8-15 inches deep. The soils here were mostly virgin Timakwa and Whitman soil series. Soils in the generator/vault area were dug down to about 5-6 feet below During the period of November 18 to 22, 2016, CCG began a second remedial effort at the generator area at the request of NPU. Additional contaminated soil removal was coordinated with the CTDEEP Spills Unit and with Paul Burgess, LEP NPU Consultant. Additional soil removal, post-excavation soil sampling, parking lot test pits, and surface water sampling were completed. As directed by DEEP, remedial efforts at Stony Brook tributary were deemed complete and all PP booms and spill pads were to be removed. Additional soil removal in the generator area took place at initial sample locations: #20-1, 20-2, 20-3, 26, and at sample points #29, 30, 31, and 32 where ETPH levels were above the RDEC in the first soil removal event. Soils at these sample points have since been removed and disposed of. Please refer to Table #1 and site maps for locations. All post-excavation samples after the second round of remediation in the generator area were found to be either ND or within RSRs. SOIL & ENVIRONMENTAL SERVICES, INC. 11 – NPU, Stony Brook Site, Oakdale, CT Soils were removed on November 18-22 in the generator AOC at the following locations: at the electric vault area and underneath electric lines, underneath the asphalt parking lot, at the sidewalls facing beneath the building, and the septic tank area. Two test pits dug in the parking lot in front of the building were non-detectable for ETPH. One sample was over the RDEC of 510 ppm at #55 sidewall. The CTDEEP 95% UCL protocol was employed. Results are attached and the mean result from the sample population was ~80 ppm. The 510 ppm #55 is therefore not significant. Samples #12A and 12B were analyzed near wetland sample #12 that initially had an ETPH level of 150 ppm. Samples 12A and B were both ND for ETPH and 12B was also ND for AVOCs. Initial surface water sampling was completed. As directed by the CTDEEP Spills Unit, remedial efforts at Stony Brook tributary were deemed complete as of October 24, 2016. Water sample SW #2 from the tributary was ND for ETPH and for AVOCs. No groundwater was encountered down to bedrock at 6-7 feet below grade in the generator area. Total disposal is complete and amounted to 227.93 tons. Soil and waste profile sheets, weight tickets, and receipts are on file and general statements are included in the Appendix. Disposal was arranged at Ondricks Soil Reclamation facility in Chicopee, MA. Again, please note that soils have since been excavated and removed at sample locations #20-1 bottom, 20-2 bottom, 20-3 sidewall, #26 bottom, #29 sidewall, and at #30, 31, and 32 bottoms and sidewalls. Soils were also excavated and removed at sample locations #43 sidewall, at composite #43/44 sidewall, and at all soils surrounding #1 Root in C horizon. All contaminated soil above RSRs has now been removed from the two AOCs at the NPU site and no further remedial work is required. Please refer to all lab data, map, MSRs, etc. that are included at the end of this text. SOIL & ENVIRONMENTAL SERVICES, INC. 12 – NPU, Stony Brook Site, Oakdale, CT Please contact us if you have any questions. Sincerely, Donald Fortunato Donald Fortunato Principal, LEP Martina Castanho Martina Castanho Principal, LEP SOIL & ENVIRONMENTAL SERVICES, INC. SAMPLING PROCEDURE – SOILS As part of the soil remediation process, post-excavation soil samples are collected to determine when all contaminated soil has been removed. Soil samples were collected in the field with stainless steel trowels and knives and all sampling followed proper sampling procedures and chain-of-custody protocol. All soil samples were inspected in the field for visual stains and odor. Once back at the office, each sample and/or duplicate are again inspected for visual stains and odor. The individual samples are scanned with the Thermo 580EZ Photo Ionization Detector (PID). That model was now replaced with a mini RAE PID. Results are recorded on our Soil Sample Screening Result sheets. Selected samples are also tested using the Hanby TPH/PNA in-house testing kit as shown with the Screening Sheets. This is a rough screening tool for information and to aid in picking samples for eventual laboratory analysis. Based on our PID results and Hanby test results and our experience, selected soil samples are then prepared for submission to CET, a Connecticut certified laboratory for official analysis. Labels are then made for the samples and the chain of custody is prepared. Selected samples are then transferred to the lab and are generally analyzed for Extractable Total Petroleum Hydrocarbons (ETPH), Aromatic & Halogenated Volatile Organics (VOCs and AVOCs), and Polynuclear Aromatic Hydrocarbons (PNAs). . Background samples and field blanks are also prepared. Background Sample. A background sample is a sample collected upgradient of the area of potential contamination where there is little or no chance of migration of the contaminants of concern (EPA 1991g). Background samples are collected from the background reference area (Section 4.5), determine the natural composition and variability of the soil and are considered “clean” samples. Field Blanks. Field blanks are samples prepared in the field using certified clean sand or soil and then submitted to the laboratory for analysis (EPA 1991g). A field blank is used to evaluate contamination error associated with sampling methodology and laboratory procedures. It also provides information about contaminants that may be introduced during sample collection, storage, and, transport. SOIL & ENVIRONMENTAL SERVICES, INC. Permeability testing Soil cores were collected in 2-inch and 3-inch diameter permeameter tubes for soil permeability testing. Tests were conducted by the falling head method for saturated hydraulic conductivity. Core tubes were plastic and metal and core length varied from 6 inches to 12 inches. The larger tubes are used in any soil profile where stones are present to insure water passage during testing. Soil permeability testing followed procedures outlined in the CTDEP Seepage and Pollutant Renovation Analysis for Sewage Disposal Systems” (K. Healy, 1982). Duplicate samples were run on selected soil samples. Permeability: Soil permeability is the quality of the soil that enables water or air to move through it. Accepted, as a measure of this quality is the rate at which a saturated soil transmits water. That rate is the "saturated hydraulic conductivity" of soil physics. In line with conventional usage in the engineering profession and traditional usage in published soil surveys, this rate of flow, principally downward, continues to be expressed as "permeability". It is expressed in inches per hour. Permeability class in/hour very slow <0.06 slow 0.06 - 0.20 moderately slow 0.2 - 0.60 moderate 0.6 - 2.0 moderately rapid 2.0 - 6.0 rapid 6.0 - 20 very rapid >20 Source: NRCS SOIL & ENVIRONMENTAL SERVICES, INC. AOC at generator in C horizon. The massive, firm C horizon was a very fine sandy loam to loamy very fine sand. Permeability was tested and was in NRCS permeability classes of slow (0.06 - 0.2 in/hr.), very slow (.01 - .06 in/hr.), and moderately slow. Soil permeability results at AOC at generator in C horizon at 4-6 feet are as follows: 1 101 C, lvfs, massive K = 0.45 in/hour, 0.9 ft/day 102 massive C, vfsl K = 0.30 in/hour, 0.6 ft/day #103 (fsl, massive, C) K = .39 in/hour, 0.78 ft/day 104 C, lvs, massive K = 0.55 in/hour, 1.1 ft/day 105 massive C, vfsl to fsl K = 0.450 in/hour, 0.9 ft/day #106 (vfsl-vfsl massive, C) K = .29 in/hour, 0.58 ft/day #duplicate 106 (vfsl-vfsl massive, C) K = .33 in/hour, 0.66 ft/day Table#1 - SOIL SAMPLE RESULTS NPU, Stony Brook Site, Oakdale, CT Above RSRs shown in bold Above ND and <RSRs in italics All results in parts per million (ppm) unless noted; ppb - parts per billion ND - Non-detectable NE – Not Established blank – not tested Res. DEC = “residential direct exposure criteria” GAPMC = “GA pollutant mobility criteria” Res Vol (Vapor) volatiles all below RSRs RSRs - CTDEEP “Remediation Standard Regulations” (RSRs), January 1996; Rev 2013. Constituent (s) ETPH Ethylbenzene Toluene Xylenes PNAs Trimethylbenzenes, gasoline breakdown compounds Residential DEC 500 500 500 500 Variable Variable GA PMC 500 10.1 20 19.5 Variable Variable Post-excavation samples 0-8 inches, wetlands #1 bottom ND #2 bottom ND ND #3 bottom ND ND or <RSRs ND or <RSRs ND or <RSRs ND or <RSRs #4 bottom ND #5 bottom ND #6 bottom ND ND or <RSRs ND or <RSRs ND or <RSRs ND or <RSRs #7 bottom ND ND or <RSRs ND or <RSRs ND or <RSRs ND or <RSRs #8 bottom ND #9 bottom ND ND #10 bottom ND #11 sidewall 0-24 inches ND ND or <RSRs ND or <RSRs ND or <RSRs ND or <RSRs #12 bottom 150 ND #12A bottom retest ND #12B bottom retest ND ND ND ND ND #13 bottom ND #14 bottom ND ND or <RSRs ND or <RSRs ND or <RSRs ND or <RSRs Table#1 continued - SOIL SAMPLE RESULTS NPU, Stony Brook Site, Oakdale, CT NOTE: Soils have since been excavated and removed at sample locations #20-1 bottom, 20-2 bottom, 20-3 sidewall, #26 bottom, #29 sidewall, and at #30, 31, and 32 bottoms and sidewalls. Constituent (s) ETPH Ethylbenzene Toluene Xylenes PNAs Trimethylbenzenes, gasoline breakdown compounds Residential DEC 500 500 500 500 Variable Variable GA PMC 500 10.1 20 19.5 Variable Variable Post-excavation samples Generator Area (1st cleanup) #20-1 bottom 6 ft. (soil was removed) #20-2 bottom 3-6 ft. (soil was removed) 4400 ND or <RSRs ND or <RSRs ND or <RSRs >RSRs #20-3 sidewall 3-6 ft. (soil was removed) 3400 <RSRs #21 bottom 4 ft. ND #22 sidewall 1-2.5 ft. ND #24 bottom 4 ft. ND #25 bottom 6 ft. ND ND or <RSRs ND or <RSRs ND or <RSRs ND ND or <RSRs #26 bottom 6 ft. (soil was removed) 5400 <RSRs #27 bottom at 2-3 ft. ND #28 bottom 2 ft. at trench ND #29 sidewall near septic (soil was removed) 760 #30 bottom at 6 ft. (soil was removed) 3100 ND #31 sidewall under asphalt (removed soil) 18,000 ND or <RSRs ND or <RSRs ND or <RSRs ND >RSRs #32 sidewall near building (soil was removed) 1500 ND or <RSRs <RSRs Waste #1 for disposal use 5,200 3.5 ND 29.0 <RSRs >RSRs Table #1 continued - SOIL SAMPLE RESULTS NPU, Stony Brook Site, Oakdale, CT NOTE: Soils were excavated and removed at sample locations #43 sidewall, at composite #43/44 sidewall, and at all soils surrounding #1 Root in C horizon. Constituent (s) ETPH Ethylbenzene Toluene Xylenes PNAs Trimethylbenzenes, gasoline breakdown compounds Residential DEC 500 500 500 500 Variable Variable GA PMC 500 10.1 20 19.5 Variable Variable Post-excavation samples Generator Area (2nd cleanup) #43 sidewall 4-6 ft. (soil removed) 4600 ND ND 7.4 ND #44 sidewall 4-6 ft. 210 ND ND ND <RSRs #45 sidewall 0-3 ft. ND <RSRs #46 sidewall 1-3 ft. ND ND ND ND ND #47 sidewall 4-6 ft. ND #48 sidewall 4-6 ft. ND #43/44 sidewall 4-6 ft. ( soil removed) 4300 ND #50 bottom 6 ft. ND ND ND <RSRs <RSRs #51 bottom 5 ft, 130 #52 bottom 5-6 ft. ND <RSRs ND ND 0.0012 #53 sidewall 2-5 ft. ND #54 sidewall 1-5 ft. 85 #55 sidewall 1-4.5 ft. 510 <RSRs ND <RSRs <RSRs #56 bottom 5-7 ft. ND #57 sidewall 1-5 ft. ND #58 bottom 4-7 ft. ND #60 bottom 4-7 ft. ND ND ND ND <RSRs #61 sidewall 0-3 ft. ND #62 sidewall 0.5-2 ft. ND #63 TP #1 5-9 inches ND #64 TP #2 5-9 inches ND #65 0-12 inches at pipe outfall 490 #1 Root @4-6 ft. in virgin C horizon (removed soil) 5000 ND ND 0.270 2.470 Surface Water @ Stony Brook tributary SW #1 SW #2 ND ND ND ND Above RSRs depicted in bold Above ND and <RSRs in italics All results in parts per million (ppm) unless noted; ppb - parts per billion ND - Non-detectable NE – Not Established blank – not tested Res. DEC = “residential direct exposure criteria” GAPMC = “GA pollutant mobility criteria” Res Vol (Vapor) volatiles all below RSRs RSRs- CTDEEP “Remediation Standard Regulations” (RSRs), January 1996; Rev 2013. SOIL & ENVIRONMENTAL SERVICES, INC. 61 Plants Dam Road, East Lyme, CT 06333 860-739-6691 Fax 739-4150 soilinc@gmail.com Martina A. Castanho – Soil Scientist, CT LEP Certified Professional Soil Scientist #2302 (SSSA) Professional Soil Scientist Member (SSSSNE) CT Licensed Environmental Professional (LEP #236) BS Natural Resources, University of Rhode Island, 1978. Thirty-seven years ex perience Experience: Five years Soil Conservationist and Soil Scientist, USDA-NRCS (SCS). Three years Environmental Scientist, US EPA, SES, Inc. – President, Soil Scientist, CTLEP. Twenty-five years - soil investigations, wetland delineations, Phase I, II, II Environmental Assessments, soil and water sampling, contaminated site remediation, and permeability testing. Donald J. Fortunato – Soil Scientist, CT LEP Certified Professional Soil Scientist #2278 (SSSA) Professional Soil Scientist Member (SSSSNE) CT Licensed Environmental Professional (LEP #235) BS Environmental Science, Stockton University, 1975. Graduate study in soil science, Rutgers University 1977-78. Forty years experience Experience: Nine years District Conservationist, Soil Conservationist, USDA-NRCS (SCS). SES, Inc. - Twenty-seven years SES Soil Scientist, soil investigations, wetland delineations, soil and water sampling, Phase I, II, II Environmental Assessments, contaminated site remediation, and soil permeability testing. APPENDIX !:', / 18"RCP),']1,'=255.40 Wi W'r ·t-lEND ;BENCI-NARK.--. '----&,TOP OF CONC.CURB \!~lEV:~~60·3'- /"",0' RIP RAP "" SPLASH PAD -~ (O£PTH=f.5") wr 14-::'_~~~~-~-'~, ..\"\'y 18"RCP.--'inv=255.40 -'1fI'(iII1;!!:'\: ~!.,.""e.:j ,. Ii!!IV-\1;.J-ld~ \,I ~."1,,-'rl' .-'7n u: ":,~'I,i'.13'x20'RIPRAP SPlASH PAD (DEPTl-I=I.5) B ?END UNITiD.O 86LF-18"RCP S=I.QX \65'x 100'8u/LDIN~ FFE~26200 !F£=25/.00 • f Elev~26()·'o o \. I \ \ ___•••>>--••)>-__~c",-<~.~/----..~'--, '<6'O~~:"~!i:'/1>--~.-------.'--..>----..CONCRETE:TRANSFORMER PAD ~_ __ STANDBY GENS£[OUTDOOR ENCLOSURE _./_ ON CONCRETE PAD ------(~-.... ---- Sample Locations Wetlands Area Source: Green Site Design, NTS See Detail Sheet Woods 63 64 1 2 3 4 5 6 7 8 9 1011 SW 12 12A 12B 13 14 15 SW #1 SW #2 »:~'o· 0./ o<0C\j I \ \ \ / o \ ff -260 9E\e'J-- -2------ Generator AOC 22 SW 55 SW 62 SW 25 B 25 B 24 B 54 SW 53 SW 51 B 50 B 52 B 59 B 27 B 60 B 57 SW 56 B 58 B old #32 removed old #26 removed old #29 removed old #30 removed old #31 removed Generator AOC 28 B 48 SW 22 SW 44 SW 43 SW 46 SW 45SW 47 SW old #20-1, 20-2, and 20-3 removed For Reference 45 SW 43 SW 44 SW 48 SW 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 A B C D 0 Data set ETPH ppm 210 36 36 36 36 36 36 130 36 36 85 510 36 36 36 36 36 36 The CTDEEP 95% UCL protocol. A B LcDEFGHJK 1 Normal Background Statistics for Uncensored Full Data Sets 2 3 User Selected Options 4 DateITime of Computation ProUCL 5.112/21/2016 3:52:45 PM 5 From File 1.xls 6 Full Precision OFF 7 Confidence Coefficient 95% 8 Coverage 95% 9 New or Future K Observations 10 11 CO 12 13 General Statistics 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 Total Number of Observations 18 Number of Distinct Observations 5 Minimum 36 First Quartile 36 Second Largest 210 Median 36 Maximum 510 Third Quartile 36 Mean 79.94 SD 116.7 Coefficient of Variation 1.459 Skewness 3.361 Mean of logged Data 3.948 SO of logged Data 0.772 Critical Values for Background Threshold Values (BTVs) Tolerance Factor K (For UTL)2.453 d2max (for USL) Shapiro Wilk Test Statistic 5%Shapiro Wilk Critical Value Lilliefors Test Statistic Normal GOF Test 0.448 0.897 0.425 Shapiro Wilk GOF Test Data Not Normal at 5%Significance Level Lilliefors GOF Test 5%Lilliefors Critical Value 0.202 Data Not Normal at 5%Significance Level Data Not Normal at 5%Significance Level Background Statistics Assuming Normal Distribution 95%UTL with 95%Coverage 3662 95%UPL (t)288.5 95%USL 372.1 90%Percentile (z) 95%Percentile (z) 99%Percentile (z) 229.5 271.9 351.4 38 39 40 41 42 Note:The use of USL tends to yield a conservative estimate of BTV,especially when the sample size starts exceeding 20. Therefore,one may use USL to estimate a BTV only when the data set represents a background data set free of outliers and consists of observations collected from clean unimpacted locations. The use of USL tends to provide a balance between false positives and false negatives provided the data represents a background data set and when many onsite observations need to be compared with the BTV. 37 I 2.~41 IIIit I 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 A B C D E F G H I J K L Normal UCL Statistics for Uncensored Full Data Sets User Selected Options Date/Time of Computation ProUCL 5.112/21/2016 1:43:55 PM From File 1.xls Full Precision OFF Confidence Coefficient 95% C0 General Statistics Total Number of Observations 18 Number of Distinct Observations 5 Number of Missing Observations 0 Minimum 36 Mean 79.94 Maximum 510 Median 36 SD 116.7 SD of logged Data 0.772 Coefficient of Variation 1.459 Skewness 3.361 Normal GOF Test Shapiro Wilk Test Statistic 0.448 Shapiro Wilk GOF Test 5% Shapiro Wilk Critical Value 0.897 Data Not Normal at 5% Significance Level Lilliefors Test Statistic 0.425 Lilliefors GOF Test 5% Lilliefors Critical Value 0.202 Data Not Normal at 5% Significance Level Data Not Normal at 5% Significance Level Assuming Normal Distribution 95% Normal UCL 95% UCLs (Adjusted for Skewness) 95% Student's-t UCL 127.8 95% Adjusted-CLT UCL (Chen-1995) 148.5 95% Modified-t UCL (Johnson-1978) 131.4 These recommendations are based upon the results of the simulation studies summarized in Singh, Maichle, and Lee (2006). However, simulations results will not cover all Real World data sets; for additional insight the user may want to consult a statistician. Suggested UCL to Use Data do not follow a Discernible Distribution, May want to try Nonparametric UCLs Note: Suggestions regarding the selection of a 95% UCL are provided to help the user to select the most appropriate 95% UCL. Recommendations are based upon data size, data distribution, and skewness. B C D E F G H I Nonparametric UCL Statistics for Uncensored Full Data Sets J K 2 3 User Selected Options 4 DatelTime of Computation ProUCL 5.112/21/20163:51 :31 PM 5 From File 1.xls 6 Full Precision OFF 7 Confidence Coefficient 95% 8·N.umberof Bootstrap Operations 2000 9 10 11 CO 12 13 14 15 16 17 18 19 20 21 22 General Statistics Total Number of Observations 18 Number of Distinct Observations 5 Number of Missing Observations 0 Mean 79.94 Median 36 Std.Error of Mean 27.5 Skewness 3.361 SD of logged Data 0.772 Minimum 36 Maximum 510 SD 116.7 Coefficient of Variation 1.459 Mean of logged Data 3.948 Nonparametric Distribution Free UCL Statistics Data do not follow a Discernible Distribution (0.05) 24 25 26 27 28 29- 30 31 32 33 34 35 36 Assuming Normal Distribution 95%Normal UCL 95%UCLs (Adjusted for Skewness) 95%Adjusted-Cl,T UCL (Chen-1995)148.5 95%Modified-t UCL (Johnson-1978)131.4 95%Student's-t UCL 127.8 Nonparametric Distribution Free UCLs 95%CLT UCL 95%Standard Bootstrap UCL 95%Hall's Bootstrap UCL 95%BCA Bootstrap UCL 90%Chebyshev(Mean,Sd)UCL 97.5%Chebyshev(Mean,Sd)UCL 125.2 123.7 276.2 149.2 162.4 251.7 95%Jackknife UCL 95%Bootstrap-t UCL 95%Percentile Bootstrap UCL 127.8 252.3 128.2 95%Chebyshev(Mean,Sd)UCL 99%Chebyshev(Mean,Sd)UCL 199.8 353.6 37 38 ~9 40 Suggested UCL to Use 95%Chebyshev (Mean,Sd)UCl 199.8 4·Note:Suggestions regarding the selection of a 95%UCL are provided to help the user to select the most appropriate 95%UCL. Recommendations are based upon data size,data distribution,and skewness. These recommendations are based upon the results of the simulation studies summarized in Singh,Maichle,and Lee (2006). However,simulations results will not cover all Real World data sets:for additional insight the user may want to consult a statistician. 42 43 44 45 L 1 1I { IIiI ! I --..---------.-.--.--~---1-----;"lHistogramforCOreo181i15i , I Number ofVa!ues I Minimum 36.0°1I 510.00 !Maximum i 14 SD I I,4 116.681 I Skewness 3.361 I Kurtosis 12.011 I 13 DMean 79.941 I I o Median 36.00\.I oNormal DistributionI [ I 12 o Less Bins IoMoreBins I 1.1 IIIIIIIIII I 1D I I I I -g I I II i ('l-I ?:.c::=e1g.14\Ill:7I IIIIIiI6II I II!'5 II I II I i I ~ I II 1II I I II I I II~II IIII I I I I I I I !I I 0 0 n 0 o IDv I--------- 47 95 142 190 237 284 332 379 427 47.: I IJL Page 1 of 2 11/22/2016 1:28 PM UST Compliance Inspection Checklist Connecticut Department of Energy and Environmental Protection Storage Tank and PCB Enforcement Unit 79 Elm Street, Hartford, CT 06106 860-424-3374 This is a compliance audit only. It is not a full inspection and not all compliance areas have been reviewed. GENERAL: Inspection Date: 11/22/2016 Site ID: 86-50365 Inspector George Purple Site Name Cherry Lane Reason Compliance Site Address 260 Cherry Lane MONTVILLE, CT Inspection Type Partial Inspection Contacts Contact Type Contact Information Owner CITY OF NORWICH, 16 S. Golden st. NORWICH, CT 06360, Phone: (860) 823-4168-, Email: markdecker@npumail.com Tank ID: A-1 - Currently In Use (1000 gallons) – Installed: 1/1/0001 Construction Fiberglass Reinforced Plastic Life Expectancy 30 years Construction Notes Tank Options Double Walled Corrosion Protection Type: Not Required Impressed Current System Structure to soil voltage Compartment: a - Diesel (1000 gallons) Spill Prevention Spill Containment Overfill Prevention Product Notes Spill Prevention Note Release Detection No release detection required Piping – Installed: Construction Copper Corrosion Protection Type Construction Notes Piping Options Metallic piping isolated from soil and water, Metallic fittings isolated from soil and water Piping Release Detection Pump Type American Suction (Check Valve is at Tank) Line Leak Detector Primary Method Narrative Comments The tank was installed late 94 to mid 95. Tank is a double walled FRP with interstitial sensor. The release was caused by the contractor when they moved the old diesel generator it crimped the return line at the tank. Most of the site has been dug up and confirmation samples have been takken. They will be submitted when they respond to the NOV. The current thought is to remove the tank because the new generator has a 850 gallon belly tank. Potential Violations Regulation: CT state regulation CGS 22a-430 Violation Reason: An unpermitted discharge of regulated substance from a UST system has occurred. Page 2 of 2 11/22/2016 1:28 PM Required Action: Report the spill to CT DEEP at (860) 424-3338 and hire a spill clean-up contractor and/or an environmental consultant to remediate contaminated soils and/or groundwater to applicable standards. Regulation: CT state regulation CGS 22a-449(e) Violation Reason: The owner or operator has failed to submit the requisite annual UST facility notification and/or the requisite annual UST facility fee(s). Required Action: Submit the requisite annual UST facility notification form and/or the requisite annual UST facility fee(s). Regulation: CT state regulation 102(a)(5)(A)(ii) Violation Reason: Could not verify that the overfill protection device was installed at the required 90% alert or 95% shut off level. Required Action: Please provide overfill protection installation (including measurements) at the 90% alert and 95% shut off level. Applies To: TANK A-1 (Containing Diesel with Capacity of 1000 gallons) Inspector Signature Recipient Signature CITY OF NORWICH Recipient Printed Name Facility Owner Position/Title From: Fabris, Gemma Sent: Tuesday, November 22, 2016 2:44 PM To: Valerie Kent Cc: Laura Huren; DEMHS-DL HMGP Subject: RE: NPU Stony Brook Water Treatment Plant Generator - FEMA-DR-4046-CT-16R Valerie, Thank you for your below synopsis of the situation regarding installation of a generator at Stony Brook WTP. Basically, in order for the project to be found eligible and in compliance and for the City to be reimbursed you will need to provide the following:  Letter from appropriate official stating that all work has been completed satisfactorily and in compliance with all local state and Federal rules and regulations. (this obviously includes any remediation work that had to be done).  Reimbursement documentation showing all project costs, clearly identified by invoice and checks showing paid. (meaning, you will have had to complete all final payments). All work must be completed on this grant by 2/25/2017 and payments should be processed ( you can submit for full reimbursement up until this date)– if you do not think this will be done in time please sent me a letter requesting a time extension that outlines reasons for delay and projected completion date. I will need to send up to FEMA for their approval. You would need to get this in to me within the next week or so if possible to give FEMA adequate time to review. Any questions please do not hesitate to contact me. Thank you, Gemma FEMA email LAB DATA 80 Lupes Drive Stratford, CT 06615 Tel: (203) 377-9984 Fax: (203) 377-9952 e-mail: cet1@cetlabs.com Client:Mr. Don Fortunato Soil & Environmental Service 61 Plants Dam Road East Lyme, CT 06333 Analytical Report CET# 6100133 Report Date:October 11, 2016 Project: NPU Stony Brook, Montville Rhode Island Certification: 199Massachusetts laboratory Certificate: M-CT903 Connecticut Laboratory Certificate: PH 0116 New York Certification: 11982 Page 1 of 28 Project: NPU Stony Brook, Montville CET # : 6100133 Sample ID Laboratory ID Matrix Collection Date/Time Receipt Date SAMPLE SUMMARY The sample(s) were received at 3.5 C. This report contains analytical data associated with following samples only. 3 0-8in 6100133-01 Soil 10/06/201610/05/2016 6 0-8in 6100133-02 Soil 10/06/201610/05/2016 7 0-8in 6100133-03 Soil 10/06/201610/05/2016 11 SW 0-24in 6100133-04 Soil 10/06/201610/05/2016 14 0-8in 6100133-05 Soil 10/06/201610/05/2016 20-2 SW 3-6ft 6100133-06 Soil 10/06/201610/05/2016 Notes Date/Time AnalyzedPreparedBatchDilutionRLResultLaboratory ID Client Sample ID Units Analyst: MRH Matrix: Soil Analyte: Total Solids [EPA 160.3 modified] 76 10/07/2016 10/07/2016 14:406100133-01 %3 0-8in 1.0 1 B6J0710 70 10/07/2016 10/07/2016 14:406100133-02 %6 0-8in 1.0 1 B6J0710 60 10/07/2016 10/07/2016 14:406100133-03 %7 0-8in 1.0 1 B6J0710 74 10/07/2016 10/07/2016 14:406100133-04 %11 SW 0-24in 1.0 1 B6J0710 74 10/07/2016 10/07/2016 14:406100133-05 %14 0-8in 1.0 1 B6J0710 67 10/07/2016 10/07/2016 14:406100133-06 %20-2 SW 3-6ft 1.0 1 B6J0710 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 2 of 28 Project: NPU Stony Brook, Montville CET # : 6100133 Client Sample ID 3 0-8in Lab ID: 6100133-01 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6J0805 10/08/2016 10/08/2016 13:5866EPA 3550C Surrogate: Octacosane 83.5 %10/08/2016 10/08/2016 13:58B6J080550 - 150 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Methyl-t-Butyl Ether (MTBE)ND 1.76 B6J1017 10/10/2016 10/10/2016 15:195.8 EPA 5035A-L Benzene ND 1.76 B6J1017 10/10/2016 10/10/2016 15:195.8 EPA 5035A-L Toluene ND 1.76 B6J1017 10/10/2016 10/10/2016 15:195.8 EPA 5035A-L Chlorobenzene ND 1.76 B6J1017 10/10/2016 10/10/2016 15:195.8 EPA 5035A-L Ethylbenzene ND 1.76 B6J1017 10/10/2016 10/10/2016 15:195.8 EPA 5035A-L m+p Xylenes 15 1.76 B6J1017 10/10/2016 10/10/2016 15:195.8 EPA 5035A-L o-Xylene ND 1.76 B6J1017 10/10/2016 10/10/2016 15:195.8 EPA 5035A-L Styrene ND 1.76 B6J1017 10/10/2016 10/10/2016 15:195.8 EPA 5035A-L Isopropylbenzene ND 1.76 B6J1017 10/10/2016 10/10/2016 15:195.8 EPA 5035A-L Bromobenzene ND 1.76 B6J1017 10/10/2016 10/10/2016 15:195.8 EPA 5035A-L n-Propylbenzene ND 1.76 B6J1017 10/10/2016 10/10/2016 15:195.8 EPA 5035A-L 2-Chlorotoluene ND 1.76 B6J1017 10/10/2016 10/10/2016 15:195.8 EPA 5035A-L 4-Chlorotoluene ND 1.76 B6J1017 10/10/2016 10/10/2016 15:195.8 EPA 5035A-L 1,3,5-Trimethylbenzene ND 1.76 B6J1017 10/10/2016 10/10/2016 15:195.8 EPA 5035A-L tert-Butylbenzene ND 1.76 B6J1017 10/10/2016 10/10/2016 15:195.8 EPA 5035A-L 1,2,4-Trimethylbenzene 8.6 1.76 B6J1017 10/10/2016 10/10/2016 15:195.8 EPA 5035A-L sec-Butylbenzene ND 1.76 B6J1017 10/10/2016 10/10/2016 15:195.8 EPA 5035A-L 1,3-Dichlorobenzene ND 1.76 B6J1017 10/10/2016 10/10/2016 15:195.8 EPA 5035A-L 4-Isopropyltoluene ND 1.76 B6J1017 10/10/2016 10/10/2016 15:195.8 EPA 5035A-L 1,4-Dichlorobenzene ND 1.76 B6J1017 10/10/2016 10/10/2016 15:195.8 EPA 5035A-L 1,2-Dichlorobenzene ND 1.76 B6J1017 10/10/2016 10/10/2016 15:195.8 EPA 5035A-L n-Butylbenzene ND 1.76 B6J1017 10/10/2016 10/10/2016 15:195.8 EPA 5035A-L 1,2,4-Trichlorobenzene ND 1.76 B6J1017 10/10/2016 10/10/2016 15:195.8 EPA 5035A-L Hexachlorobutadiene ND 1.76 B6J1017 10/10/2016 10/10/2016 15:195.8 EPA 5035A-L Naphthalene ND 1.76 B6J1017 10/10/2016 10/10/2016 15:195.8 EPA 5035A-L 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 3 of 28 Project: NPU Stony Brook, Montville CET # : 6100133 Client Sample ID 3 0-8in Lab ID: 6100133-01 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics 1,2,3-Trichlorobenzene ND 1.76 B6J1017 10/10/2016 10/10/2016 15:195.8 EPA 5035A-L Surrogate: 1,2-Dichloroethane-d4 92.8 %10/10/2016 10/10/2016 15:19B6J101770 - 130 Surrogate: Toluene-d8 91.0 %10/10/2016 10/10/2016 15:19B6J101770 - 130 Surrogate: 4-Bromofluorobenzene 78.5 %10/10/2016 10/10/2016 15:19B6J101770 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 4 of 28 Project: NPU Stony Brook, Montville CET # : 6100133 Client Sample ID 6 0-8in Lab ID: 6100133-02 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6J0805 10/08/2016 10/08/2016 15:3072EPA 3550C Surrogate: Octacosane 78.0 %10/08/2016 10/08/2016 15:30B6J080550 - 150 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Methyl-t-Butyl Ether (MTBE)ND 1.43 B6J0732 10/07/2016 10/07/2016 22:105.1 EPA 5035A-L Benzene ND 1.43 B6J0732 10/07/2016 10/07/2016 22:105.1 EPA 5035A-L Toluene 7.7 1.43 B6J0732 10/07/2016 10/07/2016 22:105.1 EPA 5035A-L Chlorobenzene ND 1.43 B6J0732 10/07/2016 10/07/2016 22:105.1 EPA 5035A-L Ethylbenzene 14 1.43 B6J0732 10/07/2016 10/07/2016 22:105.1 EPA 5035A-L m+p Xylenes 72 1.43 B6J0732 10/07/2016 10/07/2016 22:105.1 EPA 5035A-L o-Xylene 38 1.43 B6J0732 10/07/2016 10/07/2016 22:105.1 EPA 5035A-L Styrene ND 1.43 B6J0732 10/07/2016 10/07/2016 22:105.1 EPA 5035A-L Isopropylbenzene 5.4 1.43 B6J0732 10/07/2016 10/07/2016 22:105.1 EPA 5035A-L Bromobenzene ND 1.43 B6J0732 10/07/2016 10/07/2016 22:105.1 EPA 5035A-L n-Propylbenzene 35 1.43 B6J0732 10/07/2016 10/07/2016 22:105.1 EPA 5035A-L 2-Chlorotoluene ND 1.43 B6J0732 10/07/2016 10/07/2016 22:105.1 EPA 5035A-L 4-Chlorotoluene ND 1.43 B6J0732 10/07/2016 10/07/2016 22:105.1 EPA 5035A-L 1,3,5-Trimethylbenzene 88 1.43 B6J0732 10/07/2016 10/07/2016 22:105.1 EPA 5035A-L tert-Butylbenzene ND 1.43 B6J0732 10/07/2016 10/07/2016 22:105.1 EPA 5035A-L 1,2,4-Trimethylbenzene 310 1.43 B6J0732 10/07/2016 10/07/2016 22:105.1 EPA 5035A-L sec-Butylbenzene 14 1.43 B6J0732 10/07/2016 10/07/2016 22:105.1 EPA 5035A-L 1,3-Dichlorobenzene ND 1.43 B6J0732 10/07/2016 10/07/2016 22:105.1 EPA 5035A-L 4-Isopropyltoluene 16 1.43 B6J0732 10/07/2016 10/07/2016 22:105.1 EPA 5035A-L 1,4-Dichlorobenzene ND 1.43 B6J0732 10/07/2016 10/07/2016 22:105.1 EPA 5035A-L 1,2-Dichlorobenzene ND 1.43 B6J0732 10/07/2016 10/07/2016 22:105.1 EPA 5035A-L n-Butylbenzene 25 1.43 B6J0732 10/07/2016 10/07/2016 22:105.1 EPA 5035A-L 1,2,4-Trichlorobenzene ND 1.43 B6J0732 10/07/2016 10/07/2016 22:105.1 EPA 5035A-L Hexachlorobutadiene ND 1.43 B6J0732 10/07/2016 10/07/2016 22:105.1 EPA 5035A-L *C1 Naphthalene 28 1.43 B6J0732 10/07/2016 10/07/2016 22:105.1 EPA 5035A-L 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 5 of 28 Project: NPU Stony Brook, Montville CET # : 6100133 Client Sample ID 6 0-8in Lab ID: 6100133-02 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics 1,2,3-Trichlorobenzene ND 1.43 B6J0732 10/07/2016 10/07/2016 22:105.1 EPA 5035A-L Surrogate: 1,2-Dichloroethane-d4 98.7 %10/07/2016 10/07/2016 22:10B6J073270 - 130 Surrogate: Toluene-d8 95.3 %10/07/2016 10/07/2016 22:10B6J073270 - 130 Surrogate: 4-Bromofluorobenzene 81.2 %10/07/2016 10/07/2016 22:10B6J073270 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 6 of 28 Project: NPU Stony Brook, Montville CET # : 6100133 Client Sample ID 7 0-8in Lab ID: 6100133-03 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6J0805 10/08/2016 10/08/2016 15:5284EPA 3550C Surrogate: Octacosane 82.4 %10/08/2016 10/08/2016 15:52B6J080550 - 150 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Methyl-t-Butyl Ether (MTBE)ND 1.86 B6J0732 10/07/2016 10/07/2016 22:327.8 EPA 5035A-L Benzene ND 1.86 B6J0732 10/07/2016 10/07/2016 22:327.8 EPA 5035A-L Toluene ND 1.86 B6J0732 10/07/2016 10/07/2016 22:327.8 EPA 5035A-L Chlorobenzene ND 1.86 B6J0732 10/07/2016 10/07/2016 22:327.8 EPA 5035A-L Ethylbenzene ND 1.86 B6J0732 10/07/2016 10/07/2016 22:327.8 EPA 5035A-L m+p Xylenes 9.2 1.86 B6J0732 10/07/2016 10/07/2016 22:327.8 EPA 5035A-L o-Xylene ND 1.86 B6J0732 10/07/2016 10/07/2016 22:327.8 EPA 5035A-L Styrene ND 1.86 B6J0732 10/07/2016 10/07/2016 22:327.8 EPA 5035A-L Isopropylbenzene ND 1.86 B6J0732 10/07/2016 10/07/2016 22:327.8 EPA 5035A-L Bromobenzene ND 1.86 B6J0732 10/07/2016 10/07/2016 22:327.8 EPA 5035A-L n-Propylbenzene ND 1.86 B6J0732 10/07/2016 10/07/2016 22:327.8 EPA 5035A-L 2-Chlorotoluene ND 1.86 B6J0732 10/07/2016 10/07/2016 22:327.8 EPA 5035A-L 4-Chlorotoluene ND 1.86 B6J0732 10/07/2016 10/07/2016 22:327.8 EPA 5035A-L 1,3,5-Trimethylbenzene ND 1.86 B6J0732 10/07/2016 10/07/2016 22:327.8 EPA 5035A-L tert-Butylbenzene ND 1.86 B6J0732 10/07/2016 10/07/2016 22:327.8 EPA 5035A-L 1,2,4-Trimethylbenzene 18 1.86 B6J0732 10/07/2016 10/07/2016 22:327.8 EPA 5035A-L sec-Butylbenzene ND 1.86 B6J0732 10/07/2016 10/07/2016 22:327.8 EPA 5035A-L 1,3-Dichlorobenzene ND 1.86 B6J0732 10/07/2016 10/07/2016 22:327.8 EPA 5035A-L 4-Isopropyltoluene ND 1.86 B6J0732 10/07/2016 10/07/2016 22:327.8 EPA 5035A-L 1,4-Dichlorobenzene ND 1.86 B6J0732 10/07/2016 10/07/2016 22:327.8 EPA 5035A-L 1,2-Dichlorobenzene ND 1.86 B6J0732 10/07/2016 10/07/2016 22:327.8 EPA 5035A-L n-Butylbenzene ND 1.86 B6J0732 10/07/2016 10/07/2016 22:327.8 EPA 5035A-L 1,2,4-Trichlorobenzene ND 1.86 B6J0732 10/07/2016 10/07/2016 22:327.8 EPA 5035A-L Hexachlorobutadiene ND 1.86 B6J0732 10/07/2016 10/07/2016 22:327.8 EPA 5035A-L *C1 Naphthalene ND 1.86 B6J0732 10/07/2016 10/07/2016 22:327.8 EPA 5035A-L 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 7 of 28 Project: NPU Stony Brook, Montville CET # : 6100133 Client Sample ID 7 0-8in Lab ID: 6100133-03 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics 1,2,3-Trichlorobenzene ND 1.86 B6J0732 10/07/2016 10/07/2016 22:327.8 EPA 5035A-L Surrogate: 1,2-Dichloroethane-d4 101 %10/07/2016 10/07/2016 22:32B6J073270 - 130 Surrogate: Toluene-d8 95.4 %10/07/2016 10/07/2016 22:32B6J073270 - 130 Surrogate: 4-Bromofluorobenzene 79.6 %10/07/2016 10/07/2016 22:32B6J073270 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 8 of 28 Project: NPU Stony Brook, Montville CET # : 6100133 Client Sample ID 11 SW 0-24in Lab ID: 6100133-04 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6J0805 10/08/2016 10/08/2016 16:1567EPA 3550C Surrogate: Octacosane 86.5 %10/08/2016 10/08/2016 16:15B6J080550 - 150 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: TWFVolatile Organics Methyl-t-Butyl Ether (MTBE)ND 94.88 B6J1018 10/10/2016 10/10/2016 15:37320EPA 5035A-H Benzene ND 94.88 B6J1018 10/10/2016 10/10/2016 15:37320EPA 5035A-H Toluene ND 94.88 B6J1018 10/10/2016 10/10/2016 15:37320EPA 5035A-H Chlorobenzene ND 94.88 B6J1018 10/10/2016 10/10/2016 15:37320EPA 5035A-H Ethylbenzene ND 94.88 B6J1018 10/10/2016 10/10/2016 15:37320EPA 5035A-H m+p Xylenes 770 94.88 B6J1018 10/10/2016 10/10/2016 15:37320EPA 5035A-H o-Xylene 390 94.88 B6J1018 10/10/2016 10/10/2016 15:37320EPA 5035A-H Styrene ND 94.88 B6J1018 10/10/2016 10/10/2016 15:37320EPA 5035A-H Isopropylbenzene ND 94.88 B6J1018 10/10/2016 10/10/2016 15:37320EPA 5035A-H Bromobenzene ND 94.88 B6J1018 10/10/2016 10/10/2016 15:37320EPA 5035A-H n-Propylbenzene ND 94.88 B6J1018 10/10/2016 10/10/2016 15:37320EPA 5035A-H 2-Chlorotoluene ND 94.88 B6J1018 10/10/2016 10/10/2016 15:37320EPA 5035A-H 4-Chlorotoluene ND 94.88 B6J1018 10/10/2016 10/10/2016 15:37320EPA 5035A-H 1,3,5-Trimethylbenzene 420 94.88 B6J1018 10/10/2016 10/10/2016 15:37320EPA 5035A-H tert-Butylbenzene ND 94.88 B6J1018 10/10/2016 10/10/2016 15:37320EPA 5035A-H 1,2,4-Trimethylbenzene 1400 94.88 B6J1018 10/10/2016 10/10/2016 15:37320EPA 5035A-H sec-Butylbenzene ND 94.88 B6J1018 10/10/2016 10/10/2016 15:37320EPA 5035A-H 1,3-Dichlorobenzene ND 94.88 B6J1018 10/10/2016 10/10/2016 15:37320EPA 5035A-H 4-Isopropyltoluene ND 94.88 B6J1018 10/10/2016 10/10/2016 15:37320EPA 5035A-H 1,4-Dichlorobenzene ND 94.88 B6J1018 10/10/2016 10/10/2016 15:37320EPA 5035A-H 1,2-Dichlorobenzene ND 94.88 B6J1018 10/10/2016 10/10/2016 15:37320EPA 5035A-H n-Butylbenzene ND 94.88 B6J1018 10/10/2016 10/10/2016 15:37320EPA 5035A-H 1,2,4-Trichlorobenzene ND 94.88 B6J1018 10/10/2016 10/10/2016 15:37320EPA 5035A-H Hexachlorobutadiene ND 94.88 B6J1018 10/10/2016 10/10/2016 15:37320EPA 5035A-H Naphthalene ND 94.88 B6J1018 10/10/2016 10/10/2016 15:37320EPA 5035A-H 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 9 of 28 Project: NPU Stony Brook, Montville CET # : 6100133 Client Sample ID 11 SW 0-24in Lab ID: 6100133-04 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: TWFVolatile Organics 1,2,3-Trichlorobenzene ND 94.88 B6J1018 10/10/2016 10/10/2016 15:37320EPA 5035A-H Surrogate: 1,2-Dichloroethane-d4 95.4 %10/10/2016 10/10/2016 15:37B6J101870 - 130 Surrogate: Toluene-d8 101 %10/10/2016 10/10/2016 15:37B6J101870 - 130 Surrogate: 4-Bromofluorobenzene 99.5 %10/10/2016 10/10/2016 15:37B6J101870 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 10 of 28 Project: NPU Stony Brook, Montville CET # : 6100133 Client Sample ID 14 0-8in Lab ID: 6100133-05 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6J0805 10/08/2016 10/08/2016 16:3867EPA 3550C Surrogate: Octacosane 79.4 %10/08/2016 10/08/2016 16:38B6J080550 - 150 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Methyl-t-Butyl Ether (MTBE)ND 1.84 B6J1017 10/10/2016 10/10/2016 15:416.2 EPA 5035A-L Benzene ND 1.84 B6J1017 10/10/2016 10/10/2016 15:416.2 EPA 5035A-L Toluene ND 1.84 B6J1017 10/10/2016 10/10/2016 15:416.2 EPA 5035A-L Chlorobenzene ND 1.84 B6J1017 10/10/2016 10/10/2016 15:416.2 EPA 5035A-L Ethylbenzene ND 1.84 B6J1017 10/10/2016 10/10/2016 15:416.2 EPA 5035A-L m+p Xylenes ND 1.84 B6J1017 10/10/2016 10/10/2016 15:416.2 EPA 5035A-L o-Xylene ND 1.84 B6J1017 10/10/2016 10/10/2016 15:416.2 EPA 5035A-L Styrene ND 1.84 B6J1017 10/10/2016 10/10/2016 15:416.2 EPA 5035A-L Isopropylbenzene ND 1.84 B6J1017 10/10/2016 10/10/2016 15:416.2 EPA 5035A-L Bromobenzene ND 1.84 B6J1017 10/10/2016 10/10/2016 15:416.2 EPA 5035A-L n-Propylbenzene ND 1.84 B6J1017 10/10/2016 10/10/2016 15:416.2 EPA 5035A-L 2-Chlorotoluene ND 1.84 B6J1017 10/10/2016 10/10/2016 15:416.2 EPA 5035A-L 4-Chlorotoluene ND 1.84 B6J1017 10/10/2016 10/10/2016 15:416.2 EPA 5035A-L 1,3,5-Trimethylbenzene ND 1.84 B6J1017 10/10/2016 10/10/2016 15:416.2 EPA 5035A-L tert-Butylbenzene ND 1.84 B6J1017 10/10/2016 10/10/2016 15:416.2 EPA 5035A-L 1,2,4-Trimethylbenzene ND 1.84 B6J1017 10/10/2016 10/10/2016 15:416.2 EPA 5035A-L sec-Butylbenzene ND 1.84 B6J1017 10/10/2016 10/10/2016 15:416.2 EPA 5035A-L 1,3-Dichlorobenzene ND 1.84 B6J1017 10/10/2016 10/10/2016 15:416.2 EPA 5035A-L 4-Isopropyltoluene ND 1.84 B6J1017 10/10/2016 10/10/2016 15:416.2 EPA 5035A-L 1,4-Dichlorobenzene ND 1.84 B6J1017 10/10/2016 10/10/2016 15:416.2 EPA 5035A-L 1,2-Dichlorobenzene ND 1.84 B6J1017 10/10/2016 10/10/2016 15:416.2 EPA 5035A-L n-Butylbenzene ND 1.84 B6J1017 10/10/2016 10/10/2016 15:416.2 EPA 5035A-L 1,2,4-Trichlorobenzene ND 1.84 B6J1017 10/10/2016 10/10/2016 15:416.2 EPA 5035A-L Hexachlorobutadiene ND 1.84 B6J1017 10/10/2016 10/10/2016 15:416.2 EPA 5035A-L Naphthalene ND 1.84 B6J1017 10/10/2016 10/10/2016 15:416.2 EPA 5035A-L 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 11 of 28 Project: NPU Stony Brook, Montville CET # : 6100133 Client Sample ID 14 0-8in Lab ID: 6100133-05 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics 1,2,3-Trichlorobenzene ND 1.84 B6J1017 10/10/2016 10/10/2016 15:416.2 EPA 5035A-L Surrogate: 1,2-Dichloroethane-d4 103 %10/10/2016 10/10/2016 15:41B6J101770 - 130 Surrogate: Toluene-d8 81.2 %10/10/2016 10/10/2016 15:41B6J101770 - 130 Surrogate: 4-Bromofluorobenzene 95.3 %10/10/2016 10/10/2016 15:41B6J101770 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 12 of 28 Project: NPU Stony Brook, Montville CET # : 6100133 Client Sample ID 20-2 SW 3-6ft Lab ID: 6100133-06 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH 4400 1 B6J0805 10/08/2016 10/08/2016 17:0175EPA 3550C 2 Surrogate: Octacosane 79.5 %10/08/2016 10/08/2016 17:01B6J080550 - 150 2 C9-C28 Fuel Oil Range Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Methyl-t-Butyl Ether (MTBE)ND 91.41 B6J0733 10/07/2016 10/07/2016 21:27340EPA 5035A-H Benzene ND 91.41 B6J0733 10/07/2016 10/07/2016 21:27340EPA 5035A-H Toluene 530 91.41 B6J0733 10/07/2016 10/07/2016 21:27340EPA 5035A-H Chlorobenzene ND 91.41 B6J0733 10/07/2016 10/07/2016 21:27340EPA 5035A-H Ethylbenzene 2600 91.41 B6J0733 10/07/2016 10/07/2016 21:27340EPA 5035A-H m+p Xylenes 12000 91.41 B6J0733 10/07/2016 10/07/2016 21:27340EPA 5035A-H o-Xylene 6000 91.41 B6J0733 10/07/2016 10/07/2016 21:27340EPA 5035A-H Styrene ND 91.41 B6J0733 10/07/2016 10/07/2016 21:27340EPA 5035A-H Isopropylbenzene 890 91.41 B6J0733 10/07/2016 10/07/2016 21:27340EPA 5035A-H Bromobenzene ND 91.41 B6J0733 10/07/2016 10/07/2016 21:27340EPA 5035A-H n-Propylbenzene 3400 91.41 B6J0733 10/07/2016 10/07/2016 21:27340EPA 5035A-H 2-Chlorotoluene ND 91.41 B6J0733 10/07/2016 10/07/2016 21:27340EPA 5035A-H 4-Chlorotoluene ND 91.41 B6J0733 10/07/2016 10/07/2016 21:27340EPA 5035A-H 1,3,5-Trimethylbenzene 7900 91.41 B6J0733 10/07/2016 10/07/2016 21:27340EPA 5035A-H tert-Butylbenzene ND 91.41 B6J0733 10/07/2016 10/07/2016 21:27340EPA 5035A-H 1,2,4-Trimethylbenzene 26000 91.41 B6J0733 10/07/2016 10/07/2016 21:27340EPA 5035A-H sec-Butylbenzene 1600 91.41 B6J0733 10/07/2016 10/07/2016 21:27340EPA 5035A-H 1,3-Dichlorobenzene ND 91.41 B6J0733 10/07/2016 10/07/2016 21:27340EPA 5035A-H 4-Isopropyltoluene 940 91.41 B6J0733 10/07/2016 10/07/2016 21:27340EPA 5035A-H 1,4-Dichlorobenzene ND 91.41 B6J0733 10/07/2016 10/07/2016 21:27340EPA 5035A-H 1,2-Dichlorobenzene ND 91.41 B6J0733 10/07/2016 10/07/2016 21:27340EPA 5035A-H n-Butylbenzene 3200 91.41 B6J0733 10/07/2016 10/07/2016 21:27340EPA 5035A-H 1,2,4-Trichlorobenzene ND 91.41 B6J0733 10/07/2016 10/07/2016 21:27340EPA 5035A-H Hexachlorobutadiene ND 91.41 B6J0733 10/07/2016 10/07/2016 21:27340EPA 5035A-H *C1 Naphthalene 3700 91.41 B6J0733 10/07/2016 10/07/2016 21:27340EPA 5035A-H 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 13 of 28 Project: NPU Stony Brook, Montville CET # : 6100133 Client Sample ID 20-2 SW 3-6ft Lab ID: 6100133-06 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics 1,2,3-Trichlorobenzene ND 91.41 B6J0733 10/07/2016 10/07/2016 21:27340EPA 5035A-H Surrogate: 1,2-Dichloroethane-d4 101 %10/07/2016 10/07/2016 21:27B6J073370 - 130 Surrogate: Toluene-d8 99.8 %10/07/2016 10/07/2016 21:27B6J073370 - 130 Surrogate: 4-Bromofluorobenzene 99.7 %10/07/2016 10/07/2016 21:27B6J073370 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 14 of 28 Project: NPU Stony Brook, Montville CET # : 6100133 QUALITY CONTROL SECTION Batch B6J0732 - EPA 8260C Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes Blank (B6J0732-BLK1)Prepared: 10/7/2016 Analyzed: 10/7/2016 Methyl-t-Butyl Ether (MTBE)2.5ND Benzene 2.5ND Toluene 2.5ND Chlorobenzene 2.5ND Ethylbenzene 2.5ND m+p Xylenes 2.5ND o-Xylene 2.5ND Styrene 2.5ND Isopropylbenzene 2.5ND Bromobenzene 2.5ND n-Propylbenzene 2.5ND 2-Chlorotoluene 2.5ND 4-Chlorotoluene 2.5ND 1,3,5-Trimethylbenzene 2.5ND tert-Butylbenzene 2.5ND 1,2,4-Trimethylbenzene 2.5ND sec-Butylbenzene 2.5ND 1,3-Dichlorobenzene 2.5ND 4-Isopropyltoluene 2.5ND 1,4-Dichlorobenzene 2.5ND 1,2-Dichlorobenzene 2.5ND n-Butylbenzene 2.5ND 1,2,4-Trichlorobenzene 2.5ND Hexachlorobutadiene 2.5ND Naphthalene 2.5ND 1,2,3-Trichlorobenzene 2.5ND 100 70 - 130Surrogate: 1,2-Dichloroethane-d4 98.8 70 - 130Surrogate: Toluene-d8 99.0 70 - 130Surrogate: 4-Bromofluorobenzene LCS (B6J0732-BS1)Prepared: 10/7/2016 Analyzed: 10/7/2016 Methyl-t-Butyl Ether (MTBE)2.5 97.7 70 - 13048.8 50.000 Benzene 2.5 98.0 70 - 13049.0 50.000 Toluene 2.5 95.8 70 - 13047.9 50.000 Chlorobenzene 2.5 100 70 - 13050.1 50.000 Ethylbenzene 2.5 101 70 - 13050.5 50.000 m+p Xylenes 2.5 101 70 - 130101 100.000 o-Xylene 2.5 101 70 - 13050.6 50.000 Styrene 2.5 104 70 - 13052.2 50.000 Isopropylbenzene 2.5 101 70 - 13050.4 50.000 Bromobenzene 2.5 102 70 - 13050.9 50.000 n-Propylbenzene 2.5 104 70 - 13052.0 50.000 2-Chlorotoluene 2.5 103 70 - 13051.5 50.000 4-Chlorotoluene 2.5 103 70 - 13051.6 50.000 1,3,5-Trimethylbenzene 2.5 103 70 - 13051.7 50.000 tert-Butylbenzene 2.5 102 70 - 13051.1 50.000 1,2,4-Trimethylbenzene 2.5 103 70 - 13051.7 50.000 sec-Butylbenzene 2.5 103 70 - 13051.7 50.000 1,3-Dichlorobenzene 2.5 102 70 - 13051.0 50.000 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 15 of 28 Project: NPU Stony Brook, Montville CET # : 6100133 Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes LCS (B6J0732-BS1) - Continued Prepared: 10/7/2016 Analyzed: 10/7/2016 4-Isopropyltoluene 2.5 105 70 - 13052.3 50.000 1,4-Dichlorobenzene 2.5 102 70 - 13051.0 50.000 1,2-Dichlorobenzene 2.5 103 70 - 13051.4 50.000 n-Butylbenzene 2.5 104 70 - 13051.8 50.000 1,2,4-Trichlorobenzene 2.5 101 70 - 13050.4 50.000 Hexachlorobutadiene 2.5 102 70 - 13051.1 50.000 Naphthalene 2.5 101 70 - 13050.4 50.000 1,2,3-Trichlorobenzene 2.5 100 70 - 13050.1 50.000 99.4 70 - 130Surrogate: 1,2-Dichloroethane-d4 99.7 70 - 130Surrogate: Toluene-d8 99.0 70 - 130Surrogate: 4-Bromofluorobenzene 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 16 of 28 Project: NPU Stony Brook, Montville CET # : 6100133 Batch B6J0733 - EPA 8260C Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes Blank (B6J0733-BLK1)Prepared: 10/7/2016 Analyzed: 10/7/2016 Methyl-t-Butyl Ether (MTBE)2.5ND Benzene 2.5ND Toluene 2.5ND Chlorobenzene 2.5ND Ethylbenzene 2.5ND m+p Xylenes 2.5ND o-Xylene 2.5ND Styrene 2.5ND Isopropylbenzene 2.5ND Bromobenzene 2.5ND n-Propylbenzene 2.5ND 2-Chlorotoluene 2.5ND 4-Chlorotoluene 2.5ND 1,3,5-Trimethylbenzene 2.5ND tert-Butylbenzene 2.5ND 1,2,4-Trimethylbenzene 2.5ND sec-Butylbenzene 2.5ND 1,3-Dichlorobenzene 2.5ND 4-Isopropyltoluene 2.5ND 1,4-Dichlorobenzene 2.5ND 1,2-Dichlorobenzene 2.5ND n-Butylbenzene 2.5ND 1,2,4-Trichlorobenzene 2.5ND Hexachlorobutadiene 2.5ND Naphthalene 2.5ND 1,2,3-Trichlorobenzene 2.5ND 100 70 - 130Surrogate: 1,2-Dichloroethane-d4 98.8 70 - 130Surrogate: Toluene-d8 99.0 70 - 130Surrogate: 4-Bromofluorobenzene LCS (B6J0733-BS1)Prepared: 10/7/2016 Analyzed: 10/7/2016 Methyl-t-Butyl Ether (MTBE)2.5 97.7 70 - 13048.8 50.000 Benzene 2.5 98.0 70 - 13049.0 50.000 Toluene 2.5 95.8 70 - 13047.9 50.000 Chlorobenzene 2.5 100 70 - 13050.1 50.000 Ethylbenzene 2.5 101 70 - 13050.5 50.000 m+p Xylenes 2.5 101 70 - 130101 100.000 o-Xylene 2.5 101 70 - 13050.6 50.000 Styrene 2.5 104 70 - 13052.2 50.000 Isopropylbenzene 2.5 101 70 - 13050.4 50.000 Bromobenzene 2.5 102 70 - 13050.9 50.000 n-Propylbenzene 2.5 104 70 - 13052.0 50.000 2-Chlorotoluene 2.5 103 70 - 13051.5 50.000 4-Chlorotoluene 2.5 103 70 - 13051.6 50.000 1,3,5-Trimethylbenzene 2.5 103 70 - 13051.7 50.000 tert-Butylbenzene 2.5 102 70 - 13051.1 50.000 1,2,4-Trimethylbenzene 2.5 103 70 - 13051.7 50.000 sec-Butylbenzene 2.5 103 70 - 13051.7 50.000 1,3-Dichlorobenzene 2.5 102 70 - 13051.0 50.000 4-Isopropyltoluene 2.5 105 70 - 13052.3 50.000 1,4-Dichlorobenzene 2.5 102 70 - 13051.0 50.000 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 17 of 28 Project: NPU Stony Brook, Montville CET # : 6100133 Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes LCS (B6J0733-BS1) - Continued Prepared: 10/7/2016 Analyzed: 10/7/2016 1,2-Dichlorobenzene 2.5 103 70 - 13051.4 50.000 n-Butylbenzene 2.5 104 70 - 13051.8 50.000 1,2,4-Trichlorobenzene 2.5 101 70 - 13050.4 50.000 Hexachlorobutadiene 2.5 102 70 - 13051.1 50.000 Naphthalene 2.5 101 70 - 13050.4 50.000 1,2,3-Trichlorobenzene 2.5 100 70 - 13050.1 50.000 99.4 70 - 130Surrogate: 1,2-Dichloroethane-d4 99.7 70 - 130Surrogate: Toluene-d8 99.0 70 - 130Surrogate: 4-Bromofluorobenzene 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 18 of 28 Project: NPU Stony Brook, Montville CET # : 6100133 Batch B6J0805 - CT-ETPH Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(mg/kg) (mg/kg)Notes Blank (B6J0805-BLK1)Prepared: 10/8/2016 Analyzed: 10/8/2016 ETPH 50ND 80.8 50 - 150Surrogate: Octacosane LCS (B6J0805-BS1)Prepared: 10/8/2016 Analyzed: 10/8/2016 ETPH 50 71.5 60 - 1201070 1,500.000 85.7 50 - 150Surrogate: Octacosane Duplicate (B6J0805-DUP1)Source: 6100133-01 Prepared: 10/8/2016 Analyzed: 10/8/2016 ETPH 66 ND 30ND 81.3 50 - 150Surrogate: Octacosane Matrix Spike (B6J0805-MS1)Source: 6100133-01 Prepared: 10/8/2016 Analyzed: 10/8/2016 ETPH 66 ND 84.8 50 - 1501680 1,976.466 79.9 50 - 150Surrogate: Octacosane Matrix Spike Dup (B6J0805-MSD1)Source: 6100133-01 Prepared: 10/8/2016 Analyzed: 10/8/2016 ETPH 66 ND 86.6 50 - 150 1.93 301710 1,972.517 78.0 50 - 150Surrogate: Octacosane 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 19 of 28 Project: NPU Stony Brook, Montville CET # : 6100133 Batch B6J1017 - EPA 8260C Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes Blank (B6J1017-BLK1)Prepared: 10/10/2016 Analyzed: 10/10/2016 Methyl-t-Butyl Ether (MTBE)2.5ND Benzene 2.5ND Toluene 2.5ND Chlorobenzene 2.5ND Ethylbenzene 2.5ND m+p Xylenes 2.5ND o-Xylene 2.5ND Styrene 2.5ND Isopropylbenzene 2.5ND Bromobenzene 2.5ND n-Propylbenzene 2.5ND 2-Chlorotoluene 2.5ND 4-Chlorotoluene 2.5ND 1,3,5-Trimethylbenzene 2.5ND tert-Butylbenzene 2.5ND 1,2,4-Trimethylbenzene 2.5ND sec-Butylbenzene 2.5ND 1,3-Dichlorobenzene 2.5ND 4-Isopropyltoluene 2.5ND 1,4-Dichlorobenzene 2.5ND 1,2-Dichlorobenzene 2.5ND n-Butylbenzene 2.5ND 1,2,4-Trichlorobenzene 2.5ND Hexachlorobutadiene 2.5ND Naphthalene 2.5ND 1,2,3-Trichlorobenzene 2.5ND 69.9 70 - 130Surrogate: 1,2-Dichloroethane-d4 L 108 70 - 130Surrogate: Toluene-d8 101 70 - 130Surrogate: 4-Bromofluorobenzene LCS (B6J1017-BS1)Prepared: 10/10/2016 Analyzed: 10/10/2016 Methyl-t-Butyl Ether (MTBE)2.5 78.8 70 - 13039.4 50.000 Benzene 2.5 79.8 70 - 13039.9 50.000 Toluene 2.5 108 70 - 13053.9 50.000 Chlorobenzene 2.5 89.0 70 - 13044.5 50.000 Ethylbenzene 2.5 85.6 70 - 13042.8 50.000 m+p Xylenes 2.5 88.3 70 - 13088.3 100.000 o-Xylene 2.5 85.1 70 - 13042.5 50.000 Styrene 2.5 90.5 70 - 13045.3 50.000 Isopropylbenzene 2.5 79.4 70 - 13039.7 50.000 Bromobenzene 2.5 89.0 70 - 13044.5 50.000 n-Propylbenzene 2.5 85.3 70 - 13042.7 50.000 2-Chlorotoluene 2.5 87.5 70 - 13043.8 50.000 4-Chlorotoluene 2.5 86.9 70 - 13043.4 50.000 1,3,5-Trimethylbenzene 2.5 86.9 70 - 13043.4 50.000 tert-Butylbenzene 2.5 83.3 70 - 13041.7 50.000 1,2,4-Trimethylbenzene 2.5 88.3 70 - 13044.1 50.000 sec-Butylbenzene 2.5 83.0 70 - 13041.5 50.000 1,3-Dichlorobenzene 2.5 88.4 70 - 13044.2 50.000 4-Isopropyltoluene 2.5 84.7 70 - 13042.3 50.000 1,4-Dichlorobenzene 2.5 88.5 70 - 13044.3 50.000 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 20 of 28 Project: NPU Stony Brook, Montville CET # : 6100133 Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes LCS (B6J1017-BS1) - Continued Prepared: 10/10/2016 Analyzed: 10/10/2016 1,2-Dichlorobenzene 2.5 90.2 70 - 13045.1 50.000 n-Butylbenzene 2.5 85.2 70 - 13042.6 50.000 1,2,4-Trichlorobenzene 2.5 89.7 70 - 13044.9 50.000 Hexachlorobutadiene 2.5 84.2 70 - 13042.1 50.000 Naphthalene 2.5 90.2 70 - 13045.1 50.000 1,2,3-Trichlorobenzene 2.5 91.2 70 - 13045.6 50.000 99.5 70 - 130Surrogate: 1,2-Dichloroethane-d4 77.5 70 - 130Surrogate: Toluene-d8 91.6 70 - 130Surrogate: 4-Bromofluorobenzene 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 21 of 28 Project: NPU Stony Brook, Montville CET # : 6100133 Batch B6J1018 - EPA 8260C Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes Blank (B6J1018-BLK1)Prepared: 10/10/2016 Analyzed: 10/10/2016 Methyl-t-Butyl Ether (MTBE)2.5ND Benzene 2.5ND Toluene 2.5ND Chlorobenzene 2.5ND Ethylbenzene 2.5ND m+p Xylenes 2.5ND o-Xylene 2.5ND Styrene 2.5ND Isopropylbenzene 2.5ND Bromobenzene 2.5ND n-Propylbenzene 2.5ND 2-Chlorotoluene 2.5ND 4-Chlorotoluene 2.5ND 1,3,5-Trimethylbenzene 2.5ND tert-Butylbenzene 2.5ND 1,2,4-Trimethylbenzene 2.5ND sec-Butylbenzene 2.5ND 1,3-Dichlorobenzene 2.5ND 4-Isopropyltoluene 2.5ND 1,4-Dichlorobenzene 2.5ND 1,2-Dichlorobenzene 2.5ND n-Butylbenzene 2.5ND 1,2,4-Trichlorobenzene 2.5ND Hexachlorobutadiene 2.5ND Naphthalene 2.5ND 1,2,3-Trichlorobenzene 2.5ND 101 70 - 130Surrogate: 1,2-Dichloroethane-d4 98.8 70 - 130Surrogate: Toluene-d8 98.2 70 - 130Surrogate: 4-Bromofluorobenzene LCS (B6J1018-BS1)Prepared: 10/10/2016 Analyzed: 10/10/2016 Methyl-t-Butyl Ether (MTBE)2.5 116 70 - 13057.8 50.000 Benzene 2.5 106 70 - 13052.8 50.000 Toluene 2.5 105 70 - 13052.3 50.000 Chlorobenzene 2.5 109 70 - 13054.5 50.000 Ethylbenzene 2.5 110 70 - 13054.8 50.000 m+p Xylenes 2.5 110 70 - 130110 100.000 o-Xylene 2.5 110 70 - 13054.8 50.000 Styrene 2.5 106 70 - 13052.9 50.000 Isopropylbenzene 2.5 110 70 - 13054.9 50.000 Bromobenzene 2.5 105 70 - 13052.5 50.000 n-Propylbenzene 2.5 112 70 - 13056.1 50.000 2-Chlorotoluene 2.5 110 70 - 13055.0 50.000 4-Chlorotoluene 2.5 110 70 - 13055.0 50.000 1,3,5-Trimethylbenzene 2.5 111 70 - 13055.6 50.000 tert-Butylbenzene 2.5 110 70 - 13054.8 50.000 1,2,4-Trimethylbenzene 2.5 106 70 - 13052.8 50.000 sec-Butylbenzene 2.5 106 70 - 13052.9 50.000 1,3-Dichlorobenzene 2.5 107 70 - 13053.3 50.000 4-Isopropyltoluene 2.5 108 70 - 13053.9 50.000 1,4-Dichlorobenzene 2.5 107 70 - 13053.7 50.000 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 22 of 28 Project: NPU Stony Brook, Montville CET # : 6100133 Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes LCS (B6J1018-BS1) - Continued Prepared: 10/10/2016 Analyzed: 10/10/2016 1,2-Dichlorobenzene 2.5 106 70 - 13052.8 50.000 n-Butylbenzene 2.5 109 70 - 13054.3 50.000 1,2,4-Trichlorobenzene 2.5 115 70 - 13057.6 50.000 Hexachlorobutadiene 2.5 94.4 70 - 13047.2 50.000 Naphthalene 2.5 110 70 - 13055.0 50.000 1,2,3-Trichlorobenzene 2.5 101 70 - 13050.4 50.000 97.8 70 - 130Surrogate: 1,2-Dichloroethane-d4 98.3 70 - 130Surrogate: Toluene-d8 97.1 70 - 130Surrogate: 4-Bromofluorobenzene 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 23 of 28 Project: NPU Stony Brook, Montville CET # : 6100133 Quality Control Definitions and Abbreviations 80 Lupes Drive Stratford, CT 06615 Internal Standard (IS)An Analyte added to each sample or sample extract. An internal standard is used to monitor retention time, calculate relative response, and quantify analytes of interest. Surrogate Recovery The % recovery for non-target organic compounds that are spiked into all samples. Used to determine method performance. Continuing Calibration An analytical standard analyzed with each set of samples to verify initial calibration of the system. Batch Samples that are analyzed together with the same method, sequence and lot of reagents within the same time period. ND Not detected RL Reporting Limit Dilution Multiplier added to detection levels (MDL) and/or sample results due to interferences and/or high concentration of target compounds. Duplicate Result from the duplicate analysis of a sample. Result Amount of analyte found in a sample. Spike Level Amount of analyte added to a sample Matrix Spike Result Amount of analyte found including amount that was spiked. Matrix Spike Dup Amount of analyte found in duplicate spikes including amount that was spike. Matrix Spike % Recovery % Recovery of spiked amount in sample. Matrix Spike Dup % Recovery % Recovery of spiked duplicate amount in sample. RPD Relative percent difference between Matrix Spike and Matrix Spike Duplicate. Blank Method Blank that has been taken through all steps of the analysis. LCS % Recovery Laboratory Control Sample percent recovery. The amount of analyte recovered from a fortified sample. Recovery Limits A range within which specified measurements results must fall to be compliant. CC Calibration Verification Flags: H-Recovery is above the control limits L-Recovery is below the control limits B-Compound detected in the Blank P-RPD of dual column results exceeds 40% #-Sample result too high for accurate spike recovery. Connecticut Laboratory Certification PH0116 New York Certification 11982 Massachussets Laboratory Certification M-CT903 Rhode Island Certification 199 Tel: (203) 377-9984 Fax: (203) 377-9952 email: cet1@cetlabs.com 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 24 of 28 Project: NPU Stony Brook, Montville CET # : 6100133 Report Comments: Questions related to this report should be directed to David Ditta, Timothy Fusco, or Robert Blake at 203-377-9984. Sincerely, David Ditta Laboratory Director Sample Result Flags: E- The result is estimated, above the calibration range. H- The surrogate recovery is above the control limits. L- The surrogate recovery is below the control limits. B- The compound was detected in the laboratory blank. P- The Relative Percent Difference (RPD) of dual column analyses exceeds 40%. D- The RPD between the sample and the sample duplicate is high. Sample homogeneity may be a problem. +- The Surrogate was diluted out. *C1- The Continuing Calibration did not meet method specifications and was biased low for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased low. *C2- The Continuing Calibration did not meet method specifications and was biased high for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased high. *F1- The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the low side. *F2- The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the high side. I- The Analyte exceeds %RSD limits for the Initial Calibration. This is a non-directional bias. All results met standard operating procedures unless indicated by a data qualifier next to a sample result, or a narration in the QC report. Complete Environmental Testing is only responsible for the certified testing and is not directly responsible for the integrity of the sample before laboratory receipt. ND is None Detected at the specified detection limit All analyses were performed in house unless a Reference Laboratory is listed. Samples will be disposed of 30 days after the report date. 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 25 of 28 Project: NPU Stony Brook, Montville CET # : 6100133 CertificationsAnalyte CERTIFICATIONS Certified Analyses included in this Report CT-ETPH in Soil CTETPH EPA 8260C in Soil CT,NYMethyl-t-Butyl Ether (MTBE) CT,NYBenzene CT,NYToluene CT,NYChlorobenzene CT,NYEthylbenzene CT,NYm+p Xylenes CT,NYo-Xylene CT,NYStyrene CT,NYIsopropylbenzene CT,NYBromobenzene CT,NYn-Propylbenzene CT,NY2-Chlorotoluene CT,NY4-Chlorotoluene CT,NY1,3,5-Trimethylbenzene CT,NYtert-Butylbenzene CT,NY1,2,4-Trimethylbenzene CT,NYsec-Butylbenzene CT,NY1,3-Dichlorobenzene CT,NY4-Isopropyltoluene CT,NY1,4-Dichlorobenzene CT,NY1,2-Dichlorobenzene CT,NYn-Butylbenzene CT,NY1,2,4-Trichlorobenzene CT,NYHexachlorobutadiene CT,NYNaphthalene CT1,2,3-Trichlorobenzene Complete Environmental Testing operates under the following certifications and accreditations: Code Description Number Expires Connecticut Public Health 09/30/2016CTPH0116 New York Certification (NELAC)04/01/2017NY11982 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 26 of 28 Page 27 of 28 Page 28 of 28 80 Lupes Drive Stratford, CT 06615 Tel: (203) 377-9984 Fax: (203) 377-9952 e-mail: cet1@cetlabs.com Client:Mr. Don Fortunato Soil & Environmental Service 61 Plants Dam Road East Lyme, CT 06333 Analytical Report CET# 6100134 Report Date:October 10, 2016 Project: NPU Stony Brook, Montville Rhode Island Certification: 199Massachusetts laboratory Certificate: M-CT903 Connecticut Laboratory Certificate: PH 0116 New York Certification: 11982 Page 1 of 12 Project: NPU Stony Brook, Montville CET # : 6100134 Sample ID Laboratory ID Matrix Collection Date/Time Receipt Date SAMPLE SUMMARY The sample(s) were received at 3.5 C. This report contains analytical data associated with following samples only. 5 0-8in 6100134-01 Soil 10/06/201610/05/2016 8 0-8in 6100134-02 Soil 10/06/201610/05/2016 13 0-8in 6100134-03 Soil 10/06/201610/05/2016 15 0-8in 6100134-04 Soil 10/06/201610/05/2016 22 SW 1-2.5ft 6100134-05 Soil 10/06/201610/05/2016 4 0-8in 6100134-06 Soil 10/06/201610/05/2016 Notes Date/Time AnalyzedPreparedBatchDilutionRLResultLaboratory ID Client Sample ID Units Analyst: MRH Matrix: Soil Analyte: Total Solids [EPA 160.3 modified] 79 10/07/2016 10/07/2016 14:406100134-01 %5 0-8in 1.0 1 B6J0710 63 10/07/2016 10/07/2016 14:406100134-02 %8 0-8in 1.0 1 B6J0710 63 10/07/2016 10/07/2016 14:406100134-03 %13 0-8in 1.0 1 B6J0710 75 10/07/2016 10/07/2016 14:406100134-04 %15 0-8in 1.0 1 B6J0710 91 10/07/2016 10/07/2016 14:406100134-05 %22 SW 1-2.5ft 1.0 1 B6J0710 73 10/07/2016 10/07/2016 14:406100134-06 %4 0-8in 1.0 1 B6J0710 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 2 of 12 Project: NPU Stony Brook, Montville CET # : 6100134 Client Sample ID 5 0-8in Lab ID: 6100134-01 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6J0805 10/08/2016 10/08/2016 17:2463EPA 3550C Surrogate: Octacosane 78.4 %10/08/2016 10/08/2016 17:24B6J080550 - 150 Client Sample ID 8 0-8in Lab ID: 6100134-02 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6J0805 10/08/2016 10/08/2016 17:4779EPA 3550C Surrogate: Octacosane 77.7 %10/08/2016 10/08/2016 17:47B6J080550 - 150 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 3 of 12 Project: NPU Stony Brook, Montville CET # : 6100134 Client Sample ID 13 0-8in Lab ID: 6100134-03 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6J0805 10/08/2016 10/08/2016 18:1080EPA 3550C Surrogate: Octacosane 67.1 %10/08/2016 10/08/2016 18:10B6J080550 - 150 Client Sample ID 15 0-8in Lab ID: 6100134-04 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6J0805 10/08/2016 10/08/2016 18:3266EPA 3550C Surrogate: Octacosane 77.5 %10/08/2016 10/08/2016 18:32B6J080550 - 150 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 4 of 12 Project: NPU Stony Brook, Montville CET # : 6100134 Client Sample ID 22 SW 1-2.5ft Lab ID: 6100134-05 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6J0805 10/08/2016 10/08/2016 18:5555EPA 3550C Surrogate: Octacosane 75.9 %10/08/2016 10/08/2016 18:55B6J080550 - 150 Client Sample ID 4 0-8in Lab ID: 6100134-06 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6J0805 10/08/2016 10/08/2016 19:1869EPA 3550C Surrogate: Octacosane 77.8 %10/08/2016 10/08/2016 19:18B6J080550 - 150 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 5 of 12 Project: NPU Stony Brook, Montville CET # : 6100134 QUALITY CONTROL SECTION Batch B6J0710 - EPA 160.3 modified Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(%) (%)Notes Duplicate (B6J0710-DUP1)Source: 6100134-05 Prepared: 10/7/2016 Analyzed: 10/7/2016 Total Solids 1.0 91 0.367 20091 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 6 of 12 Project: NPU Stony Brook, Montville CET # : 6100134 Batch B6J0805 - CT-ETPH Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(mg/kg) (mg/kg)Notes Blank (B6J0805-BLK1)Prepared: 10/8/2016 Analyzed: 10/8/2016 ETPH 50ND 80.8 50 - 150Surrogate: Octacosane LCS (B6J0805-BS1)Prepared: 10/8/2016 Analyzed: 10/8/2016 ETPH 50 71.5 60 - 1201070 1,500.000 85.7 50 - 150Surrogate: Octacosane 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 7 of 12 Project: NPU Stony Brook, Montville CET # : 6100134 Quality Control Definitions and Abbreviations 80 Lupes Drive Stratford, CT 06615 Internal Standard (IS)An Analyte added to each sample or sample extract. An internal standard is used to monitor retention time, calculate relative response, and quantify analytes of interest. Surrogate Recovery The % recovery for non-target organic compounds that are spiked into all samples. Used to determine method performance. Continuing Calibration An analytical standard analyzed with each set of samples to verify initial calibration of the system. Batch Samples that are analyzed together with the same method, sequence and lot of reagents within the same time period. ND Not detected RL Reporting Limit Dilution Multiplier added to detection levels (MDL) and/or sample results due to interferences and/or high concentration of target compounds. Duplicate Result from the duplicate analysis of a sample. Result Amount of analyte found in a sample. Spike Level Amount of analyte added to a sample Matrix Spike Result Amount of analyte found including amount that was spiked. Matrix Spike Dup Amount of analyte found in duplicate spikes including amount that was spike. Matrix Spike % Recovery % Recovery of spiked amount in sample. Matrix Spike Dup % Recovery % Recovery of spiked duplicate amount in sample. RPD Relative percent difference between Matrix Spike and Matrix Spike Duplicate. Blank Method Blank that has been taken through all steps of the analysis. LCS % Recovery Laboratory Control Sample percent recovery. The amount of analyte recovered from a fortified sample. Recovery Limits A range within which specified measurements results must fall to be compliant. CC Calibration Verification Flags: H-Recovery is above the control limits L-Recovery is below the control limits B-Compound detected in the Blank P-RPD of dual column results exceeds 40% #-Sample result too high for accurate spike recovery. Connecticut Laboratory Certification PH0116 New York Certification 11982 Massachussets Laboratory Certification M-CT903 Rhode Island Certification 199 Tel: (203) 377-9984 Fax: (203) 377-9952 email: cet1@cetlabs.com 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 8 of 12 Project: NPU Stony Brook, Montville CET # : 6100134 Report Comments: Questions related to this report should be directed to David Ditta, Timothy Fusco, or Robert Blake at 203-377-9984. Sincerely, David Ditta Laboratory Director Sample Result Flags: E- The result is estimated, above the calibration range. H- The surrogate recovery is above the control limits. L- The surrogate recovery is below the control limits. B- The compound was detected in the laboratory blank. P- The Relative Percent Difference (RPD) of dual column analyses exceeds 40%. D- The RPD between the sample and the sample duplicate is high. Sample homogeneity may be a problem. +- The Surrogate was diluted out. *C1- The Continuing Calibration did not meet method specifications and was biased low for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased low. *C2- The Continuing Calibration did not meet method specifications and was biased high for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased high. *F1- The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the low side. *F2- The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the high side. I- The Analyte exceeds %RSD limits for the Initial Calibration. This is a non-directional bias. All results met standard operating procedures unless indicated by a data qualifier next to a sample result, or a narration in the QC report. Complete Environmental Testing is only responsible for the certified testing and is not directly responsible for the integrity of the sample before laboratory receipt. ND is None Detected at the specified detection limit All analyses were performed in house unless a Reference Laboratory is listed. Samples will be disposed of 30 days after the report date. 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 9 of 12 Project: NPU Stony Brook, Montville CET # : 6100134 CertificationsAnalyte CERTIFICATIONS Certified Analyses included in this Report CT-ETPH in Soil CTETPH Complete Environmental Testing operates under the following certifications and accreditations: Code Description Number Expires Connecticut Public Health 09/30/2016CTPH0116 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 10 of 12 Page 11 of 12 Page 12 of 12 80 Lupes Drive Stratford, CT 06615 Tel: (203) 377-9984 Fax: (203) 377-9952 e-mail: cet1@cetlabs.com Client:Mr. Don Fortunato Soil & Environmental Service 61 Plants Dam Road East Lyme, CT 06333 Analytical Report CET# 6100135 Report Date:October 12, 2016 Project: NPU Stony Brook, Montville Rhode Island Certification: 199Massachusetts laboratory Certificate: M-CT903 Connecticut Laboratory Certificate: PH 0116 New York Certification: 11982 Page 1 of 18 Project: NPU Stony Brook, Montville CET # : 6100135 Sample ID Laboratory ID Matrix Collection Date/Time Receipt Date SAMPLE SUMMARY The sample(s) were received at 3.5 C. This report contains analytical data associated with following samples only. 1 0-8in 6100135-01 Soil 10/06/201610/05/2016 2 0-8in 6100135-02 Soil 10/06/201610/05/2016 9 0-8in 6100135-03 Soil 10/06/201610/05/2016 10 0-8in 6100135-04 Soil 10/06/201610/05/2016 12 0-8in 6100135-05 Soil 10/06/201610/05/2016 20-1 Bot 6ft 6100135-06 Soil 10/06/201610/05/2016 20-3 SW 3-6ft 6100135-07 Soil 10/06/201610/05/2016 21 Bot 2.5ft 6100135-08 Soil 10/06/201610/05/2016 Notes Date/Time AnalyzedPreparedBatchDilutionRLResultLaboratory ID Client Sample ID Units Analyst: MRH Matrix: Soil Analyte: Total Solids [EPA 160.3 modified] 87 10/07/2016 10/12/2016 10:406100135-01 %1 0-8in 1.0 1 B6J0717 80 10/07/2016 10/12/2016 10:406100135-02 %2 0-8in 1.0 1 B6J0717 50 10/07/2016 10/12/2016 10:406100135-03 %9 0-8in 1.0 1 B6J0717 72 10/07/2016 10/12/2016 10:406100135-04 %10 0-8in 1.0 1 B6J0717 66 10/07/2016 10/12/2016 10:406100135-05 %12 0-8in 1.0 1 B6J0717 64 10/07/2016 10/12/2016 10:406100135-06 %20-1 Bot 6ft 1.0 1 B6J0717 66 10/07/2016 10/12/2016 10:406100135-07 %20-3 SW 3-6ft 1.0 1 B6J0717 91 10/07/2016 10/12/2016 10:406100135-08 %21 Bot 2.5ft 1.0 1 B6J0717 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 2 of 18 Project: NPU Stony Brook, Montville CET # : 6100135 Client Sample ID 1 0-8in Lab ID: 6100135-01 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6J0810 10/08/2016 10/09/2016 14:2157EPA 3550C Surrogate: Octacosane 89.3 %10/08/2016 10/09/2016 14:21B6J081050 - 150 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 3 of 18 Project: NPU Stony Brook, Montville CET # : 6100135 Client Sample ID 2 0-8in Lab ID: 6100135-02 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6J0810 10/08/2016 10/09/2016 14:4462EPA 3550C Surrogate: Octacosane 87.8 %10/08/2016 10/09/2016 14:44B6J081050 - 150 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8270D Matrix: Soil Analyst: ALBSemivolatile Organics Naphthalene ND 0.996 B6J0729 10/07/2016 10/11/2016 16:14370EPA 3545A 2-Methyl Naphthalene ND 0.996 B6J0729 10/07/2016 10/11/2016 16:14370EPA 3545A Acenaphthylene ND 0.996 B6J0729 10/07/2016 10/11/2016 16:14370EPA 3545A Acenaphthene ND 0.996 B6J0729 10/07/2016 10/11/2016 16:14370EPA 3545A Fluorene ND 0.996 B6J0729 10/07/2016 10/11/2016 16:14370EPA 3545A Phenanthrene ND 0.996 B6J0729 10/07/2016 10/11/2016 16:14370EPA 3545A Anthracene ND 0.996 B6J0729 10/07/2016 10/11/2016 16:14370EPA 3545A Fluoranthene ND 0.996 B6J0729 10/07/2016 10/11/2016 16:14370EPA 3545A Pyrene ND 0.996 B6J0729 10/07/2016 10/11/2016 16:14370EPA 3545A Benzo[a]anthracene ND 0.996 B6J0729 10/07/2016 10/11/2016 16:14370EPA 3545A Chrysene ND 0.996 B6J0729 10/07/2016 10/11/2016 16:14370EPA 3545A Benzo[b]fluoranthene ND 0.996 B6J0729 10/07/2016 10/11/2016 16:14370EPA 3545A Benzo[k]fluoranthene ND 0.996 B6J0729 10/07/2016 10/11/2016 16:14370EPA 3545A Benzo[a]pyrene ND 0.996 B6J0729 10/07/2016 10/11/2016 16:14370EPA 3545A Indeno[1,2,3-cd]pyrene ND 0.996 B6J0729 10/07/2016 10/11/2016 16:14370EPA 3545A Dibenz[a,h]anthracene ND 0.996 B6J0729 10/07/2016 10/11/2016 16:14370EPA 3545A Benzo[g,h,i]perylene ND 0.996 B6J0729 10/07/2016 10/11/2016 16:14370EPA 3545A Surrogate: Nitrobenzene-d5 37.3 %10/07/2016 10/11/2016 16:14B6J072930 - 130 Surrogate: 2-Fluorobiphenyl 57.6 %10/07/2016 10/11/2016 16:14B6J072930 - 130 Surrogate: Terphenyl-d14 87.0 %10/07/2016 10/11/2016 16:14B6J072930 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 4 of 18 Project: NPU Stony Brook, Montville CET # : 6100135 Client Sample ID 9 0-8in Lab ID: 6100135-03 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6J0810 10/08/2016 10/09/2016 15:07100EPA 3550C Surrogate: Octacosane 66.0 %10/08/2016 10/09/2016 15:07B6J081050 - 150 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8270D Matrix: Soil Analyst: ALBSemivolatile Organics Naphthalene ND 1.009 B6J0729 10/07/2016 10/11/2016 16:50600EPA 3545A 2-Methyl Naphthalene ND 1.009 B6J0729 10/07/2016 10/11/2016 16:50600EPA 3545A Acenaphthylene ND 1.009 B6J0729 10/07/2016 10/11/2016 16:50600EPA 3545A Acenaphthene ND 1.009 B6J0729 10/07/2016 10/11/2016 16:50600EPA 3545A Fluorene ND 1.009 B6J0729 10/07/2016 10/11/2016 16:50600EPA 3545A Phenanthrene ND 1.009 B6J0729 10/07/2016 10/11/2016 16:50600EPA 3545A Anthracene ND 1.009 B6J0729 10/07/2016 10/11/2016 16:50600EPA 3545A Fluoranthene ND 1.009 B6J0729 10/07/2016 10/11/2016 16:50600EPA 3545A Pyrene ND 1.009 B6J0729 10/07/2016 10/11/2016 16:50600EPA 3545A Benzo[a]anthracene ND 1.009 B6J0729 10/07/2016 10/11/2016 16:50600EPA 3545A Chrysene ND 1.009 B6J0729 10/07/2016 10/11/2016 16:50600EPA 3545A Benzo[b]fluoranthene ND 1.009 B6J0729 10/07/2016 10/11/2016 16:50600EPA 3545A Benzo[k]fluoranthene ND 1.009 B6J0729 10/07/2016 10/11/2016 16:50600EPA 3545A Benzo[a]pyrene ND 1.009 B6J0729 10/07/2016 10/11/2016 16:50600EPA 3545A Indeno[1,2,3-cd]pyrene ND 1.009 B6J0729 10/07/2016 10/11/2016 16:50600EPA 3545A Dibenz[a,h]anthracene ND 1.009 B6J0729 10/07/2016 10/11/2016 16:50600EPA 3545A Benzo[g,h,i]perylene ND 1.009 B6J0729 10/07/2016 10/11/2016 16:50600EPA 3545A Surrogate: Nitrobenzene-d5 38.2 %10/07/2016 10/11/2016 16:50B6J072930 - 130 Surrogate: 2-Fluorobiphenyl 59.8 %10/07/2016 10/11/2016 16:50B6J072930 - 130 Surrogate: Terphenyl-d14 80.9 %10/07/2016 10/11/2016 16:50B6J072930 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 5 of 18 Project: NPU Stony Brook, Montville CET # : 6100135 Client Sample ID 10 0-8in Lab ID: 6100135-04 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6J1016 10/10/2016 10/10/2016 23:5165EPA 3550C Surrogate: Octacosane 77.9 %10/10/2016 10/10/2016 23:51B6J101650 - 150 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 6 of 18 Project: NPU Stony Brook, Montville CET # : 6100135 Client Sample ID 12 0-8in Lab ID: 6100135-05 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH 150 1 B6J1016 10/10/2016 10/11/2016 00:1371EPA 3550C 2 Surrogate: Octacosane 74.0 %10/10/2016 10/11/2016 00:13B6J101650 - 150 2 C9-C28 Fuel Oil Range Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8270D Matrix: Soil Analyst: ALBSemivolatile Organics Naphthalene ND 1.007 B6J0729 10/07/2016 10/11/2016 17:27460EPA 3545A 2-Methyl Naphthalene ND 1.007 B6J0729 10/07/2016 10/11/2016 17:27460EPA 3545A Acenaphthylene ND 1.007 B6J0729 10/07/2016 10/11/2016 17:27460EPA 3545A Acenaphthene ND 1.007 B6J0729 10/07/2016 10/11/2016 17:27460EPA 3545A Fluorene ND 1.007 B6J0729 10/07/2016 10/11/2016 17:27460EPA 3545A Phenanthrene ND 1.007 B6J0729 10/07/2016 10/11/2016 17:27460EPA 3545A Anthracene ND 1.007 B6J0729 10/07/2016 10/11/2016 17:27460EPA 3545A Fluoranthene ND 1.007 B6J0729 10/07/2016 10/11/2016 17:27460EPA 3545A Pyrene ND 1.007 B6J0729 10/07/2016 10/11/2016 17:27460EPA 3545A Benzo[a]anthracene ND 1.007 B6J0729 10/07/2016 10/11/2016 17:27460EPA 3545A Chrysene ND 1.007 B6J0729 10/07/2016 10/11/2016 17:27460EPA 3545A Benzo[b]fluoranthene ND 1.007 B6J0729 10/07/2016 10/11/2016 17:27460EPA 3545A Benzo[k]fluoranthene ND 1.007 B6J0729 10/07/2016 10/11/2016 17:27460EPA 3545A Benzo[a]pyrene ND 1.007 B6J0729 10/07/2016 10/11/2016 17:27460EPA 3545A Indeno[1,2,3-cd]pyrene ND 1.007 B6J0729 10/07/2016 10/11/2016 17:27460EPA 3545A Dibenz[a,h]anthracene ND 1.007 B6J0729 10/07/2016 10/11/2016 17:27460EPA 3545A Benzo[g,h,i]perylene ND 1.007 B6J0729 10/07/2016 10/11/2016 17:27460EPA 3545A Surrogate: Nitrobenzene-d5 39.9 %10/07/2016 10/11/2016 17:27B6J072930 - 130 Surrogate: 2-Fluorobiphenyl 57.8 %10/07/2016 10/11/2016 17:27B6J072930 - 130 Surrogate: Terphenyl-d14 95.8 %10/07/2016 10/11/2016 17:27B6J072930 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 7 of 18 Project: NPU Stony Brook, Montville CET # : 6100135 Client Sample ID 20-1 Bot 6ft Lab ID: 6100135-06 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH 4500 1 B6J1016 10/10/2016 10/11/2016 00:3677EPA 3550C 2 Surrogate: Octacosane 77.5 %10/10/2016 10/11/2016 00:36B6J101650 - 150 2 C9-C28 Fuel Oil Range 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 8 of 18 Project: NPU Stony Brook, Montville CET # : 6100135 Client Sample ID 20-3 SW 3-6ft Lab ID: 6100135-07 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH 3400 1 B6J1016 10/10/2016 10/11/2016 00:5876EPA 3550C 2 Surrogate: Octacosane 76.4 %10/10/2016 10/11/2016 00:58B6J101650 - 150 2 C9-C28 Fuel Oil Range Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8270D Matrix: Soil Analyst: ALBSemivolatile Organics Naphthalene ND 1 B6J0729 10/07/2016 10/11/2016 18:04450EPA 3545A 2-Methyl Naphthalene 3700 1 B6J0729 10/07/2016 10/11/2016 18:04450EPA 3545A Acenaphthylene ND 1 B6J0729 10/07/2016 10/11/2016 18:04450EPA 3545A Acenaphthene ND 1 B6J0729 10/07/2016 10/11/2016 18:04450EPA 3545A Fluorene ND 1 B6J0729 10/07/2016 10/11/2016 18:04450EPA 3545A Phenanthrene 720 1 B6J0729 10/07/2016 10/11/2016 18:04450EPA 3545A Anthracene ND 1 B6J0729 10/07/2016 10/11/2016 18:04450EPA 3545A Fluoranthene ND 1 B6J0729 10/07/2016 10/11/2016 18:04450EPA 3545A Pyrene ND 1 B6J0729 10/07/2016 10/11/2016 18:04450EPA 3545A Benzo[a]anthracene ND 1 B6J0729 10/07/2016 10/11/2016 18:04450EPA 3545A Chrysene ND 1 B6J0729 10/07/2016 10/11/2016 18:04450EPA 3545A Benzo[b]fluoranthene ND 1 B6J0729 10/07/2016 10/11/2016 18:04450EPA 3545A Benzo[k]fluoranthene ND 1 B6J0729 10/07/2016 10/11/2016 18:04450EPA 3545A Benzo[a]pyrene ND 1 B6J0729 10/07/2016 10/11/2016 18:04450EPA 3545A Indeno[1,2,3-cd]pyrene ND 1 B6J0729 10/07/2016 10/11/2016 18:04450EPA 3545A Dibenz[a,h]anthracene ND 1 B6J0729 10/07/2016 10/11/2016 18:04450EPA 3545A Benzo[g,h,i]perylene ND 1 B6J0729 10/07/2016 10/11/2016 18:04450EPA 3545A Surrogate: Nitrobenzene-d5 45.2 %10/07/2016 10/11/2016 18:04B6J072930 - 130 Surrogate: 2-Fluorobiphenyl 66.4 %10/07/2016 10/11/2016 18:04B6J072930 - 130 Surrogate: Terphenyl-d14 106 %10/07/2016 10/11/2016 18:04B6J072930 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 9 of 18 Project: NPU Stony Brook, Montville CET # : 6100135 Client Sample ID 21 Bot 2.5ft Lab ID: 6100135-08 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6J1016 10/10/2016 10/11/2016 01:2152EPA 3550C Surrogate: Octacosane 77.8 %10/10/2016 10/11/2016 01:21B6J101650 - 150 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 10 of 18 Project: NPU Stony Brook, Montville CET # : 6100135 QUALITY CONTROL SECTION Batch B6J0729 - EPA 8270D Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes Blank (B6J0729-BLK1)Prepared: 10/7/2016 Analyzed: 10/7/2016 Naphthalene 300ND 2-Methyl Naphthalene 300ND Acenaphthylene 300ND Acenaphthene 300ND Fluorene 300ND Phenanthrene 300ND Anthracene 300ND Fluoranthene 300ND Pyrene 300ND Benzo[a]anthracene 300ND Chrysene 300ND Benzo[b]fluoranthene 300ND Benzo[k]fluoranthene 300ND Benzo[a]pyrene 300ND Indeno[1,2,3-cd]pyrene 300ND Dibenz[a,h]anthracene 300ND Benzo[g,h,i]perylene 300ND 88.9 30 - 130Surrogate: Nitrobenzene-d5 97.4 30 - 130Surrogate: 2-Fluorobiphenyl 79.9 30 - 130Surrogate: Terphenyl-d14 LCS (B6J0729-BS1)Prepared: 10/7/2016 Analyzed: 10/7/2016 Naphthalene 300 54.1 40 - 1402160 4,000.000 2-Methyl Naphthalene 300 55.2 40 - 1402210 4,000.000 Acenaphthylene 300 54.2 40 - 1402170 4,000.000 Acenaphthene 300 58.1 40 - 1402320 4,000.000 Fluorene 300 57.7 40 - 1402310 4,000.000 Phenanthrene 300 61.1 40 - 1402440 4,000.000 Anthracene 300 61.0 40 - 1402440 4,000.000 Fluoranthene 300 58.7 40 - 1402350 4,000.000 Pyrene 300 59.2 40 - 1402370 4,000.000 Benzo[a]anthracene 300 65.0 40 - 1402600 4,000.000 Chrysene 300 63.7 40 - 1402550 4,000.000 Benzo[b]fluoranthene 300 57.3 40 - 1402290 4,000.000 Benzo[k]fluoranthene 300 66.3 40 - 1402650 4,000.000 Benzo[a]pyrene 300 66.3 40 - 1402650 4,000.000 Indeno[1,2,3-cd]pyrene 300 77.5 40 - 1403100 4,000.000 Dibenz[a,h]anthracene 300 81.2 40 - 1403250 4,000.000 Benzo[g,h,i]perylene 300 72.2 40 - 1402890 4,000.000 79.2 30 - 130Surrogate: Nitrobenzene-d5 85.4 30 - 130Surrogate: 2-Fluorobiphenyl 66.6 30 - 130Surrogate: Terphenyl-d14 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 11 of 18 Project: NPU Stony Brook, Montville CET # : 6100135 Batch B6J0810 - CT-ETPH Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(mg/kg) (mg/kg)Notes Blank (B6J0810-BLK1)Prepared: 10/8/2016 Analyzed: 10/9/2016 ETPH 50ND 90.6 50 - 150Surrogate: Octacosane LCS (B6J0810-BS1)Prepared: 10/8/2016 Analyzed: 10/9/2016 ETPH 50 74.1 60 - 1201110 1,500.000 89.0 50 - 150Surrogate: Octacosane 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 12 of 18 Project: NPU Stony Brook, Montville CET # : 6100135 Batch B6J1016 - CT-ETPH Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(mg/kg) (mg/kg)Notes Blank (B6J1016-BLK1)Prepared: 10/10/2016 Analyzed: 10/10/2016 ETPH 50ND 73.4 50 - 150Surrogate: Octacosane LCS (B6J1016-BS1)Prepared: 10/10/2016 Analyzed: 10/10/2016 ETPH 50 86.2 60 - 1201290 1,500.000 74.7 50 - 150Surrogate: Octacosane 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 13 of 18 Project: NPU Stony Brook, Montville CET # : 6100135 Quality Control Definitions and Abbreviations 80 Lupes Drive Stratford, CT 06615 Internal Standard (IS)An Analyte added to each sample or sample extract. An internal standard is used to monitor retention time, calculate relative response, and quantify analytes of interest. Surrogate Recovery The % recovery for non-target organic compounds that are spiked into all samples. Used to determine method performance. Continuing Calibration An analytical standard analyzed with each set of samples to verify initial calibration of the system. Batch Samples that are analyzed together with the same method, sequence and lot of reagents within the same time period. ND Not detected RL Reporting Limit Dilution Multiplier added to detection levels (MDL) and/or sample results due to interferences and/or high concentration of target compounds. Duplicate Result from the duplicate analysis of a sample. Result Amount of analyte found in a sample. Spike Level Amount of analyte added to a sample Matrix Spike Result Amount of analyte found including amount that was spiked. Matrix Spike Dup Amount of analyte found in duplicate spikes including amount that was spike. Matrix Spike % Recovery % Recovery of spiked amount in sample. Matrix Spike Dup % Recovery % Recovery of spiked duplicate amount in sample. RPD Relative percent difference between Matrix Spike and Matrix Spike Duplicate. Blank Method Blank that has been taken through all steps of the analysis. LCS % Recovery Laboratory Control Sample percent recovery. The amount of analyte recovered from a fortified sample. Recovery Limits A range within which specified measurements results must fall to be compliant. CC Calibration Verification Flags: H-Recovery is above the control limits L-Recovery is below the control limits B-Compound detected in the Blank P-RPD of dual column results exceeds 40% #-Sample result too high for accurate spike recovery. Connecticut Laboratory Certification PH0116 New York Certification 11982 Massachussets Laboratory Certification M-CT903 Rhode Island Certification 199 Tel: (203) 377-9984 Fax: (203) 377-9952 email: cet1@cetlabs.com 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 14 of 18 Project: NPU Stony Brook, Montville CET # : 6100135 Report Comments: Questions related to this report should be directed to David Ditta, Timothy Fusco, or Robert Blake at 203-377-9984. Sincerely, David Ditta Laboratory Director Sample Result Flags: E- The result is estimated, above the calibration range. H- The surrogate recovery is above the control limits. L- The surrogate recovery is below the control limits. B- The compound was detected in the laboratory blank. P- The Relative Percent Difference (RPD) of dual column analyses exceeds 40%. D- The RPD between the sample and the sample duplicate is high. Sample homogeneity may be a problem. +- The Surrogate was diluted out. *C1- The Continuing Calibration did not meet method specifications and was biased low for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased low. *C2- The Continuing Calibration did not meet method specifications and was biased high for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased high. *F1- The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the low side. *F2- The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the high side. I- The Analyte exceeds %RSD limits for the Initial Calibration. This is a non-directional bias. All results met standard operating procedures unless indicated by a data qualifier next to a sample result, or a narration in the QC report. Complete Environmental Testing is only responsible for the certified testing and is not directly responsible for the integrity of the sample before laboratory receipt. ND is None Detected at the specified detection limit All analyses were performed in house unless a Reference Laboratory is listed. Samples will be disposed of 30 days after the report date. 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 15 of 18 Project: NPU Stony Brook, Montville CET # : 6100135 CertificationsAnalyte CERTIFICATIONS Certified Analyses included in this Report CT-ETPH in Soil CTETPH EPA 8270D in Soil CT,NYNaphthalene CT,NY2-Methyl Naphthalene CT,NYAcenaphthylene CT,NYAcenaphthene CT,NYFluorene CT,NYPhenanthrene CT,NYAnthracene CT,NYFluoranthene CT,NYPyrene CT,NYBenzo[a]anthracene CT,NYChrysene CT,NYBenzo[b]fluoranthene CT,NYBenzo[k]fluoranthene CT,NYBenzo[a]pyrene CT,NYIndeno[1,2,3-cd]pyrene CT,NYDibenz[a,h]anthracene CT,NYBenzo[g,h,i]perylene Complete Environmental Testing operates under the following certifications and accreditations: Code Description Number Expires Connecticut Public Health 09/30/2016CTPH0116 New York Certification (NELAC)04/01/2017NY11982 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 16 of 18 Page 17 of 18 Page 18 of 18 80 Lupes Drive Stratford, CT 06615 Tel: (203) 377-9984 Fax: (203) 377-9952 e-mail: cet1@cetlabs.com Client:Mr. Don Fortunato Soil & Environmental Service 61 Plants Dam Road East Lyme, CT 06333 Analytical Report CET# 6100211 Report Date:October 12, 2016 Project: NPU Stony Brook, Montville Rhode Island Certification: 199Massachusetts laboratory Certificate: M-CT903 Connecticut Laboratory Certificate: PH 0116 New York Certification: 11982 Page 1 of 12 Project: NPU Stony Brook, Montville CET # : 6100211 Sample ID Laboratory ID Matrix Collection Date/Time Receipt Date SAMPLE SUMMARY The sample(s) were received at 2.5 C. This report contains analytical data associated with following samples only. 25 B 6100211-01 Soil 10/10/201610/07/2016 26 B 6100211-02 Soil 10/10/201610/07/2016 29 B 6100211-03 Soil 10/10/201610/07/2016 30 B 6100211-04 Soil 10/10/201610/07/2016 31 B 6100211-05 Soil 10/10/201610/07/2016 Notes Date/Time AnalyzedPreparedBatchDilutionRLResultLaboratory ID Client Sample ID Units Analyst: PB Matrix: Soil Analyte: Total Solids [EPA 160.3 modified] 78 10/11/2016 10/11/2016 14:466100211-01 %25 B 1.0 1 B6J1109 75 10/11/2016 10/11/2016 14:466100211-02 %26 B 1.0 1 B6J1109 91 10/11/2016 10/11/2016 14:466100211-03 %29 B 1.0 1 B6J1109 74 10/11/2016 10/11/2016 14:466100211-04 %30 B 1.0 1 B6J1109 93 10/11/2016 10/11/2016 14:466100211-05 %31 B 1.0 1 B6J1109 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 2 of 12 Project: NPU Stony Brook, Montville CET # : 6100211 Client Sample ID 25 B Lab ID: 6100211-01 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6J1127 10/11/2016 10/12/2016 01:2664EPA 3550C *F1 Surrogate: Octacosane 82.9 %10/11/2016 10/12/2016 01:26B6J112750 - 150 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8270D Matrix: Soil Analyst: ALBSemivolatile Organics Naphthalene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A 2-Methyl Naphthalene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Acenaphthylene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Acenaphthene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Fluorene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Phenanthrene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Anthracene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Fluoranthene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Pyrene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Benzo[a]anthracene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Chrysene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Benzo[b]fluoranthene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Benzo[k]fluoranthene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Benzo[a]pyrene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Indeno[1,2,3-cd]pyrene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Dibenz[a,h]anthracene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Benzo[g,h,i]perylene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Surrogate: Nitrobenzene-d5 38.9 %10/11/2016 10/12/2016 10:50B6J112130 - 130 Surrogate: 2-Fluorobiphenyl 36.1 %10/11/2016 10/12/2016 10:50B6J112130 - 130 Surrogate: Terphenyl-d14 52.3 %10/11/2016 10/12/2016 10:50B6J112130 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 3 of 12 Project: NPU Stony Brook, Montville CET # : 6100211 Client Sample ID 26 B Lab ID: 6100211-02 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH 5400 1 B6J1127 10/11/2016 10/12/2016 03:0166EPA 3550C 2*F1 Surrogate: Octacosane 84.5 %10/11/2016 10/12/2016 03:01B6J112750 - 150 2 C9-C28 Fuel Oil Range Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8270D Matrix: Soil Analyst: ALBSemivolatile Organics Naphthalene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A 2-Methyl Naphthalene 7300 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Acenaphthylene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Acenaphthene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Fluorene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Phenanthrene 1000 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Anthracene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Fluoranthene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Pyrene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Benzo[a]anthracene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Chrysene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Benzo[b]fluoranthene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Benzo[k]fluoranthene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Benzo[a]pyrene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Indeno[1,2,3-cd]pyrene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Dibenz[a,h]anthracene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Benzo[g,h,i]perylene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Surrogate: Nitrobenzene-d5 64.9 %10/11/2016 10/12/2016 15:07B6J112130 - 130 Surrogate: 2-Fluorobiphenyl 86.4 %10/11/2016 10/12/2016 15:07B6J112130 - 130 Surrogate: Terphenyl-d14 88.0 %10/11/2016 10/12/2016 15:07B6J112130 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 4 of 12 Project: NPU Stony Brook, Montville CET # : 6100211 Client Sample ID 29 B Lab ID: 6100211-03 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH 760 1 B6J1127 10/11/2016 10/12/2016 03:2555EPA 3550C 2*F1 Surrogate: Octacosane 88.4 %10/11/2016 10/12/2016 03:25B6J112750 - 150 2 C9-C28 Fuel Oil Range Client Sample ID 30 B Lab ID: 6100211-04 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH 3100 1 B6J1127 10/11/2016 10/12/2016 03:4867EPA 3550C 2*F1 Surrogate: Octacosane 80.3 %10/11/2016 10/12/2016 03:48B6J112750 - 150 2 C9-C28 Fuel Oil Range 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 5 of 12 Project: NPU Stony Brook, Montville CET # : 6100211 Client Sample ID 31 B Lab ID: 6100211-05 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH 18000 1 B6J1127 10/11/2016 10/12/2016 04:1254EPA 3550C 2*F1 Surrogate: Octacosane 85.5 %10/11/2016 10/12/2016 04:12B6J112750 - 150 2 C9-C28 Fuel Oil Range 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 6 of 12 Project: NPU Stony Brook, Montville CET # : 6100211 QUALITY CONTROL SECTION Batch B6J1121 - EPA 8270D Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes Blank (B6J1121-BLK1)Prepared: 10/11/2016 Analyzed: 10/12/2016 Naphthalene 300ND 2-Methyl Naphthalene 300ND Acenaphthylene 300ND Acenaphthene 300ND Fluorene 300ND Phenanthrene 300ND Anthracene 300ND Fluoranthene 300ND Pyrene 300ND Benzo[a]anthracene 300ND Chrysene 300ND Benzo[b]fluoranthene 300ND Benzo[k]fluoranthene 300ND Benzo[a]pyrene 300ND Indeno[1,2,3-cd]pyrene 300ND Dibenz[a,h]anthracene 300ND Benzo[g,h,i]perylene 300ND 60.2 30 - 130Surrogate: Nitrobenzene-d5 65.1 30 - 130Surrogate: 2-Fluorobiphenyl 82.7 30 - 130Surrogate: Terphenyl-d14 LCS (B6J1121-BS1)Prepared: 10/11/2016 Analyzed: 10/12/2016 Naphthalene 300 63.1 40 - 1402530 4,000.000 2-Methyl Naphthalene 300 63.4 40 - 1402540 4,000.000 Acenaphthylene 300 62.6 40 - 1402500 4,000.000 Acenaphthene 300 68.9 40 - 1402760 4,000.000 Fluorene 300 71.2 40 - 1402850 4,000.000 Phenanthrene 300 76.0 40 - 1403040 4,000.000 Anthracene 300 76.1 40 - 1403040 4,000.000 Fluoranthene 300 74.9 40 - 1403000 4,000.000 Pyrene 300 75.4 40 - 1403020 4,000.000 Benzo[a]anthracene 300 81.5 40 - 1403260 4,000.000 Chrysene 300 80.3 40 - 1403210 4,000.000 Benzo[b]fluoranthene 300 92.0 40 - 1403680 4,000.000 Benzo[k]fluoranthene 300 105 40 - 1404200 4,000.000 Benzo[a]pyrene 300 101 40 - 1404050 4,000.000 Indeno[1,2,3-cd]pyrene 300 105 40 - 1404220 4,000.000 Dibenz[a,h]anthracene 300 113 40 - 1404540 4,000.000 Benzo[g,h,i]perylene 300 93.8 40 - 1403750 4,000.000 62.7 30 - 130Surrogate: Nitrobenzene-d5 67.6 30 - 130Surrogate: 2-Fluorobiphenyl 81.3 30 - 130Surrogate: Terphenyl-d14 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 7 of 12 Project: NPU Stony Brook, Montville CET # : 6100211 Batch B6J1127 - CT-ETPH Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(mg/kg) (mg/kg)Notes Blank (B6J1127-BLK1)Prepared: 10/11/2016 Analyzed: 10/12/2016 ETPH 50ND 84.0 50 - 150Surrogate: Octacosane LCS (B6J1127-BS1)Prepared: 10/11/2016 Analyzed: 10/12/2016 ETPH 50 60 - 1201150 L 86.1 50 - 150Surrogate: Octacosane Duplicate (B6J1127-DUP1)Source: 6100211-01 Prepared: 10/11/2016 Analyzed: 10/12/2016 ETPH 64 ND 30ND 86.5 50 - 150Surrogate: Octacosane Matrix Spike (B6J1127-MS1)Source: 6100211-01 Prepared: 10/11/2016 Analyzed: 10/12/2016 ETPH 64 ND 50 - 1501490 L 84.4 50 - 150Surrogate: Octacosane Matrix Spike Dup (B6J1127-MSD1)Source: 6100211-01 Prepared: 10/11/2016 Analyzed: 10/12/2016 ETPH 64 ND 50 - 150 14.8 301730 L 89.6 50 - 150Surrogate: Octacosane 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 8 of 12 Project: NPU Stony Brook, Montville CET # : 6100211 Quality Control Definitions and Abbreviations 80 Lupes Drive Stratford, CT 06615 Internal Standard (IS)An Analyte added to each sample or sample extract. An internal standard is used to monitor retention time, calculate relative response, and quantify analytes of interest. Surrogate Recovery The % recovery for non-target organic compounds that are spiked into all samples. Used to determine method performance. Continuing Calibration An analytical standard analyzed with each set of samples to verify initial calibration of the system. Batch Samples that are analyzed together with the same method, sequence and lot of reagents within the same time period. ND Not detected RL Reporting Limit Dilution Multiplier added to detection levels (MDL) and/or sample results due to interferences and/or high concentration of target compounds. Duplicate Result from the duplicate analysis of a sample. Result Amount of analyte found in a sample. Spike Level Amount of analyte added to a sample Matrix Spike Result Amount of analyte found including amount that was spiked. Matrix Spike Dup Amount of analyte found in duplicate spikes including amount that was spike. Matrix Spike % Recovery % Recovery of spiked amount in sample. Matrix Spike Dup % Recovery % Recovery of spiked duplicate amount in sample. RPD Relative percent difference between Matrix Spike and Matrix Spike Duplicate. Blank Method Blank that has been taken through all steps of the analysis. LCS % Recovery Laboratory Control Sample percent recovery. The amount of analyte recovered from a fortified sample. Recovery Limits A range within which specified measurements results must fall to be compliant. CC Calibration Verification Flags: H-Recovery is above the control limits L-Recovery is below the control limits B-Compound detected in the Blank P-RPD of dual column results exceeds 40% #-Sample result too high for accurate spike recovery. Connecticut Laboratory Certification PH0116 New York Certification 11982 Massachussets Laboratory Certification M-CT903 Rhode Island Certification 199 Tel: (203) 377-9984 Fax: (203) 377-9952 email: cet1@cetlabs.com 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 9 of 12 Project: NPU Stony Brook, Montville CET # : 6100211 Report Comments: Questions related to this report should be directed to David Ditta, Timothy Fusco, or Robert Blake at 203-377-9984. Sincerely, David Ditta Laboratory Director Sample Result Flags: E- The result is estimated, above the calibration range. H- The surrogate recovery is above the control limits. L- The surrogate recovery is below the control limits. B- The compound was detected in the laboratory blank. P- The Relative Percent Difference (RPD) of dual column analyses exceeds 40%. D- The RPD between the sample and the sample duplicate is high. Sample homogeneity may be a problem. +- The Surrogate was diluted out. *C1- The Continuing Calibration did not meet method specifications and was biased low for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased low. *C2- The Continuing Calibration did not meet method specifications and was biased high for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased high. *F1- The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the low side. *F2- The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the high side. I- The Analyte exceeds %RSD limits for the Initial Calibration. This is a non-directional bias. All results met standard operating procedures unless indicated by a data qualifier next to a sample result, or a narration in the QC report. Complete Environmental Testing is only responsible for the certified testing and is not directly responsible for the integrity of the sample before laboratory receipt. ND is None Detected at the specified detection limit All analyses were performed in house unless a Reference Laboratory is listed. Samples will be disposed of 30 days after the report date. 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 10 of 12 Project: NPU Stony Brook, Montville CET # : 6100211 CertificationsAnalyte CERTIFICATIONS Certified Analyses included in this Report CT-ETPH in Soil CTETPH EPA 8270D in Soil CT,NYNaphthalene CT,NY2-Methyl Naphthalene CT,NYAcenaphthylene CT,NYAcenaphthene CT,NYFluorene CT,NYPhenanthrene CT,NYAnthracene CT,NYFluoranthene CT,NYPyrene CT,NYBenzo[a]anthracene CT,NYChrysene CT,NYBenzo[b]fluoranthene CT,NYBenzo[k]fluoranthene CT,NYBenzo[a]pyrene CT,NYIndeno[1,2,3-cd]pyrene CT,NYDibenz[a,h]anthracene CT,NYBenzo[g,h,i]perylene Complete Environmental Testing operates under the following certifications and accreditations: Code Description Number Expires Connecticut Public Health 09/30/2016CTPH0116 New York Certification (NELAC)04/01/2017NY11982 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 11 of 12 Page 12 of 12 80 Lupes Drive Stratford, CT 06615 Tel: (203) 377-9984 Fax: (203) 377-9952 e-mail: cet1@cetlabs.com Client:Mr. Don Fortunato Soil & Environmental Service 61 Plants Dam Road East Lyme, CT 06333 Analytical Report CET# 6100215 Report Date:October 14, 2016 Project: NPU Stony Brook, Montville Rhode Island Certification: 199Massachusetts laboratory Certificate: M-CT903 Connecticut Laboratory Certificate: PH 0116 New York Certification: 11982 Page 1 of 12 Project: NPU Stony Brook, Montville CET # : 6100215 Sample ID Laboratory ID Matrix Collection Date/Time Receipt Date SAMPLE SUMMARY The sample(s) were received at 2.5 C. This report contains analytical data associated with following samples only. SW 1 0-6in 6100215-01 Water 10/10/201613:0010/07/2016 GW 1 6100215-02 Water 10/10/201611:3010/07/2016 Blank 6100215-03 Water 10/10/201616:0010/07/2016 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 2 of 12 Project: NPU Stony Brook, Montville CET # : 6100215 Notes Date/Time AnalyzedPreparedBatchDilutionRLResultLaboratory ID Client Sample ID Units Analyst: KP Matrix: Water pH analyzed in lab Analyte: pH [SM 4500-H B] 5.83 10/11/2016 10/11/2016 16:076100215-03 pH UnitsBlankNA 1 B6J1123 Notes Date/Time AnalyzedPreparedBatchDilutionRLResultLaboratory ID Client Sample ID Units Analyst: SS Matrix: WaterPrep: EPA 3005A Analyte: Total Lead [EPA 200.7] ND 10/14/2016 10/14/2016 16:076100215-03 mg/LBlank0.013 1 B6J1402 Notes Date/Time AnalyzedPreparedBatchDilutionRLResultLaboratory ID Client Sample ID Units Analyst: SS Matrix: WaterPrep: EPA 3005A Analyte: Total Copper [EPA 200.7] 4.8 10/14/2016 10/14/2016 16:076100215-03 mg/LBlank0.040 1 B6J1402 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 3 of 12 Project: NPU Stony Brook, Montville CET # : 6100215 Client Sample ID SW 1 0-6in Lab ID: 6100215-01 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/L) Result (mg/L)Analyte Prep Method Method: CT-ETPH Matrix: Water Analyst: MHConn. Extractable TPH ETPH 10 1 B6J1111 10/11/2016 10/11/2016 22:160.10 EPA 3510C 2 Surrogate: Octacosane 78.8 %10/11/2016 10/11/2016 22:16B6J111150 - 150 2 C9-C28 Fuel Oil Range Client Sample ID GW 1 Lab ID: 6100215-02 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/L) Result (mg/L)Analyte Prep Method Method: CT-ETPH Matrix: Water Analyst: MHConn. Extractable TPH ETPH 33 1 B6J1111 10/11/2016 10/11/2016 22:400.10 EPA 3510C 2 Surrogate: Octacosane 78.0 %10/11/2016 10/11/2016 22:40B6J111150 - 150 2 C9-C28 Fuel Oil Range 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 4 of 12 Project: NPU Stony Brook, Montville CET # : 6100215 Client Sample ID Blank Lab ID: 6100215-03 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/L) Result (mg/L)Analyte Prep Method Method: CT-ETPH Matrix: Water Analyst: MHConn. Extractable TPH ETPH ND 1 B6J1111 10/11/2016 10/11/2016 23:030.10 EPA 3510C Surrogate: Octacosane 85.3 %10/11/2016 10/11/2016 23:03B6J111150 - 150 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 5 of 12 Project: NPU Stony Brook, Montville CET # : 6100215 QUALITY CONTROL SECTION Batch B6J1111 - CT-ETPH Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(mg/L) (mg/L)Notes Blank (B6J1111-BLK1)Prepared: 10/11/2016 Analyzed: 10/11/2016 ETPH 0.10ND 57.9 50 - 150Surrogate: Octacosane LCS (B6J1111-BS1)Prepared: 10/11/2016 Analyzed: 10/11/2016 ETPH 0.10 67.6 60 - 1203.38 5.000 83.7 50 - 150Surrogate: Octacosane 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 6 of 12 Project: NPU Stony Brook, Montville CET # : 6100215 Batch B6J1123 - SM 4500-H B Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(pH Units) (pH Units)Notes Blank (B6J1123-BLK1)Prepared: 10/11/2016 Analyzed: 10/11/2016 pH 5.91 Duplicate (B6J1123-DUP1)Source: 6100215-03 Prepared: 10/11/2016 Analyzed: 10/11/2016 pH 5.83 0.513 55.86 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 7 of 12 Project: NPU Stony Brook, Montville CET # : 6100215 Batch B6J1402 - EPA 200.7 Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(mg/L) (mg/L)Notes Blank (B6J1402-BLK1)Prepared: 10/14/2016 Analyzed: 10/14/2016 Lead 0.0050ND Copper 0.040ND LCS (B6J1402-BS1)Prepared: 10/14/2016 Analyzed: 10/14/2016 Lead 0.0050 88.4 85 - 1150.177 0.200 Copper 0.040 90.3 85 - 1150.181 0.200 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 8 of 12 Project: NPU Stony Brook, Montville CET # : 6100215 Quality Control Definitions and Abbreviations 80 Lupes Drive Stratford, CT 06615 Internal Standard (IS)An Analyte added to each sample or sample extract. An internal standard is used to monitor retention time, calculate relative response, and quantify analytes of interest. Surrogate Recovery The % recovery for non-target organic compounds that are spiked into all samples. Used to determine method performance. Continuing Calibration An analytical standard analyzed with each set of samples to verify initial calibration of the system. Batch Samples that are analyzed together with the same method, sequence and lot of reagents within the same time period. ND Not detected RL Reporting Limit Dilution Multiplier added to detection levels (MDL) and/or sample results due to interferences and/or high concentration of target compounds. Duplicate Result from the duplicate analysis of a sample. Result Amount of analyte found in a sample. Spike Level Amount of analyte added to a sample Matrix Spike Result Amount of analyte found including amount that was spiked. Matrix Spike Dup Amount of analyte found in duplicate spikes including amount that was spike. Matrix Spike % Recovery % Recovery of spiked amount in sample. Matrix Spike Dup % Recovery % Recovery of spiked duplicate amount in sample. RPD Relative percent difference between Matrix Spike and Matrix Spike Duplicate. Blank Method Blank that has been taken through all steps of the analysis. LCS % Recovery Laboratory Control Sample percent recovery. The amount of analyte recovered from a fortified sample. Recovery Limits A range within which specified measurements results must fall to be compliant. CC Calibration Verification Flags: H-Recovery is above the control limits L-Recovery is below the control limits B-Compound detected in the Blank P-RPD of dual column results exceeds 40% #-Sample result too high for accurate spike recovery. Connecticut Laboratory Certification PH0116 New York Certification 11982 Massachussets Laboratory Certification M-CT903 Rhode Island Certification 199 Tel: (203) 377-9984 Fax: (203) 377-9952 email: cet1@cetlabs.com 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 9 of 12 Project: NPU Stony Brook, Montville CET # : 6100215 Report Comments: Questions related to this report should be directed to David Ditta, Timothy Fusco, or Robert Blake at 203-377-9984. Sincerely, David Ditta Laboratory Director Sample Result Flags: E- The result is estimated, above the calibration range. H- The surrogate recovery is above the control limits. L- The surrogate recovery is below the control limits. B- The compound was detected in the laboratory blank. P- The Relative Percent Difference (RPD) of dual column analyses exceeds 40%. D- The RPD between the sample and the sample duplicate is high. Sample homogeneity may be a problem. +- The Surrogate was diluted out. *C1- The Continuing Calibration did not meet method specifications and was biased low for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased low. *C2- The Continuing Calibration did not meet method specifications and was biased high for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased high. *F1- The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the low side. *F2- The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the high side. I- The Analyte exceeds %RSD limits for the Initial Calibration. This is a non-directional bias. All results met standard operating procedures unless indicated by a data qualifier next to a sample result, or a narration in the QC report. Complete Environmental Testing is only responsible for the certified testing and is not directly responsible for the integrity of the sample before laboratory receipt. ND is None Detected at the specified detection limit All analyses were performed in house unless a Reference Laboratory is listed. Samples will be disposed of 30 days after the report date. 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 10 of 12 Project: NPU Stony Brook, Montville CET # : 6100215 CertificationsAnalyte CERTIFICATIONS Certified Analyses included in this Report CT-ETPH in Water CTETPH EPA 200.7 in Water CT,MA,NY,RILead CT,MA,NY,RICopper SM 4500-H B in Water CT,MA,RIpH Complete Environmental Testing operates under the following certifications and accreditations: Code Description Number Expires Connecticut Public Health 09/30/2016CTPH0116 Massachusetts Laboratory Certification 06/30/2016MAM-CT903 New York Certification (NELAC)04/01/2017NY11982 Rhode Island Certification 09/30/2016RILAO 00227 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 11 of 12 Page 12 of 12 80 Lupes Drive Stratford, CT 06615 Tel: (203) 377-9984 Fax: (203) 377-9952 e-mail: cet1@cetlabs.com Client:Mr. Don Fortunato Soil & Environmental Service 61 Plants Dam Road East Lyme, CT 06333 Analytical Report CET# 6100216 Report Date:October 17, 2016 Project: NPU Stony Brook, Montville Rhode Island Certification: 199Massachusetts laboratory Certificate: M-CT903 Connecticut Laboratory Certificate: PH 0116 New York Certification: 11982 Page 1 of 10 Project: NPU Stony Brook, Montville CET # : 6100216 Sample ID Laboratory ID Matrix Collection Date/Time Receipt Date SAMPLE SUMMARY The sample(s) were received at 2.5 C. This report contains analytical data associated with following samples only. 24 B 6100216-01 Soil 10/10/201610/07/2016 27 B 6100216-02 Soil 10/10/201610/07/2016 28 B 6100216-03 Soil 10/10/201610/07/2016 32 SW 6100216-04 Soil 10/10/201610/07/2016 Notes Date/Time AnalyzedPreparedBatchDilutionRLResultLaboratory ID Client Sample ID Units Analyst: PB Matrix: Soil Analyte: Total Solids [EPA 160.3 modified] 81 10/11/2016 10/11/2016 14:466100216-01 %24 B 1.0 1 B6J1109 69 10/11/2016 10/11/2016 14:466100216-02 %27 B 1.0 1 B6J1109 81 10/11/2016 10/11/2016 14:466100216-03 %28 B 1.0 1 B6J1109 89 10/11/2016 10/11/2016 14:466100216-04 %32 SW 1.0 1 B6J1109 Client Sample ID 24 B Lab ID: 6100216-01 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6J1342 10/13/2016 10/13/2016 23:5862EPA 3550C *F1 Surrogate: Octacosane 88.1 %10/13/2016 10/13/2016 23:58B6J134250 - 150 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 2 of 10 Project: NPU Stony Brook, Montville CET # : 6100216 Client Sample ID 27 B Lab ID: 6100216-02 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6J1342 10/13/2016 10/14/2016 00:2272EPA 3550C *F1 Surrogate: Octacosane 83.5 %10/13/2016 10/14/2016 00:22B6J134250 - 150 Client Sample ID 28 B Lab ID: 6100216-03 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6J1342 10/13/2016 10/14/2016 00:4661EPA 3550C *F1 Surrogate: Octacosane 92.8 %10/13/2016 10/14/2016 00:46B6J134250 - 150 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 3 of 10 Project: NPU Stony Brook, Montville CET # : 6100216 Client Sample ID 32 SW Lab ID: 6100216-04 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH 1500 1 B6J1342 10/13/2016 10/14/2016 01:0956EPA 3550C *F1 Surrogate: Octacosane 86.5 %10/13/2016 10/14/2016 01:09B6J134250 - 150 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8270D Matrix: Soil Analyst: ALBSemivolatile Organics Naphthalene ND 1.019 B6J1502 10/15/2016 10/17/2016 10:24350EPA 3545A 2-Methyl Naphthalene ND 1.019 B6J1502 10/15/2016 10/17/2016 10:24350EPA 3545A Acenaphthylene ND 1.019 B6J1502 10/15/2016 10/17/2016 10:24350EPA 3545A Acenaphthene ND 1.019 B6J1502 10/15/2016 10/17/2016 10:24350EPA 3545A Fluorene ND 1.019 B6J1502 10/15/2016 10/17/2016 10:24350EPA 3545A Phenanthrene ND 1.019 B6J1502 10/15/2016 10/17/2016 10:24350EPA 3545A Anthracene ND 1.019 B6J1502 10/15/2016 10/17/2016 10:24350EPA 3545A Fluoranthene ND 1.019 B6J1502 10/15/2016 10/17/2016 10:24350EPA 3545A Pyrene ND 1.019 B6J1502 10/15/2016 10/17/2016 10:24350EPA 3545A Benzo[a]anthracene ND 1.019 B6J1502 10/15/2016 10/17/2016 10:24350EPA 3545A Chrysene ND 1.019 B6J1502 10/15/2016 10/17/2016 10:24350EPA 3545A Benzo[b]fluoranthene ND 1.019 B6J1502 10/15/2016 10/17/2016 10:24350EPA 3545A Benzo[k]fluoranthene ND 1.019 B6J1502 10/15/2016 10/17/2016 10:24350EPA 3545A Benzo[a]pyrene ND 1.019 B6J1502 10/15/2016 10/17/2016 10:24350EPA 3545A Indeno[1,2,3-cd]pyrene ND 1.019 B6J1502 10/15/2016 10/17/2016 10:24350EPA 3545A Dibenz[a,h]anthracene ND 1.019 B6J1502 10/15/2016 10/17/2016 10:24350EPA 3545A Benzo[g,h,i]perylene ND 1.019 B6J1502 10/15/2016 10/17/2016 10:24350EPA 3545A Surrogate: Nitrobenzene-d5 53.0 %10/15/2016 10/17/2016 10:24B6J150230 - 130 Surrogate: 2-Fluorobiphenyl 54.4 %10/15/2016 10/17/2016 10:24B6J150230 - 130 Surrogate: Terphenyl-d14 79.1 %10/15/2016 10/17/2016 10:24B6J150230 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 4 of 10 Project: NPU Stony Brook, Montville CET # : 6100216 QUALITY CONTROL SECTION Batch B6J1342 - CT-ETPH Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(mg/kg) (mg/kg)Notes Blank (B6J1342-BLK1)Prepared: 10/13/2016 Analyzed: 10/13/2016 ETPH 50ND 108 50 - 150Surrogate: Octacosane LCS (B6J1342-BS1)Prepared: 10/13/2016 Analyzed: 10/13/2016 ETPH 50 60 - 1201260 L 105 50 - 150Surrogate: Octacosane 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 5 of 10 Project: NPU Stony Brook, Montville CET # : 6100216 Batch B6J1502 - EPA 8270D Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes Blank (B6J1502-BLK1)Prepared: 10/15/2016 Analyzed: 10/17/2016 Naphthalene 300ND 2-Methyl Naphthalene 300ND Acenaphthylene 300ND Acenaphthene 300ND Fluorene 300ND Phenanthrene 300ND Anthracene 300ND Fluoranthene 300ND Pyrene 300ND Benzo[a]anthracene 300ND Chrysene 300ND Benzo[b]fluoranthene 300ND Benzo[k]fluoranthene 300ND Benzo[a]pyrene 300ND Indeno[1,2,3-cd]pyrene 300ND Dibenz[a,h]anthracene 300ND Benzo[g,h,i]perylene 300ND 62.9 30 - 130Surrogate: Nitrobenzene-d5 68.6 30 - 130Surrogate: 2-Fluorobiphenyl 86.8 30 - 130Surrogate: Terphenyl-d14 LCS (B6J1502-BS1)Prepared: 10/15/2016 Analyzed: 10/17/2016 Naphthalene 300 59.9 40 - 1402400 4,000.000 2-Methyl Naphthalene 300 63.4 40 - 1402540 4,000.000 Acenaphthylene 300 60.4 40 - 1402420 4,000.000 Acenaphthene 300 67.4 40 - 1402700 4,000.000 Fluorene 300 55.2 40 - 1402210 4,000.000 Phenanthrene 300 75.0 40 - 1403000 4,000.000 Anthracene 300 70.7 40 - 1402830 4,000.000 Fluoranthene 300 85.3 40 - 1403410 4,000.000 Pyrene 300 85.7 40 - 1403430 4,000.000 Benzo[a]anthracene 300 82.3 40 - 1403290 4,000.000 Chrysene 300 76.9 40 - 1403080 4,000.000 Benzo[b]fluoranthene 300 90.3 40 - 1403610 4,000.000 Benzo[k]fluoranthene 300 97.5 40 - 1403900 4,000.000 Benzo[a]pyrene 300 91.4 40 - 1403660 4,000.000 Indeno[1,2,3-cd]pyrene 300 130 40 - 1405180 4,000.000 Dibenz[a,h]anthracene 300 134 40 - 1405360 4,000.000 Benzo[g,h,i]perylene 300 125 40 - 1405010 4,000.000 58.2 30 - 130Surrogate: Nitrobenzene-d5 62.5 30 - 130Surrogate: 2-Fluorobiphenyl 72.5 30 - 130Surrogate: Terphenyl-d14 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 6 of 10 Project: NPU Stony Brook, Montville CET # : 6100216 Quality Control Definitions and Abbreviations 80 Lupes Drive Stratford, CT 06615 Internal Standard (IS)An Analyte added to each sample or sample extract. An internal standard is used to monitor retention time, calculate relative response, and quantify analytes of interest. Surrogate Recovery The % recovery for non-target organic compounds that are spiked into all samples. Used to determine method performance. Continuing Calibration An analytical standard analyzed with each set of samples to verify initial calibration of the system. Batch Samples that are analyzed together with the same method, sequence and lot of reagents within the same time period. ND Not detected RL Reporting Limit Dilution Multiplier added to detection levels (MDL) and/or sample results due to interferences and/or high concentration of target compounds. Duplicate Result from the duplicate analysis of a sample. Result Amount of analyte found in a sample. Spike Level Amount of analyte added to a sample Matrix Spike Result Amount of analyte found including amount that was spiked. Matrix Spike Dup Amount of analyte found in duplicate spikes including amount that was spike. Matrix Spike % Recovery % Recovery of spiked amount in sample. Matrix Spike Dup % Recovery % Recovery of spiked duplicate amount in sample. RPD Relative percent difference between Matrix Spike and Matrix Spike Duplicate. Blank Method Blank that has been taken through all steps of the analysis. LCS % Recovery Laboratory Control Sample percent recovery. The amount of analyte recovered from a fortified sample. Recovery Limits A range within which specified measurements results must fall to be compliant. CC Calibration Verification Flags: H-Recovery is above the control limits L-Recovery is below the control limits B-Compound detected in the Blank P-RPD of dual column results exceeds 40% #-Sample result too high for accurate spike recovery. Connecticut Laboratory Certification PH0116 New York Certification 11982 Massachussets Laboratory Certification M-CT903 Rhode Island Certification 199 Tel: (203) 377-9984 Fax: (203) 377-9952 email: cet1@cetlabs.com 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 7 of 10 Project: NPU Stony Brook, Montville CET # : 6100216 Report Comments: Questions related to this report should be directed to David Ditta, Timothy Fusco, or Robert Blake at 203-377-9984. Sincerely, David Ditta Laboratory Director Sample Result Flags: E- The result is estimated, above the calibration range. H- The surrogate recovery is above the control limits. L- The surrogate recovery is below the control limits. B- The compound was detected in the laboratory blank. P- The Relative Percent Difference (RPD) of dual column analyses exceeds 40%. D- The RPD between the sample and the sample duplicate is high. Sample homogeneity may be a problem. +- The Surrogate was diluted out. *C1- The Continuing Calibration did not meet method specifications and was biased low for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased low. *C2- The Continuing Calibration did not meet method specifications and was biased high for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased high. *F1- The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the low side. *F2- The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the high side. I- The Analyte exceeds %RSD limits for the Initial Calibration. This is a non-directional bias. All results met standard operating procedures unless indicated by a data qualifier next to a sample result, or a narration in the QC report. Complete Environmental Testing is only responsible for the certified testing and is not directly responsible for the integrity of the sample before laboratory receipt. ND is None Detected at the specified detection limit All analyses were performed in house unless a Reference Laboratory is listed. Samples will be disposed of 30 days after the report date. 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 8 of 10 Project: NPU Stony Brook, Montville CET # : 6100216 CertificationsAnalyte CERTIFICATIONS Certified Analyses included in this Report CT-ETPH in Soil CTETPH EPA 8270D in Soil CT,NYNaphthalene CT,NY2-Methyl Naphthalene CT,NYAcenaphthylene CT,NYAcenaphthene CT,NYFluorene CT,NYPhenanthrene CT,NYAnthracene CT,NYFluoranthene CT,NYPyrene CT,NYBenzo[a]anthracene CT,NYChrysene CT,NYBenzo[b]fluoranthene CT,NYBenzo[k]fluoranthene CT,NYBenzo[a]pyrene CT,NYIndeno[1,2,3-cd]pyrene CT,NYDibenz[a,h]anthracene CT,NYBenzo[g,h,i]perylene Complete Environmental Testing operates under the following certifications and accreditations: Code Description Number Expires Connecticut Public Health 09/30/2016CTPH0116 New York Certification (NELAC)04/01/2017NY11982 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 9 of 10 Page 10 of 10 80 Lupes Drive Stratford, CT 06615 Tel: (203) 377-9984 Fax: (203) 377-9952 e-mail: cet1@cetlabs.com Client:Mr. Don Fortunato Soil & Environmental Service 61 Plants Dam Road East Lyme, CT 06333 Analytical Report CET# 6100217 Report Date:October 18, 2016 Project: NPU Stony Brook, Montville Rhode Island Certification: 199Massachusetts laboratory Certificate: M-CT903 Connecticut Laboratory Certificate: PH 0116 New York Certification: 11982 Page 1 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Sample ID Laboratory ID Matrix Collection Date/Time Receipt Date SAMPLE SUMMARY The sample(s) were received at 2.5 C. This report contains analytical data associated with following samples only. Waste 1 6100217-01 Soil 10/10/201616:0010/07/2016 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 2 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Notes Date/Time AnalyzedPreparedBatchDilutionRLResultLaboratory ID Client Sample ID Units Analyst: MRH Matrix: Soil Analyte: Percent Solids [SM 2540 G] 79 10/12/2016 10/14/2016 10:006100217-01 %Waste 1 1.0 1 B6J1205 Notes Date/Time AnalyzedPreparedBatchDilutionRLResultLaboratory ID Client Sample ID Units Analyst: JF Matrix: Soil Analyte: Flashpoint [EPA 1010A] >200 F 10/13/2016 10/13/2016 10:226100217-01 FWaste 1 NA 1 B6J1309 Notes Date/Time AnalyzedPreparedBatchDilutionRLResultLaboratory ID Client Sample ID Units Analyst: JZ Matrix: Soil Analyte: Reactive Sulfide [SW 846 Ch. 7] ND 10/17/2016 10/17/2016 09:466100217-01 mg/kg dryWaste 1 25 1 B6J1706 Notes Date/Time AnalyzedPreparedBatchDilutionRLResultLaboratory ID Client Sample ID Units Analyst: JZ Matrix: Soil Analyte: Reactive Cyanide [SW 846 Ch. 7] ND 10/17/2016 10/17/2016 09:466100217-01 mg/kg dryWaste 1 6.3 1 B6J1706 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 3 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Notes Date/Time AnalyzedPreparedBatchDilutionRLResultLaboratory ID Client Sample ID Units Analyst: KP Matrix: Soil Analyte: pH [EPA 9045D] 6.32 10/11/2016 10/11/2016 16:386100217-01 pH UnitsWaste 1 NA 1 B6J1124 Notes Date/Time AnalyzedPreparedBatchDilutionRLResultLaboratory ID Client Sample ID Units Analyst: KP Matrix: Soil Analyte: Mercury [EPA 7471B] ND 10/12/2016 10/17/2016 15:476100217-01 mg/kg dryWaste 1 0.25 1 B6J1212 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 4 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Client Sample ID Waste 1 Lab ID: 6100217-01 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: EPA 6010C Matrix: Soil Analyst: SSTotal Metals Lead 6.3 1 B6J1404 10/14/2016 10/17/2016 16:302.5 EPA 3050B Selenium ND 1 B6J1404 10/14/2016 10/17/2016 16:301.3 EPA 3050B Cadmium ND 1 B6J1404 10/14/2016 10/17/2016 16:300.63 EPA 3050B Chromium 17 1 B6J1404 10/14/2016 10/17/2016 16:302.5 EPA 3050B Arsenic 7.0 1 B6J1404 10/14/2016 10/17/2016 16:301.3 EPA 3050B Barium 49 1 B6J1404 10/14/2016 10/17/2016 16:302.5 EPA 3050B Silver ND 1 B6J1404 10/14/2016 10/17/2016 16:302.5 EPA 3050B Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH 5200 1 B6J1342 10/13/2016 10/14/2016 01:3363EPA 3550C 2*F1 Surrogate: Octacosane 93.2 %10/13/2016 10/14/2016 01:33B6J134250 - 150 2 C9-C28 Fuel Oil Range Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8270D Matrix: Soil Analyst: ALBSemivolatile Organics Phenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 1,3-Dichlorobenzene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A n-Nitroso-di-n-propylamine ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Pyridine ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A *C2 n-Nitroso-dimethylamine ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A bis(2-Chloroethyl)ether ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 5 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Client Sample ID Waste 1 Lab ID: 6100217-01 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8270D Matrix: Soil Analyst: ALBSemivolatile Organics Aniline ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2-Chlorophenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 1,4-Dichlorobenzene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Benzyl Alcohol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 1,2-Dichlorobenzene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A bis(2-Chloroisopropyl)ether ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Hexachloroethane ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2-Methyl Phenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 3+4 Methyl Phenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Naphthalene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2-Nitrophenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2,4-Dichlorophenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Hexachlorobutadiene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 4-Chloro-3-methylphenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Nitrobenzene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Isophorone ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2,4-Dimethylphenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A bis(2-Chloroethoxy)methane ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Benzoic Acid ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 1,2,4-Trichlorobenzene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2,6-Dichlorophenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 4-Chloroaniline ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 1,2,4,5-Tetrachlorobenzene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2-Methyl Naphthalene 9700 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Acenaphthylene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Acenaphthene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Dibenzofuran ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Fluorene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Hexachlorocyclopentadiene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A *F1*C1 2,4,6-Trichlorophenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2,4,5-Trichlorophenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2,4-Dinitrophenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A *F1*C1 4-Nitrophenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2-Chloronaphthalene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2-Nitroaniline ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Dimethylphthalate ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2,6-Dinitrotoluene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 4-Nitroaniline ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2,4-Dinitrotoluene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2,3,4,6-Tetrachlorophenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 4-Chlorophenyl-phenylether ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 6 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Client Sample ID Waste 1 Lab ID: 6100217-01 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8270D Matrix: Soil Analyst: ALBSemivolatile Organics Diethylphthalate ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Phenanthrene 1400 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Anthracene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Carbazole ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Fluoranthene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Pyrene 540 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A n-Nitrosodiphenylamine ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Pentachlorophenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 3-Nitroaniline ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 4,6-Dinitro-2-methylphenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A *C1 1,2-Diphenylhydrazine ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 4-Bromophenyl-phenylether ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Hexachlorobenzene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Di-n-butylphthalate ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Pentachloronitrobenzene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Benzo[a]anthracene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Chrysene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Butylbenzylphthalate ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 3,3-Dichlorobenzidine ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A *F1 bis(2-Ethylhexyl)phthalate ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Di-n-octylphthalate ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Benzo[b]fluoranthene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Benzo[k]fluoranthene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Benzo[a]pyrene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Indeno[1,2,3-cd]pyrene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Dibenz[a,h]anthracene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Benzo[g,h,i]perylene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Surrogate: 2-Fluorophenol 59.6 %10/11/2016 10/12/2016 20:05B6J112130 - 130 Surrogate: Phenol-d6 60.9 %10/11/2016 10/12/2016 20:05B6J112130 - 130 Surrogate: Nitrobenzene-d5 61.4 %10/11/2016 10/12/2016 20:05B6J112130 - 130 Surrogate: 2-Fluorobiphenyl 108 %10/11/2016 10/12/2016 20:05B6J112130 - 130 Surrogate: 2,4,6-Tribromophenol 86.0 %10/11/2016 10/12/2016 20:05B6J112130 - 130 Surrogate: Terphenyl-d14 110 %10/11/2016 10/12/2016 20:05B6J112130 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 7 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Client Sample ID Waste 1 Lab ID: 6100217-01 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Dichlorodifluoromethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:543600EPA 5035A-H *C1 Chloromethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:542400EPA 5035A-H *C1 Vinyl Chloride ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H *C1 Bromomethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:542400EPA 5035A-H Chloroethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:542400EPA 5035A-H Trichlorofluoromethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:549600EPA 5035A-H Acetone ND 379.51 B6J1719 10/17/2016 10/17/2016 14:5436000EPA 5035A-H Acrylonitrile ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541900EPA 5035A-H Trichlorotrifluoroethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:549600EPA 5035A-H 1,1-Dichloroethene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H *C2 Methylene Chloride ND 379.51 B6J1719 10/17/2016 10/17/2016 14:5412000EPA 5035A-H Carbon Disulfide ND 379.51 B6J1719 10/17/2016 10/17/2016 14:542400EPA 5035A-H *C2 Methyl-t-Butyl Ether (MTBE)ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H trans-1,2-Dichloroethene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,1-Dichloroethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 2-Butanone (MEK)ND 379.51 B6J1719 10/17/2016 10/17/2016 14:546000EPA 5035A-H 2,2-Dichloropropane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H cis-1,2-Dichloroethene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Chloroform ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Tetrahydrofuran ND 379.51 B6J1719 10/17/2016 10/17/2016 14:546000EPA 5035A-H 1,1,1-Trichloroethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Carbon Tetrachloride ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H *C2 1,1-Dichloropropene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Benzene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,2-Dichloroethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Trichloroethene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,2-Dichloropropane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Dibromomethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Bromodichloromethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Methyl Isobutyl Ketone ND 379.51 B6J1719 10/17/2016 10/17/2016 14:546000EPA 5035A-H cis-1,3-Dichloropropene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Toluene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H trans-1,3-Dichloropropene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 2-Hexanone ND 379.51 B6J1719 10/17/2016 10/17/2016 14:546000EPA 5035A-H 1,1,2-Trichloroethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Tetrachloroethene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,3-Dichloropropane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Dibromochloromethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,2-Dibromoethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H trans-1,4-Dichloro-2-Butene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:546000EPA 5035A-H Chlorobenzene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 8 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Client Sample ID Waste 1 Lab ID: 6100217-01 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics 1,1,1,2-Tetrachloroethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Ethylbenzene 3500 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H m+p Xylenes 16000 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H o-Xylene 13000 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Styrene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Bromoform ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Isopropylbenzene 1700 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,1,2,2-Tetrachloroethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Bromobenzene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,2,3-Trichloropropane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H n-Propylbenzene 6000 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 2-Chlorotoluene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 4-Chlorotoluene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,3,5-Trimethylbenzene 18000 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H tert-Butylbenzene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,2,4-Trimethylbenzene 38000 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H sec-Butylbenzene 3500 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,3-Dichlorobenzene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 4-Isopropyltoluene 2400 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,4-Dichlorobenzene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,2-Dichlorobenzene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H n-Butylbenzene 7100 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,2-Dibromo-3-Chloropropane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,2,4-Trichlorobenzene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Hexachlorobutadiene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Naphthalene 4400 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,2,3-Trichlorobenzene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Surrogate: 1,2-Dichloroethane-d4 109 %10/17/2016 10/17/2016 14:54B6J171970 - 130 Surrogate: Toluene-d8 101 %10/17/2016 10/17/2016 14:54B6J171970 - 130 Surrogate: 4-Bromofluorobenzene 99.5 %10/17/2016 10/17/2016 14:54B6J171970 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 9 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 QUALITY CONTROL SECTION Batch B6J1121 - EPA 8270D Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes Blank (B6J1121-BLK1)Prepared: 10/11/2016 Analyzed: 10/12/2016 Phenol 300ND 1,3-Dichlorobenzene 300ND n-Nitroso-di-n-propylamine 300ND Pyridine 300ND n-Nitroso-dimethylamine 300ND bis(2-Chloroethyl)ether 300ND Aniline 300ND 2-Chlorophenol 300ND 1,4-Dichlorobenzene 300ND Benzyl Alcohol 300ND 1,2-Dichlorobenzene 300ND bis(2-Chloroisopropyl)ether 300ND Hexachloroethane 300ND 2-Methyl Phenol 300ND 3+4 Methyl Phenol 300ND Naphthalene 300ND 2-Nitrophenol 300ND 2,4-Dichlorophenol 300ND Hexachlorobutadiene 300ND 4-Chloro-3-methylphenol 300ND Nitrobenzene 300ND Isophorone 300ND 2,4-Dimethylphenol 300ND bis(2-Chloroethoxy)methane 300ND Benzoic Acid 300ND 1,2,4-Trichlorobenzene 300ND 2,6-Dichlorophenol 300ND 4-Chloroaniline 300ND 1,2,4,5-Tetrachlorobenzene 300ND 2-Methyl Naphthalene 300ND Acenaphthylene 300ND Acenaphthene 300ND Dibenzofuran 300ND Fluorene 300ND Hexachlorocyclopentadiene 300ND 2,4,6-Trichlorophenol 300ND 2,4,5-Trichlorophenol 300ND 2,4-Dinitrophenol 300ND 4-Nitrophenol 300ND 2-Chloronaphthalene 300ND 2-Nitroaniline 300ND Dimethylphthalate 300ND 2,6-Dinitrotoluene 300ND 4-Nitroaniline 300ND 2,4-Dinitrotoluene 300ND 2,3,4,6-Tetrachlorophenol 300ND 4-Chlorophenyl-phenylether 300ND Diethylphthalate 300ND Phenanthrene 300ND 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 10 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes Blank (B6J1121-BLK1) - Continued Prepared: 10/11/2016 Analyzed: 10/12/2016 Anthracene 300ND Carbazole 300ND Fluoranthene 300ND Pyrene 300ND n-Nitrosodiphenylamine 300ND Pentachlorophenol 300ND 3-Nitroaniline 300ND 4,6-Dinitro-2-methylphenol 300ND 1,2-Diphenylhydrazine 300ND 4-Bromophenyl-phenylether 300ND Hexachlorobenzene 300ND Di-n-butylphthalate 300ND Pentachloronitrobenzene 300ND Benzo[a]anthracene 300ND Chrysene 300ND Butylbenzylphthalate 300ND 3,3-Dichlorobenzidine 300ND bis(2-Ethylhexyl)phthalate 300ND Di-n-octylphthalate 300ND Benzo[b]fluoranthene 300ND Benzo[k]fluoranthene 300ND Benzo[a]pyrene 300ND Indeno[1,2,3-cd]pyrene 300ND Dibenz[a,h]anthracene 300ND Benzo[g,h,i]perylene 300ND 63.3 30 - 130Surrogate: 2-Fluorophenol 62.1 30 - 130Surrogate: Phenol-d6 60.2 30 - 130Surrogate: Nitrobenzene-d5 65.1 30 - 130Surrogate: 2-Fluorobiphenyl 70.7 30 - 130Surrogate: 2,4,6-Tribromophenol 82.7 30 - 130Surrogate: Terphenyl-d14 LCS (B6J1121-BS1)Prepared: 10/11/2016 Analyzed: 10/12/2016 Phenol 300 69.0 30 - 1302760 4,000.000 1,3-Dichlorobenzene 300 53.4 40 - 1402140 4,000.000 n-Nitroso-di-n-propylamine 300 60.8 40 - 1402430 4,000.000 Pyridine 300 44.6 40 - 1401780 4,000.000 n-Nitroso-dimethylamine 300 58.3 40 - 1402330 4,000.000 bis(2-Chloroethyl)ether 300 57.9 40 - 1402320 4,000.000 Aniline 300 47.3 40 - 1401890 4,000.000 2-Chlorophenol 300 62.5 30 - 1302500 4,000.000 1,4-Dichlorobenzene 300 54.7 40 - 1402190 4,000.000 Benzyl Alcohol 300 50.3 30 - 1302010 4,000.000 1,2-Dichlorobenzene 300 54.9 40 - 1402200 4,000.000 bis(2-Chloroisopropyl)ether 300 49.0 40 - 1401960 4,000.000 Hexachloroethane 300 47.1 40 - 1401890 4,000.000 2-Methyl Phenol 300 70.7 30 - 1302830 4,000.000 3+4 Methyl Phenol 300 66.2 30 - 1302650 4,000.000 Naphthalene 300 63.1 40 - 1402530 4,000.000 2-Nitrophenol 300 57.9 30 - 1302310 4,000.000 2,4-Dichlorophenol 300 64.3 30 - 1302570 4,000.000 Hexachlorobutadiene 300 57.9 40 - 1402320 4,000.000 4-Chloro-3-methylphenol 300 68.0 30 - 1302720 4,000.000 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 11 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes LCS (B6J1121-BS1) - Continued Prepared: 10/11/2016 Analyzed: 10/12/2016 Nitrobenzene 300 60.6 40 - 1402420 4,000.000 Isophorone 300 63.2 40 - 1402530 4,000.000 2,4-Dimethylphenol 300 65.7 30 - 1302630 4,000.000 bis(2-Chloroethoxy)methane 300 63.7 40 - 1402550 4,000.000 Benzoic Acid 300 41.7 30 - 1301670 4,000.000 1,2,4-Trichlorobenzene 300 58.1 40 - 1402320 4,000.000 2,6-Dichlorophenol 300 59.6 30 - 1302380 4,000.000 4-Chloroaniline 300 42.0 40 - 1401680 4,000.000 1,2,4,5-Tetrachlorobenzene 300 62.2 40 - 1402490 4,000.000 2-Methyl Naphthalene 300 63.4 40 - 1402540 4,000.000 Acenaphthylene 300 62.6 40 - 1402500 4,000.000 Acenaphthene 300 68.9 40 - 1402760 4,000.000 Dibenzofuran 300 70.7 40 - 1402830 4,000.000 Fluorene 300 71.2 40 - 1402850 4,000.000 Hexachlorocyclopentadiene 300 36.2 40 - 1401450 L 4,000.000 2,4,6-Trichlorophenol 300 67.0 30 - 1302680 4,000.000 2,4,5-Trichlorophenol 300 72.9 30 - 1302920 4,000.000 2,4-Dinitrophenol 300 27.9 30 - 1301120 L 4,000.000 4-Nitrophenol 300 64.3 30 - 1302570 4,000.000 2-Chloronaphthalene 300 62.6 40 - 1402510 4,000.000 2-Nitroaniline 300 71.9 40 - 1402880 4,000.000 Dimethylphthalate 300 72.3 40 - 1402890 4,000.000 2,6-Dinitrotoluene 300 69.0 40 - 1402760 4,000.000 4-Nitroaniline 300 70.4 40 - 1402810 4,000.000 2,4-Dinitrotoluene 300 70.5 40 - 1402820 4,000.000 2,3,4,6-Tetrachlorophenol 300 71.4 30 - 1302860 4,000.000 4-Chlorophenyl-phenylether 300 71.3 40 - 1402850 4,000.000 Diethylphthalate 300 74.0 40 - 1402960 4,000.000 Phenanthrene 300 76.0 40 - 1403040 4,000.000 Anthracene 300 76.1 40 - 1403040 4,000.000 Carbazole 300 95.3 40 - 1403810 4,000.000 Fluoranthene 300 74.9 40 - 1403000 4,000.000 Pyrene 300 75.4 40 - 1403020 4,000.000 n-Nitrosodiphenylamine 300 93.3 40 - 1403730 4,000.000 Pentachlorophenol 300 63.0 30 - 1302520 4,000.000 3-Nitroaniline 300 66.9 40 - 1402670 4,000.000 4,6-Dinitro-2-methylphenol 300 30.7 30 - 1301230 4,000.000 1,2-Diphenylhydrazine 300 70.4 40 - 1402820 4,000.000 4-Bromophenyl-phenylether 300 69.8 40 - 1402790 4,000.000 Hexachlorobenzene 300 69.6 40 - 1402790 4,000.000 Di-n-butylphthalate 300 75.5 40 - 1403020 4,000.000 Pentachloronitrobenzene 300 78.9 40 - 1403160 4,000.000 Benzo[a]anthracene 300 81.5 40 - 1403260 4,000.000 Chrysene 300 80.3 40 - 1403210 4,000.000 Butylbenzylphthalate 300 80.5 40 - 1403220 4,000.000 3,3-Dichlorobenzidine 300 40 - 1404280 L bis(2-Ethylhexyl)phthalate 300 75.5 40 - 1403020 4,000.000 Di-n-octylphthalate 300 85.3 40 - 1403410 4,000.000 Benzo[b]fluoranthene 300 92.0 40 - 1403680 4,000.000 Benzo[k]fluoranthene 300 105 40 - 1404200 4,000.000 Benzo[a]pyrene 300 101 40 - 1404050 4,000.000 Indeno[1,2,3-cd]pyrene 300 105 40 - 1404220 4,000.000 Dibenz[a,h]anthracene 300 113 40 - 1404540 4,000.000 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 12 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes LCS (B6J1121-BS1) - Continued Prepared: 10/11/2016 Analyzed: 10/12/2016 Benzo[g,h,i]perylene 300 93.8 40 - 1403750 4,000.000 64.3 30 - 130Surrogate: 2-Fluorophenol 64.5 30 - 130Surrogate: Phenol-d6 62.7 30 - 130Surrogate: Nitrobenzene-d5 67.6 30 - 130Surrogate: 2-Fluorobiphenyl 82.8 30 - 130Surrogate: 2,4,6-Tribromophenol 81.3 30 - 130Surrogate: Terphenyl-d14 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 13 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Batch B6J1124 - EPA 9045D Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(pH Units) (pH Units)Notes Blank (B6J1124-BLK1)Prepared: 10/11/2016 Analyzed: 10/11/2016 pH 5.91 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 14 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Batch B6J1205 - SM 2540 G Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(%) (%)Notes Duplicate (B6J1205-DUP1)Source: 6100217-01 Prepared: 10/12/2016 Analyzed: 10/14/2016 Percent Solids 1.0 79 0.393 20080 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 15 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Batch B6J1212 - EPA 7471B Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(mg/kg) (mg/kg)Notes Blank (B6J1212-BLK1)Prepared: 10/12/2016 Analyzed: 10/17/2016 Mercury 0.20ND LCS (B6J1212-BS1)Prepared: 10/12/2016 Analyzed: 10/17/2016 Mercury 0.20 107 80 - 1202.68 2.500 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 16 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Batch B6J1342 - CT-ETPH Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(mg/kg) (mg/kg)Notes Blank (B6J1342-BLK1)Prepared: 10/13/2016 Analyzed: 10/13/2016 ETPH 50ND 108 50 - 150Surrogate: Octacosane LCS (B6J1342-BS1)Prepared: 10/13/2016 Analyzed: 10/13/2016 ETPH 50 60 - 1201260 L 105 50 - 150Surrogate: Octacosane 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 17 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Batch B6J1404 - EPA 6010C Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(mg/kg) (mg/kg)Notes Blank (B6J1404-BLK1)Prepared: 10/14/2016 Analyzed: 10/17/2016 Lead 2.0ND Selenium 1.0ND Cadmium 0.50ND Chromium 2.0ND Arsenic 1.0ND Barium 2.0ND Silver 2.0ND LCS (B6J1404-BS1)Prepared: 10/14/2016 Analyzed: 10/17/2016 Lead 2.0 98.4 80 - 12024.6 25.000 Selenium 1.0 98.2 80 - 12049.1 50.000 Cadmium 0.50 111 80 - 12027.8 25.000 Chromium 2.0 100 80 - 12025.1 25.000 Arsenic 1.0 102 80 - 12025.4 25.000 Barium 2.0 111 80 - 12027.8 25.000 Silver 2.0 94.3 80 - 1204.71 5.000 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 18 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Batch B6J1706 - SW 846 Ch. 7 Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(mg/kg) (mg/kg)Notes Blank (B6J1706-BLK1)Prepared: 10/17/2016 Analyzed: 10/17/2016 Reactive Sulfide 20ND 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 19 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(mg/kg) (mg/kg)Notes Blank (B6J1706-BLK1)Prepared: 10/17/2016 Analyzed: 10/17/2016 Reactive Cyanide 5.0ND 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 20 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Batch B6J1719 - EPA 8260C Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes Blank (B6J1719-BLK1)Prepared: 10/17/2016 Analyzed: 10/17/2016 Dichlorodifluoromethane 7.5ND Chloromethane 5.0ND Vinyl Chloride 2.5ND Bromomethane 5.0ND Chloroethane 5.0ND Trichlorofluoromethane 20ND Acetone 75ND Acrylonitrile 4.0ND Trichlorotrifluoroethane 20ND 1,1-Dichloroethene 2.5ND Methylene Chloride 25ND Carbon Disulfide 5.0ND Methyl-t-Butyl Ether (MTBE)2.5ND trans-1,2-Dichloroethene 2.5ND 1,1-Dichloroethane 2.5ND 2-Butanone (MEK)13ND 2,2-Dichloropropane 2.5ND cis-1,2-Dichloroethene 2.5ND Chloroform 2.5ND Tetrahydrofuran 13ND 1,1,1-Trichloroethane 2.5ND Carbon Tetrachloride 2.5ND 1,1-Dichloropropene 2.5ND Benzene 2.5ND 1,2-Dichloroethane 2.5ND Trichloroethene 2.5ND 1,2-Dichloropropane 2.5ND Dibromomethane 2.5ND Bromodichloromethane 2.5ND Methyl Isobutyl Ketone 13ND cis-1,3-Dichloropropene 2.5ND Toluene 2.5ND trans-1,3-Dichloropropene 2.5ND 2-Hexanone 13ND 1,1,2-Trichloroethane 2.5ND Tetrachloroethene 2.5ND 1,3-Dichloropropane 2.5ND Dibromochloromethane 2.5ND 1,2-Dibromoethane 2.5ND trans-1,4-Dichloro-2-Butene 13ND Chlorobenzene 2.5ND 1,1,1,2-Tetrachloroethane 2.5ND Ethylbenzene 2.5ND m+p Xylenes 2.5ND o-Xylene 2.5ND Styrene 2.5ND Bromoform 2.5ND Isopropylbenzene 2.5ND 1,1,2,2-Tetrachloroethane 2.5ND Bromobenzene 2.5ND 1,2,3-Trichloropropane 2.5ND n-Propylbenzene 2.5ND 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 21 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes Blank (B6J1719-BLK1) - Continued Prepared: 10/17/2016 Analyzed: 10/17/2016 2-Chlorotoluene 2.5ND 4-Chlorotoluene 2.5ND 1,3,5-Trimethylbenzene 2.5ND tert-Butylbenzene 2.5ND 1,2,4-Trimethylbenzene 2.5ND sec-Butylbenzene 2.5ND 1,3-Dichlorobenzene 2.5ND 4-Isopropyltoluene 2.5ND 1,4-Dichlorobenzene 2.5ND 1,2-Dichlorobenzene 2.5ND n-Butylbenzene 2.5ND 1,2-Dibromo-3-Chloropropane 2.5ND 1,2,4-Trichlorobenzene 2.5ND Hexachlorobutadiene 2.5ND Naphthalene 2.5ND 1,2,3-Trichlorobenzene 2.5ND 107 70 - 130Surrogate: 1,2-Dichloroethane-d4 99.0 70 - 130Surrogate: Toluene-d8 104 70 - 130Surrogate: 4-Bromofluorobenzene LCS (B6J1719-BS1)Prepared: 10/17/2016 Analyzed: 10/17/2016 Dichlorodifluoromethane 7.5 91.6 70 - 13045.8 50.000 Chloromethane 5.0 90.5 70 - 13045.3 50.000 Vinyl Chloride 2.5 98.4 70 - 13049.2 50.000 Bromomethane 5.0 108 70 - 13053.8 50.000 Chloroethane 5.0 102 70 - 13050.8 50.000 Trichlorofluoromethane 20 114 70 - 13057.2 50.000 Acetone 75 116 70 - 130116 100.000 Acrylonitrile 4.0 97.7 70 - 13048.9 50.000 Trichlorotrifluoroethane 20 120 70 - 13060.2 50.000 1,1-Dichloroethene 2.5 114 70 - 13057.2 50.000 Methylene Chloride 25 110 70 - 13055.1 50.000 Carbon Disulfide 5.0 114 70 - 13057.0 50.000 Methyl-t-Butyl Ether (MTBE)2.5 98.7 70 - 13049.3 50.000 trans-1,2-Dichloroethene 2.5 110 70 - 13055.0 50.000 1,1-Dichloroethane 2.5 107 70 - 13053.6 50.000 2-Butanone (MEK)13 104 70 - 130104 100.000 2,2-Dichloropropane 2.5 114 70 - 13056.8 50.000 cis-1,2-Dichloroethene 2.5 105 70 - 13052.4 50.000 Chloroform 2.5 104 70 - 13051.9 50.000 Tetrahydrofuran 13 95.0 70 - 13047.5 50.000 1,1,1-Trichloroethane 2.5 115 70 - 13057.3 50.000 Carbon Tetrachloride 2.5 116 70 - 13058.0 50.000 1,1-Dichloropropene 2.5 111 70 - 13055.4 50.000 Benzene 2.5 102 70 - 13050.8 50.000 1,2-Dichloroethane 2.5 98.3 70 - 13049.2 50.000 Trichloroethene 2.5 107 70 - 13053.5 50.000 1,2-Dichloropropane 2.5 98.2 70 - 13049.1 50.000 Dibromomethane 2.5 97.9 70 - 13049.0 50.000 Bromodichloromethane 2.5 101 70 - 13050.4 50.000 Methyl Isobutyl Ketone 13 99.4 70 - 13099.4 100.000 cis-1,3-Dichloropropene 2.5 97.7 70 - 13048.9 50.000 Toluene 2.5 97.0 70 - 13048.5 50.000 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 22 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes LCS (B6J1719-BS1) - Continued Prepared: 10/17/2016 Analyzed: 10/17/2016 trans-1,3-Dichloropropene 2.5 97.7 70 - 13048.9 50.000 2-Hexanone 13 102 70 - 130102 100.000 1,1,2-Trichloroethane 2.5 94.9 70 - 13047.4 50.000 Tetrachloroethene 2.5 109 70 - 13054.5 50.000 1,3-Dichloropropane 2.5 94.9 70 - 13047.5 50.000 Dibromochloromethane 2.5 101 70 - 13050.5 50.000 1,2-Dibromoethane 2.5 96.1 70 - 13048.0 50.000 trans-1,4-Dichloro-2-Butene 13 98.6 70 - 13049.3 50.000 Chlorobenzene 2.5 99.8 70 - 13049.9 50.000 1,1,1,2-Tetrachloroethane 2.5 102 70 - 13050.9 50.000 Ethylbenzene 2.5 106 70 - 13053.0 50.000 m+p Xylenes 2.5 106 70 - 130106 100.000 o-Xylene 2.5 103 70 - 13051.6 50.000 Styrene 2.5 102 70 - 13050.9 50.000 Bromoform 2.5 101 70 - 13050.3 50.000 Isopropylbenzene 2.5 108 70 - 13054.2 50.000 1,1,2,2-Tetrachloroethane 2.5 95.0 70 - 13047.5 50.000 Bromobenzene 2.5 102 70 - 13051.0 50.000 1,2,3-Trichloropropane 2.5 101 70 - 13050.5 50.000 n-Propylbenzene 2.5 112 70 - 13055.8 50.000 2-Chlorotoluene 2.5 106 70 - 13053.0 50.000 4-Chlorotoluene 2.5 105 70 - 13052.7 50.000 1,3,5-Trimethylbenzene 2.5 110 70 - 13054.9 50.000 tert-Butylbenzene 2.5 113 70 - 13056.4 50.000 1,2,4-Trimethylbenzene 2.5 108 70 - 13053.8 50.000 sec-Butylbenzene 2.5 114 70 - 13056.9 50.000 1,3-Dichlorobenzene 2.5 104 70 - 13051.9 50.000 4-Isopropyltoluene 2.5 114 70 - 13057.1 50.000 1,4-Dichlorobenzene 2.5 102 70 - 13051.2 50.000 1,2-Dichlorobenzene 2.5 101 70 - 13050.6 50.000 n-Butylbenzene 2.5 116 70 - 13057.8 50.000 1,2-Dibromo-3-Chloropropane 2.5 104 70 - 13052.1 50.000 1,2,4-Trichlorobenzene 2.5 103 70 - 13051.7 50.000 Hexachlorobutadiene 2.5 116 70 - 13057.9 50.000 Naphthalene 2.5 98.3 70 - 13049.2 50.000 1,2,3-Trichlorobenzene 2.5 101 70 - 13050.5 50.000 102 70 - 130Surrogate: 1,2-Dichloroethane-d4 99.8 70 - 130Surrogate: Toluene-d8 99.5 70 - 130Surrogate: 4-Bromofluorobenzene 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 23 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Quality Control Definitions and Abbreviations 80 Lupes Drive Stratford, CT 06615 Internal Standard (IS)An Analyte added to each sample or sample extract. An internal standard is used to monitor retention time, calculate relative response, and quantify analytes of interest. Surrogate Recovery The % recovery for non-target organic compounds that are spiked into all samples. Used to determine method performance. Continuing Calibration An analytical standard analyzed with each set of samples to verify initial calibration of the system. Batch Samples that are analyzed together with the same method, sequence and lot of reagents within the same time period. ND Not detected RL Reporting Limit Dilution Multiplier added to detection levels (MDL) and/or sample results due to interferences and/or high concentration of target compounds. Duplicate Result from the duplicate analysis of a sample. Result Amount of analyte found in a sample. Spike Level Amount of analyte added to a sample Matrix Spike Result Amount of analyte found including amount that was spiked. Matrix Spike Dup Amount of analyte found in duplicate spikes including amount that was spike. Matrix Spike % Recovery % Recovery of spiked amount in sample. Matrix Spike Dup % Recovery % Recovery of spiked duplicate amount in sample. RPD Relative percent difference between Matrix Spike and Matrix Spike Duplicate. Blank Method Blank that has been taken through all steps of the analysis. LCS % Recovery Laboratory Control Sample percent recovery. The amount of analyte recovered from a fortified sample. Recovery Limits A range within which specified measurements results must fall to be compliant. CC Calibration Verification Flags: H-Recovery is above the control limits L-Recovery is below the control limits B-Compound detected in the Blank P-RPD of dual column results exceeds 40% #-Sample result too high for accurate spike recovery. Connecticut Laboratory Certification PH0116 New York Certification 11982 Massachussets Laboratory Certification M-CT903 Rhode Island Certification 199 Tel: (203) 377-9984 Fax: (203) 377-9952 email: cet1@cetlabs.com 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 24 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Report Comments: Questions related to this report should be directed to David Ditta, Timothy Fusco, or Robert Blake at 203-377-9984. Sincerely, David Ditta Laboratory Director Sample Result Flags: E- The result is estimated, above the calibration range. H- The surrogate recovery is above the control limits. L- The surrogate recovery is below the control limits. B- The compound was detected in the laboratory blank. P- The Relative Percent Difference (RPD) of dual column analyses exceeds 40%. D- The RPD between the sample and the sample duplicate is high. Sample homogeneity may be a problem. +- The Surrogate was diluted out. *C1- The Continuing Calibration did not meet method specifications and was biased low for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased low. *C2- The Continuing Calibration did not meet method specifications and was biased high for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased high. *F1- The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the low side. *F2- The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the high side. I- The Analyte exceeds %RSD limits for the Initial Calibration. This is a non-directional bias. All results met standard operating procedures unless indicated by a data qualifier next to a sample result, or a narration in the QC report. Complete Environmental Testing is only responsible for the certified testing and is not directly responsible for the integrity of the sample before laboratory receipt. ND is None Detected at the specified detection limit All analyses were performed in house unless a Reference Laboratory is listed. Samples will be disposed of 30 days after the report date. 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 25 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 CertificationsAnalyte CERTIFICATIONS Certified Analyses included in this Report CT-ETPH in Soil CTETPH EPA 1010A in Soil CT,NYFlashpoint EPA 6010C in Soil CT,NYLead CT,NYSelenium CT,NYCadmium CT,NYChromium CT,NYArsenic CT,NYBarium CT,NYSilver EPA 7471B in Soil CT,NYMercury EPA 8260C in Soil CT,NYDichlorodifluoromethane CT,NYChloromethane CT,NYVinyl Chloride CT,NYBromomethane CT,NYChloroethane CT,NYTrichlorofluoromethane CT,NYAcetone CT,NYAcrylonitrile CT,NYTrichlorotrifluoroethane CT,NY1,1-Dichloroethene CT,NYMethylene Chloride CT,NYCarbon Disulfide CT,NYMethyl-t-Butyl Ether (MTBE) CT,NYtrans-1,2-Dichloroethene CT,NY1,1-Dichloroethane CT,NY2-Butanone (MEK) CT,NY2,2-Dichloropropane CT,NYcis-1,2-Dichloroethene CT,NYChloroform CTTetrahydrofuran CT,NY1,1,1-Trichloroethane CT,NYCarbon Tetrachloride CT,NY1,1-Dichloropropene CT,NYBenzene CT,NY1,2-Dichloroethane CT,NYTrichloroethene CT,NY1,2-Dichloropropane CT,NYDibromomethane CT,NYBromodichloromethane 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 26 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 CertificationsAnalyte CERTIFICATIONS Certified Analyses included in this Report EPA 8260C in Soil CT,NYMethyl Isobutyl Ketone CT,NYcis-1,3-Dichloropropene CT,NYToluene CT,NYtrans-1,3-Dichloropropene CT,NY2-Hexanone CT,NY1,1,2-Trichloroethane CT,NYTetrachloroethene CT,NY1,3-Dichloropropane CT,NYDibromochloromethane CT,NY1,2-Dibromoethane CT,NYtrans-1,4-Dichloro-2-Butene CT,NYChlorobenzene CT,NY1,1,1,2-Tetrachloroethane CT,NYEthylbenzene CT,NYm+p Xylenes CT,NYo-Xylene CT,NYStyrene CT,NYBromoform CT,NYIsopropylbenzene CT,NY1,1,2,2-Tetrachloroethane CT,NYBromobenzene CT,NY1,2,3-Trichloropropane CT,NYn-Propylbenzene CT,NY2-Chlorotoluene CT,NY4-Chlorotoluene CT,NY1,3,5-Trimethylbenzene CT,NYtert-Butylbenzene CT,NY1,2,4-Trimethylbenzene CT,NYsec-Butylbenzene CT,NY1,3-Dichlorobenzene CT,NY4-Isopropyltoluene CT,NY1,4-Dichlorobenzene CT,NY1,2-Dichlorobenzene CT,NYn-Butylbenzene CT,NY1,2-Dibromo-3-Chloropropane CT,NY1,2,4-Trichlorobenzene CT,NYHexachlorobutadiene CT,NYNaphthalene CT1,2,3-Trichlorobenzene EPA 8270D in Soil CT,NYPhenol CT,NY1,3-Dichlorobenzene CT,NYn-Nitroso-di-n-propylamine CT,NYPyridine 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 27 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 CertificationsAnalyte CERTIFICATIONS Certified Analyses included in this Report EPA 8270D in Soil CT,NYn-Nitroso-dimethylamine CT,NYbis(2-Chloroethyl)ether CT,NYAniline CT,NY2-Chlorophenol CT,NY1,4-Dichlorobenzene CT,NYBenzyl Alcohol CT,NY1,2-Dichlorobenzene CT,NYbis(2-Chloroisopropyl)ether CT,NYHexachloroethane CT,NY2-Methyl Phenol CT,NY3+4 Methyl Phenol CT,NYNaphthalene CT,NY2-Nitrophenol CT,NY2,4-Dichlorophenol CT,NYHexachlorobutadiene CT,NY4-Chloro-3-methylphenol CT,NYNitrobenzene CT,NYIsophorone CT,NY2,4-Dimethylphenol CT,NYbis(2-Chloroethoxy)methane CT,NYBenzoic Acid CT,NY1,2,4-Trichlorobenzene CT,NY2,6-Dichlorophenol CT,NY4-Chloroaniline CT,NY1,2,4,5-Tetrachlorobenzene CT,NY2-Methyl Naphthalene CT,NYAcenaphthylene CT,NYAcenaphthene CT,NYDibenzofuran CT,NYFluorene CT,NYHexachlorocyclopentadiene CT,NY2,4,6-Trichlorophenol CT,NY2,4,5-Trichlorophenol CT,NY2,4-Dinitrophenol CT,NY4-Nitrophenol CT,NY2-Chloronaphthalene CT,NY2-Nitroaniline CT,NYDimethylphthalate CT,NY2,6-Dinitrotoluene CT,NY4-Nitroaniline CT,NY2,4-Dinitrotoluene CT,NY2,3,4,6-Tetrachlorophenol CT,NY4-Chlorophenyl-phenylether CT,NYDiethylphthalate CT,NYPhenanthrene 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 28 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 CertificationsAnalyte CERTIFICATIONS Certified Analyses included in this Report EPA 8270D in Soil CT,NYAnthracene CT,NYCarbazole CT,NYFluoranthene CT,NYPyrene CT,NYn-Nitrosodiphenylamine CT,NYPentachlorophenol CT,NY3-Nitroaniline CT,NY4,6-Dinitro-2-methylphenol CT1,2-Diphenylhydrazine CT,NY4-Bromophenyl-phenylether CT,NYHexachlorobenzene CT,NYDi-n-butylphthalate CT,NYPentachloronitrobenzene CT,NYBenzo[a]anthracene CT,NYChrysene CT,NYButylbenzylphthalate CT,NY3,3-Dichlorobenzidine CT,NYbis(2-Ethylhexyl)phthalate CT,NYDi-n-octylphthalate CT,NYBenzo[b]fluoranthene CT,NYBenzo[k]fluoranthene CT,NYBenzo[a]pyrene CT,NYIndeno[1,2,3-cd]pyrene CT,NYDibenz[a,h]anthracene CT,NYBenzo[g,h,i]perylene EPA 9045D in Soil CTpH SW 846 Ch. 7 in Soil CTReactive Cyanide CTReactive Sulfide Complete Environmental Testing operates under the following certifications and accreditations: Code Description Number Expires Connecticut Public Health 09/30/2016CTPH0116 New York Certification (NELAC)04/01/2017NY11982 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 29 of 30 Page 30 of 30 80 Lupes Drive Stratford, CT 06615 Tel: (203) 377-9984 Fax: (203) 377-9952 e-mail: cet1@cetlabs.com Client:Mr. Don Fortunato Soil & Environmental Service 61 Plants Dam Road East Lyme, CT 06333 Analytical Report CET# 6110624 Report Date:December 01, 2016 Project: NPU, Oakdale Rhode Island Certification: 199Massachusetts laboratory Certificate: M-CT903 Connecticut Laboratory Certificate: PH 0116 New York NELAP Accreditation: 11982 Page 1 of 48 Project: NPU, Oakdale CET # : 6110624 Sample ID Laboratory ID Matrix Collection Date/Time Receipt Date SAMPLE SUMMARY The sample(s) were received at 4.9 C. This report contains analytical data associated with following samples only. 52 5-6ft 6110624-01 Soil 11/22/201611/19/2016 53 2-5ft 6110624-02 Soil 11/22/201611/19/2016 54 1-5ft 6110624-03 Soil 11/22/201611/19/2016 55 1-4.5ft 6110624-04 Soil 11/22/201611/19/2016 56 5-7ft 6110624-05 Soil 11/22/201611/19/2016 57 1-5ft 6110624-06 Soil 11/22/201611/19/2016 58 4-7ft 6110624-07 Soil 11/22/201611/19/2016 60 4-7ft 6110624-08 Soil 11/22/201611/19/2016 61 0-3ft 6110624-09 Soil 11/22/201611/19/2016 62 0.5-2ft 6110624-10 Soil 11/22/201611/19/2016 43 4-6ft 6110624-11 Soil 11/22/201611/18/2016 44 4-6ft 6110624-12 Soil 11/22/201611/18/2016 45 0-3ft 6110624-13 Soil 11/22/201611/18/2016 46 1-3ft 6110624-14 Soil 11/22/201611/18/2016 47 4-6ft 6110624-15 Soil 11/22/201611/18/2016 48 4-6ft 6110624-16 Soil 11/22/201611/18/2016 43/44A 4-6ft 6110624-17 Soil 11/22/201611/18/2016 50 6ft 6110624-18 Soil 11/22/201612:0011/19/2016 51 5ft 6110624-19 Soil 11/22/201612:0011/19/2016 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 2 of 48 Project: NPU, Oakdale CET # : 6110624 Notes Date/Time AnalyzedPreparedBatchDilutionRLResultLaboratory ID Client Sample ID Units Analyst: ALM Matrix: Soil Analyte: Percent Solids [SM 2540 G] 77 11/29/2016 11/29/2016 09:146110624-01 %52 5-6ft 1.0 1 B6K2907 87 11/29/2016 11/29/2016 09:146110624-02 %53 2-5ft 1.0 1 B6K2907 87 11/29/2016 11/29/2016 09:146110624-03 %54 1-5ft 1.0 1 B6K2907 88 11/29/2016 11/29/2016 09:146110624-04 %55 1-4.5ft 1.0 1 B6K2907 76 11/29/2016 11/29/2016 09:146110624-05 %56 5-7ft 1.0 1 B6K2907 92 11/29/2016 11/29/2016 09:146110624-06 %57 1-5ft 1.0 1 B6K2907 77 11/29/2016 11/29/2016 09:146110624-07 %58 4-7ft 1.0 1 B6K2907 81 11/29/2016 11/29/2016 09:146110624-08 %60 4-7ft 1.0 1 B6K2907 85 11/29/2016 11/29/2016 09:146110624-09 %61 0-3ft 1.0 1 B6K2907 93 11/29/2016 11/29/2016 09:146110624-10 %62 0.5-2ft 1.0 1 B6K2907 75 11/29/2016 11/29/2016 09:146110624-11 %43 4-6ft 1.0 1 B6K2907 75 11/29/2016 11/29/2016 09:146110624-12 %44 4-6ft 1.0 1 B6K2907 82 11/29/2016 11/29/2016 09:146110624-13 %45 0-3ft 1.0 1 B6K2907 79 11/29/2016 11/29/2016 09:146110624-14 %46 1-3ft 1.0 1 B6K2907 77 11/29/2016 11/29/2016 09:146110624-15 %47 4-6ft 1.0 1 B6K2907 80 11/29/2016 11/29/2016 09:146110624-16 %48 4-6ft 1.0 1 B6K2907 76 11/29/2016 11/29/2016 09:146110624-17 %43/44A 4-6ft 1.0 1 B6K2907 76 11/29/2016 11/29/2016 09:146110624-18 %50 6ft 1.0 1 B6K2907 78 11/29/2016 11/29/2016 09:146110624-19 %51 5ft 1.0 1 B6K2907 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 3 of 48 Project: NPU, Oakdale CET # : 6110624 Client Sample ID 52 5-6ft Lab ID: 6110624-01 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6K2605 11/26/2016 11/27/2016 19:3266EPA 3550C *F1 Surrogate: Octacosane 56.1 %11/26/2016 11/27/2016 19:32B6K260550 - 150 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Dichlorodifluoromethane ND 2.11 B6K2842 11/28/2016 11/28/2016 19:4121EPA 5035A-L Chloromethane ND 2.11 B6K2842 11/28/2016 11/28/2016 19:4114EPA 5035A-L Vinyl Chloride ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L Bromomethane ND 2.11 B6K2842 11/28/2016 11/28/2016 19:4114EPA 5035A-L Chloroethane ND 2.11 B6K2842 11/28/2016 11/28/2016 19:4114EPA 5035A-L Trichlorofluoromethane ND 2.11 B6K2842 11/28/2016 11/28/2016 19:4155EPA 5035A-L Acetone ND 2.11 B6K2842 11/28/2016 11/28/2016 19:41210EPA 5035A-L Acrylonitrile ND 2.11 B6K2842 11/28/2016 11/28/2016 19:4111EPA 5035A-L Trichlorotrifluoroethane ND 2.11 B6K2842 11/28/2016 11/28/2016 19:4155EPA 5035A-L 1,1-Dichloroethene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L Methylene Chloride ND 2.11 B6K2842 11/28/2016 11/28/2016 19:4169EPA 5035A-L *F1*C1 Carbon Disulfide ND 2.11 B6K2842 11/28/2016 11/28/2016 19:4114EPA 5035A-L Methyl-t-Butyl Ether (MTBE)ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L trans-1,2-Dichloroethene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L 1,1-Dichloroethane ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L 2-Butanone (MEK)ND 2.11 B6K2842 11/28/2016 11/28/2016 19:4134EPA 5035A-L 2,2-Dichloropropane ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L cis-1,2-Dichloroethene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L Chloroform ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L Tetrahydrofuran ND 2.11 B6K2842 11/28/2016 11/28/2016 19:4134EPA 5035A-L *C2 1,1,1-Trichloroethane ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L Carbon Tetrachloride ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L 1,1-Dichloropropene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L Benzene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L 1,2-Dichloroethane ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L Trichloroethene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L 1,2-Dichloropropane ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 4 of 48 Project: NPU, Oakdale CET # : 6110624 Client Sample ID 52 5-6ft Lab ID: 6110624-01 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Dibromomethane ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L Bromodichloromethane ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L Methyl Isobutyl Ketone ND 2.11 B6K2842 11/28/2016 11/28/2016 19:4134EPA 5035A-L cis-1,3-Dichloropropene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L Toluene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L trans-1,3-Dichloropropene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L 2-Hexanone ND 2.11 B6K2842 11/28/2016 11/28/2016 19:4134EPA 5035A-L 1,1,2-Trichloroethane ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L Tetrachloroethene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L 1,3-Dichloropropane ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L Dibromochloromethane ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L 1,2-Dibromoethane ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L trans-1,4-Dichloro-2-Butene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:4134EPA 5035A-L Chlorobenzene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L 1,1,1,2-Tetrachloroethane ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L Ethylbenzene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L m+p Xylenes ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L o-Xylene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L Styrene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L Bromoform ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L Isopropylbenzene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L 1,1,2,2-Tetrachloroethane ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L Bromobenzene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L 1,2,3-Trichloropropane ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L n-Propylbenzene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L 2-Chlorotoluene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L 4-Chlorotoluene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L 1,3,5-Trimethylbenzene 12 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L tert-Butylbenzene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L 1,2,4-Trimethylbenzene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L sec-Butylbenzene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L 1,3-Dichlorobenzene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L 4-Isopropyltoluene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L 1,4-Dichlorobenzene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L 1,2-Dichlorobenzene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L n-Butylbenzene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L 1,2-Dibromo-3-Chloropropane ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L 1,2,4-Trichlorobenzene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L Hexachlorobutadiene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 5 of 48 Project: NPU, Oakdale CET # : 6110624 Client Sample ID 52 5-6ft Lab ID: 6110624-01 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Naphthalene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L 1,2,3-Trichlorobenzene ND 2.11 B6K2842 11/28/2016 11/28/2016 19:416.9 EPA 5035A-L Surrogate: 1,2-Dichloroethane-d4 103 %11/28/2016 11/28/2016 19:41B6K284270 - 130 Surrogate: Toluene-d8 101 %11/28/2016 11/28/2016 19:41B6K284270 - 130 Surrogate: 4-Bromofluorobenzene 95.3 %11/28/2016 11/28/2016 19:41B6K284270 - 130 Client Sample ID 53 2-5ft Lab ID: 6110624-02 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6K2605 11/26/2016 11/27/2016 19:5557EPA 3550C *F1 Surrogate: Octacosane 66.9 %11/26/2016 11/27/2016 19:55B6K260550 - 150 Client Sample ID 54 1-5ft Lab ID: 6110624-03 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH 85 1 B6K2605 11/26/2016 11/28/2016 19:1357EPA 3550C 2*F1 Surrogate: Octacosane 99.2 %11/26/2016 11/28/2016 19:13B6K260550 - 150 2 C9-C28 Fuel Oil Range 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 6 of 48 Project: NPU, Oakdale CET # : 6110624 Client Sample ID 55 1-4.5ft Lab ID: 6110624-04 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH 510 1 B6K2606 11/26/2016 11/27/2016 19:4457EPA 3550C 2*F1 Surrogate: Octacosane 84.0 %11/26/2016 11/27/2016 19:44B6K260650 - 150 2 C9-C28 Fuel Oil Range Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Dichlorodifluoromethane ND 1.89 B6K2842 11/28/2016 11/28/2016 20:0316EPA 5035A-L Chloromethane ND 1.89 B6K2842 11/28/2016 11/28/2016 20:0311EPA 5035A-L Vinyl Chloride ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L Bromomethane ND 1.89 B6K2842 11/28/2016 11/28/2016 20:0311EPA 5035A-L Chloroethane ND 1.89 B6K2842 11/28/2016 11/28/2016 20:0311EPA 5035A-L Trichlorofluoromethane ND 1.89 B6K2842 11/28/2016 11/28/2016 20:0343EPA 5035A-L Acetone ND 1.89 B6K2842 11/28/2016 11/28/2016 20:03160EPA 5035A-L Acrylonitrile ND 1.89 B6K2842 11/28/2016 11/28/2016 20:038.6 EPA 5035A-L Trichlorotrifluoroethane ND 1.89 B6K2842 11/28/2016 11/28/2016 20:0343EPA 5035A-L 1,1-Dichloroethene ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L Methylene Chloride ND 1.89 B6K2842 11/28/2016 11/28/2016 20:0354EPA 5035A-L *F1*C1 Carbon Disulfide ND 1.89 B6K2842 11/28/2016 11/28/2016 20:0311EPA 5035A-L Methyl-t-Butyl Ether (MTBE)ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L trans-1,2-Dichloroethene ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L 1,1-Dichloroethane ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L 2-Butanone (MEK)ND 1.89 B6K2842 11/28/2016 11/28/2016 20:0327EPA 5035A-L 2,2-Dichloropropane ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L cis-1,2-Dichloroethene ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L Chloroform ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L Tetrahydrofuran ND 1.89 B6K2842 11/28/2016 11/28/2016 20:0327EPA 5035A-L *C2 1,1,1-Trichloroethane ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L Carbon Tetrachloride ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L 1,1-Dichloropropene ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L Benzene ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L 1,2-Dichloroethane ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L Trichloroethene ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L 1,2-Dichloropropane ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 7 of 48 Project: NPU, Oakdale CET # : 6110624 Client Sample ID 55 1-4.5ft Lab ID: 6110624-04 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Dibromomethane ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L Bromodichloromethane ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L Methyl Isobutyl Ketone ND 1.89 B6K2842 11/28/2016 11/28/2016 20:0327EPA 5035A-L cis-1,3-Dichloropropene ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L Toluene ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L trans-1,3-Dichloropropene ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L 2-Hexanone ND 1.89 B6K2842 11/28/2016 11/28/2016 20:0327EPA 5035A-L 1,1,2-Trichloroethane ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L Tetrachloroethene ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L 1,3-Dichloropropane ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L Dibromochloromethane ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L 1,2-Dibromoethane ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L trans-1,4-Dichloro-2-Butene ND 1.89 B6K2842 11/28/2016 11/28/2016 20:0327EPA 5035A-L Chlorobenzene ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L 1,1,1,2-Tetrachloroethane ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L Ethylbenzene 28 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L m+p Xylenes 140 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L o-Xylene 100 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L Styrene ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L Bromoform ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L Isopropylbenzene 8.4 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L 1,1,2,2-Tetrachloroethane ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L Bromobenzene ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L 1,2,3-Trichloropropane ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L n-Propylbenzene 56 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L 2-Chlorotoluene ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L 4-Chlorotoluene ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L 1,3,5-Trimethylbenzene 150 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L tert-Butylbenzene ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L 1,2,4-Trimethylbenzene 520 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L E sec-Butylbenzene 18 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L 1,3-Dichlorobenzene ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L 4-Isopropyltoluene 13 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L 1,4-Dichlorobenzene ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L 1,2-Dichlorobenzene ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L n-Butylbenzene 43 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L 1,2-Dibromo-3-Chloropropane ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L 1,2,4-Trichlorobenzene ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L Hexachlorobutadiene ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 8 of 48 Project: NPU, Oakdale CET # : 6110624 Client Sample ID 55 1-4.5ft Lab ID: 6110624-04 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Naphthalene 56 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L 1,2,3-Trichlorobenzene ND 1.89 B6K2842 11/28/2016 11/28/2016 20:035.4 EPA 5035A-L Surrogate: 1,2-Dichloroethane-d4 110 %11/28/2016 11/28/2016 20:03B6K284270 - 130 Surrogate: Toluene-d8 101 %11/28/2016 11/28/2016 20:03B6K284270 - 130 Surrogate: 4-Bromofluorobenzene 91.2 %11/28/2016 11/28/2016 20:03B6K284270 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 9 of 48 Project: NPU, Oakdale CET # : 6110624 Client Sample ID 55 1-4.5ft Lab ID: 6110624-04RE1(Dilution) Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Dichlorodifluoromethane ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20420EPA 5035A-H Chloromethane ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20280EPA 5035A-H Vinyl Chloride ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H Bromomethane ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20280EPA 5035A-H Chloroethane ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20280EPA 5035A-H Trichlorofluoromethane ND 49.75 B6K3045 11/30/2016 11/30/2016 14:201100EPA 5035A-H Acetone ND 49.75 B6K3045 11/30/2016 11/30/2016 14:204200EPA 5035A-H Acrylonitrile ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20230EPA 5035A-H Trichlorotrifluoroethane ND 49.75 B6K3045 11/30/2016 11/30/2016 14:201100EPA 5035A-H 1,1-Dichloroethene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H Methylene Chloride ND 49.75 B6K3045 11/30/2016 11/30/2016 14:201400EPA 5035A-H Carbon Disulfide ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20280EPA 5035A-H Methyl-t-Butyl Ether (MTBE)ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H trans-1,2-Dichloroethene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H 1,1-Dichloroethane ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H 2-Butanone (MEK)ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20710EPA 5035A-H *C2 2,2-Dichloropropane ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H cis-1,2-Dichloroethene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H Chloroform ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H Tetrahydrofuran ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20710EPA 5035A-H *C2 1,1,1-Trichloroethane ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H Carbon Tetrachloride ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H 1,1-Dichloropropene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H Benzene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H 1,2-Dichloroethane ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H Trichloroethene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H 1,2-Dichloropropane ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H Dibromomethane ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H Bromodichloromethane ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H Methyl Isobutyl Ketone ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20710EPA 5035A-H cis-1,3-Dichloropropene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H Toluene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H trans-1,3-Dichloropropene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H 2-Hexanone ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20710EPA 5035A-H *C2 1,1,2-Trichloroethane ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H Tetrachloroethene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H *C2 1,3-Dichloropropane ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H Dibromochloromethane ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H 1,2-Dibromoethane ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 10 of 48 Project: NPU, Oakdale CET # : 6110624 Client Sample ID 55 1-4.5ft Lab ID: 6110624-04RE1(Dilution) Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics trans-1,4-Dichloro-2-Butene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20710EPA 5035A-H Chlorobenzene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H 1,1,1,2-Tetrachloroethane ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H Ethylbenzene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H m+p Xylenes ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H o-Xylene 170 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H Styrene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H Bromoform ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H Isopropylbenzene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H 1,1,2,2-Tetrachloroethane ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H Bromobenzene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H 1,2,3-Trichloropropane ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H n-Propylbenzene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H 2-Chlorotoluene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H 4-Chlorotoluene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H 1,3,5-Trimethylbenzene 390 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H tert-Butylbenzene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H 1,2,4-Trimethylbenzene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H sec-Butylbenzene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H 1,3-Dichlorobenzene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H 4-Isopropyltoluene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H 1,4-Dichlorobenzene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H 1,2-Dichlorobenzene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H n-Butylbenzene 170 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H 1,2-Dibromo-3-Chloropropane ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H 1,2,4-Trichlorobenzene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H Hexachlorobutadiene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H Naphthalene 170 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H 1,2,3-Trichlorobenzene ND 49.75 B6K3045 11/30/2016 11/30/2016 14:20140EPA 5035A-H Surrogate: 1,2-Dichloroethane-d4 97.4 %11/30/2016 11/30/2016 14:20B6K304570 - 130 Surrogate: Toluene-d8 99.5 %11/30/2016 11/30/2016 14:20B6K304570 - 130 Surrogate: 4-Bromofluorobenzene 102 %11/30/2016 11/30/2016 14:20B6K304570 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 11 of 48 Project: NPU, Oakdale CET # : 6110624 Client Sample ID 56 5-7ft Lab ID: 6110624-05 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6K2606 11/26/2016 11/27/2016 20:0866EPA 3550C *F1 Surrogate: Octacosane 55.5 %11/26/2016 11/27/2016 20:08B6K260650 - 150 Client Sample ID 57 1-5ft Lab ID: 6110624-06 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6K2606 11/26/2016 11/27/2016 21:4354EPA 3550C *F1 Surrogate: Octacosane 80.2 %11/26/2016 11/27/2016 21:43B6K260650 - 150 Client Sample ID 58 4-7ft Lab ID: 6110624-07 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6K2606 11/26/2016 11/27/2016 22:0765EPA 3550C *F1 Surrogate: Octacosane 74.3 %11/26/2016 11/27/2016 22:07B6K260650 - 150 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 12 of 48 Project: NPU, Oakdale CET # : 6110624 Client Sample ID 60 4-7ft Lab ID: 6110624-08 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6K2606 11/26/2016 12/01/2016 10:4161EPA 3550C *F1 Surrogate: Octacosane 87.4 %11/26/2016 12/01/2016 10:41B6K260650 - 150 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Methyl-t-Butyl Ether (MTBE)ND 1.86 B6K2842 11/28/2016 11/28/2016 20:245.7 EPA 5035A-L Benzene ND 1.86 B6K2842 11/28/2016 11/28/2016 20:245.7 EPA 5035A-L Toluene ND 1.86 B6K2842 11/28/2016 11/28/2016 20:245.7 EPA 5035A-L Chlorobenzene ND 1.86 B6K2842 11/28/2016 11/28/2016 20:245.7 EPA 5035A-L Ethylbenzene ND 1.86 B6K2842 11/28/2016 11/28/2016 20:245.7 EPA 5035A-L m+p Xylenes ND 1.86 B6K2842 11/28/2016 11/28/2016 20:245.7 EPA 5035A-L o-Xylene ND 1.86 B6K2842 11/28/2016 11/28/2016 20:245.7 EPA 5035A-L Styrene ND 1.86 B6K2842 11/28/2016 11/28/2016 20:245.7 EPA 5035A-L Isopropylbenzene ND 1.86 B6K2842 11/28/2016 11/28/2016 20:245.7 EPA 5035A-L Bromobenzene ND 1.86 B6K2842 11/28/2016 11/28/2016 20:245.7 EPA 5035A-L n-Propylbenzene ND 1.86 B6K2842 11/28/2016 11/28/2016 20:245.7 EPA 5035A-L 2-Chlorotoluene ND 1.86 B6K2842 11/28/2016 11/28/2016 20:245.7 EPA 5035A-L 4-Chlorotoluene ND 1.86 B6K2842 11/28/2016 11/28/2016 20:245.7 EPA 5035A-L 1,3,5-Trimethylbenzene 6.4 1.86 B6K2842 11/28/2016 11/28/2016 20:245.7 EPA 5035A-L tert-Butylbenzene ND 1.86 B6K2842 11/28/2016 11/28/2016 20:245.7 EPA 5035A-L 1,2,4-Trimethylbenzene ND 1.86 B6K2842 11/28/2016 11/28/2016 20:245.7 EPA 5035A-L sec-Butylbenzene ND 1.86 B6K2842 11/28/2016 11/28/2016 20:245.7 EPA 5035A-L 1,3-Dichlorobenzene ND 1.86 B6K2842 11/28/2016 11/28/2016 20:245.7 EPA 5035A-L 4-Isopropyltoluene ND 1.86 B6K2842 11/28/2016 11/28/2016 20:245.7 EPA 5035A-L 1,4-Dichlorobenzene ND 1.86 B6K2842 11/28/2016 11/28/2016 20:245.7 EPA 5035A-L 1,2-Dichlorobenzene ND 1.86 B6K2842 11/28/2016 11/28/2016 20:245.7 EPA 5035A-L n-Butylbenzene ND 1.86 B6K2842 11/28/2016 11/28/2016 20:245.7 EPA 5035A-L 1,2,4-Trichlorobenzene ND 1.86 B6K2842 11/28/2016 11/28/2016 20:245.7 EPA 5035A-L Hexachlorobutadiene ND 1.86 B6K2842 11/28/2016 11/28/2016 20:245.7 EPA 5035A-L Naphthalene ND 1.86 B6K2842 11/28/2016 11/28/2016 20:245.7 EPA 5035A-L 1,2,3-Trichlorobenzene ND 1.86 B6K2842 11/28/2016 11/28/2016 20:245.7 EPA 5035A-L 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 13 of 48 Project: NPU, Oakdale CET # : 6110624 Client Sample ID 60 4-7ft Lab ID: 6110624-08 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg) Result (ug/kg)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Surrogate: 1,2-Dichloroethane-d4 110 %11/28/2016 11/28/2016 20:24B6K284270 - 130 Surrogate: Toluene-d8 101 %11/28/2016 11/28/2016 20:24B6K284270 - 130 Surrogate: 4-Bromofluorobenzene 93.2 %11/28/2016 11/28/2016 20:24B6K284270 - 130 Client Sample ID 61 0-3ft Lab ID: 6110624-09 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6K2606 11/26/2016 12/01/2016 09:5359EPA 3550C *F1 Surrogate: Octacosane 98.6 %11/26/2016 12/01/2016 09:53B6K260650 - 150 Client Sample ID 62 0.5-2ft Lab ID: 6110624-10 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6K2606 11/26/2016 12/01/2016 10:1754EPA 3550C *F1 Surrogate: Octacosane 93.0 %11/26/2016 12/01/2016 10:17B6K260650 - 150 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 14 of 48 Project: NPU, Oakdale CET # : 6110624 Client Sample ID 43 4-6ft Lab ID: 6110624-11 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH 4600 1 B6K2606 11/26/2016 11/27/2016 23:4267EPA 3550C 2*F1 Surrogate: Octacosane 82.6 %11/26/2016 11/27/2016 23:42B6K260650 - 150 2 C9-C28 Fuel Oil Range Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Dichlorodifluoromethane ND 2.27 B6K3044 11/30/2016 11/30/2016 12:4523EPA 5035A-L Chloromethane ND 2.27 B6K3044 11/30/2016 11/30/2016 12:4515EPA 5035A-L Vinyl Chloride ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L Bromomethane ND 2.27 B6K3044 11/30/2016 11/30/2016 12:4515EPA 5035A-L Chloroethane ND 2.27 B6K3044 11/30/2016 11/30/2016 12:4515EPA 5035A-L Trichlorofluoromethane ND 2.27 B6K3044 11/30/2016 11/30/2016 12:4561EPA 5035A-L Acetone ND 2.27 B6K3044 11/30/2016 11/30/2016 12:45230EPA 5035A-L Acrylonitrile ND 2.27 B6K3044 11/30/2016 11/30/2016 12:4512EPA 5035A-L Trichlorotrifluoroethane ND 2.27 B6K3044 11/30/2016 11/30/2016 12:4561EPA 5035A-L 1,1-Dichloroethene ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L Methylene Chloride ND 2.27 B6K3044 11/30/2016 11/30/2016 12:4576EPA 5035A-L Carbon Disulfide ND 2.27 B6K3044 11/30/2016 11/30/2016 12:4515EPA 5035A-L Methyl-t-Butyl Ether (MTBE)ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L trans-1,2-Dichloroethene ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L 1,1-Dichloroethane ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L 2-Butanone (MEK)ND 2.27 B6K3044 11/30/2016 11/30/2016 12:4538EPA 5035A-L *C2 2,2-Dichloropropane ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L cis-1,2-Dichloroethene ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L Chloroform ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L Tetrahydrofuran ND 2.27 B6K3044 11/30/2016 11/30/2016 12:4538EPA 5035A-L *C2 1,1,1-Trichloroethane ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L Carbon Tetrachloride ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L 1,1-Dichloropropene ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L Benzene ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L 1,2-Dichloroethane ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L Trichloroethene ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L 1,2-Dichloropropane ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 15 of 48 Project: NPU, Oakdale CET # : 6110624 Client Sample ID 43 4-6ft Lab ID: 6110624-11 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Dibromomethane ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L Bromodichloromethane ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L Methyl Isobutyl Ketone ND 2.27 B6K3044 11/30/2016 11/30/2016 12:4538EPA 5035A-L cis-1,3-Dichloropropene ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L Toluene ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L trans-1,3-Dichloropropene ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L 2-Hexanone ND 2.27 B6K3044 11/30/2016 11/30/2016 12:4538EPA 5035A-L *C2 1,1,2-Trichloroethane ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L Tetrachloroethene ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L *C2 1,3-Dichloropropane ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L Dibromochloromethane ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L 1,2-Dibromoethane ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L trans-1,4-Dichloro-2-Butene ND 2.27 B6K3044 11/30/2016 11/30/2016 12:4538EPA 5035A-L Chlorobenzene ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L 1,1,1,2-Tetrachloroethane ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L Ethylbenzene ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L m+p Xylenes 270 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L o-Xylene 1900 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L E Styrene ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L Bromoform ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L Isopropylbenzene 160 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L 1,1,2,2-Tetrachloroethane ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L Bromobenzene ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L 1,2,3-Trichloropropane ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L n-Propylbenzene 330 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L 2-Chlorotoluene ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L 4-Chlorotoluene ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L 1,3,5-Trimethylbenzene 3700 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L E tert-Butylbenzene ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L 1,2,4-Trimethylbenzene 890 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L E sec-Butylbenzene 650 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L E 1,3-Dichlorobenzene ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L 4-Isopropyltoluene 430 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L 1,4-Dichlorobenzene ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L 1,2-Dichlorobenzene ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L n-Butylbenzene 490 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L 1,2-Dibromo-3-Chloropropane ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L 1,2,4-Trichlorobenzene ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L Hexachlorobutadiene ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 16 of 48 Project: NPU, Oakdale CET # : 6110624 Client Sample ID 43 4-6ft Lab ID: 6110624-11 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Naphthalene ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L 1,2,3-Trichlorobenzene ND 2.27 B6K3044 11/30/2016 11/30/2016 12:457.6 EPA 5035A-L Surrogate: 1,2-Dichloroethane-d4 109 %11/30/2016 11/30/2016 12:45B6K304470 - 130 Surrogate: Toluene-d8 107 %11/30/2016 11/30/2016 12:45B6K304470 - 130 Surrogate: 4-Bromofluorobenzene 88.5 %11/30/2016 11/30/2016 12:45B6K304470 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 17 of 48 Project: NPU, Oakdale CET # : 6110624 Client Sample ID 43 4-6ft Lab ID: 6110624-11RE1(Dilution) Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Dichlorodifluoromethane ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16980EPA 5035A-H Chloromethane ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16650EPA 5035A-H Vinyl Chloride ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H Bromomethane ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16650EPA 5035A-H Chloroethane ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16650EPA 5035A-H Trichlorofluoromethane ND 97.75 B6K3045 11/30/2016 11/30/2016 15:162600EPA 5035A-H Acetone ND 97.75 B6K3045 11/30/2016 11/30/2016 15:169800EPA 5035A-H Acrylonitrile ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16520EPA 5035A-H Trichlorotrifluoroethane ND 97.75 B6K3045 11/30/2016 11/30/2016 15:162600EPA 5035A-H 1,1-Dichloroethene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H Methylene Chloride ND 97.75 B6K3045 11/30/2016 11/30/2016 15:163300EPA 5035A-H Carbon Disulfide ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16650EPA 5035A-H Methyl-t-Butyl Ether (MTBE)ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H trans-1,2-Dichloroethene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H 1,1-Dichloroethane ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H 2-Butanone (MEK)ND 97.75 B6K3045 11/30/2016 11/30/2016 15:161600EPA 5035A-H *C2 2,2-Dichloropropane ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H cis-1,2-Dichloroethene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H Chloroform ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H Tetrahydrofuran ND 97.75 B6K3045 11/30/2016 11/30/2016 15:161600EPA 5035A-H *C2 1,1,1-Trichloroethane ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H Carbon Tetrachloride ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H 1,1-Dichloropropene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H Benzene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H 1,2-Dichloroethane ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H Trichloroethene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H 1,2-Dichloropropane ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H Dibromomethane ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H Bromodichloromethane ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H Methyl Isobutyl Ketone ND 97.75 B6K3045 11/30/2016 11/30/2016 15:161600EPA 5035A-H cis-1,3-Dichloropropene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H Toluene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H trans-1,3-Dichloropropene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H 2-Hexanone ND 97.75 B6K3045 11/30/2016 11/30/2016 15:161600EPA 5035A-H *C2 1,1,2-Trichloroethane ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H Tetrachloroethene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H *C2 1,3-Dichloropropane ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H Dibromochloromethane ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H 1,2-Dibromoethane ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 18 of 48 Project: NPU, Oakdale CET # : 6110624 Client Sample ID 43 4-6ft Lab ID: 6110624-11RE1(Dilution) Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics trans-1,4-Dichloro-2-Butene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:161600EPA 5035A-H Chlorobenzene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H 1,1,1,2-Tetrachloroethane ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H Ethylbenzene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H m+p Xylenes ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H o-Xylene 7400 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H Styrene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H Bromoform ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H Isopropylbenzene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H 1,1,2,2-Tetrachloroethane ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H Bromobenzene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H 1,2,3-Trichloropropane ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H n-Propylbenzene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H 2-Chlorotoluene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H 4-Chlorotoluene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H 1,3,5-Trimethylbenzene 11000 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H tert-Butylbenzene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H 1,2,4-Trimethylbenzene 490 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H sec-Butylbenzene 1200 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H 1,3-Dichlorobenzene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H 4-Isopropyltoluene 1300 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H 1,4-Dichlorobenzene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H 1,2-Dichlorobenzene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H n-Butylbenzene 1500 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H 1,2-Dibromo-3-Chloropropane ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H 1,2,4-Trichlorobenzene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H Hexachlorobutadiene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H Naphthalene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H 1,2,3-Trichlorobenzene ND 97.75 B6K3045 11/30/2016 11/30/2016 15:16330EPA 5035A-H Surrogate: 1,2-Dichloroethane-d4 102 %11/30/2016 11/30/2016 15:16B6K304570 - 130 Surrogate: Toluene-d8 101 %11/30/2016 11/30/2016 15:16B6K304570 - 130 Surrogate: 4-Bromofluorobenzene 103 %11/30/2016 11/30/2016 15:16B6K304570 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 19 of 48 Project: NPU, Oakdale CET # : 6110624 Client Sample ID 44 4-6ft Lab ID: 6110624-12 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH 210 1 B6K2606 11/26/2016 11/28/2016 00:0667EPA 3550C 2*F1 Surrogate: Octacosane 80.1 %11/26/2016 11/28/2016 00:06B6K260650 - 150 2 C9-C28 Fuel Oil Range Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Dichlorodifluoromethane ND 1.87 B6K2842 11/28/2016 11/28/2016 20:4619EPA 5035A-L Chloromethane ND 1.87 B6K2842 11/28/2016 11/28/2016 20:4612EPA 5035A-L Vinyl Chloride ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L Bromomethane ND 1.87 B6K2842 11/28/2016 11/28/2016 20:4612EPA 5035A-L Chloroethane ND 1.87 B6K2842 11/28/2016 11/28/2016 20:4612EPA 5035A-L Trichlorofluoromethane ND 1.87 B6K2842 11/28/2016 11/28/2016 20:4650EPA 5035A-L Acetone ND 1.87 B6K2842 11/28/2016 11/28/2016 20:46190EPA 5035A-L Acrylonitrile ND 1.87 B6K2842 11/28/2016 11/28/2016 20:4610EPA 5035A-L Trichlorotrifluoroethane ND 1.87 B6K2842 11/28/2016 11/28/2016 20:4650EPA 5035A-L 1,1-Dichloroethene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L Methylene Chloride ND 1.87 B6K2842 11/28/2016 11/28/2016 20:4662EPA 5035A-L *F1*C1 Carbon Disulfide ND 1.87 B6K2842 11/28/2016 11/28/2016 20:4612EPA 5035A-L Methyl-t-Butyl Ether (MTBE)ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L trans-1,2-Dichloroethene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L 1,1-Dichloroethane ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L 2-Butanone (MEK)ND 1.87 B6K2842 11/28/2016 11/28/2016 20:4631EPA 5035A-L 2,2-Dichloropropane ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L cis-1,2-Dichloroethene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L Chloroform ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L Tetrahydrofuran ND 1.87 B6K2842 11/28/2016 11/28/2016 20:4631EPA 5035A-L *C2 1,1,1-Trichloroethane ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L Carbon Tetrachloride ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L 1,1-Dichloropropene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L Benzene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L 1,2-Dichloroethane ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L Trichloroethene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L 1,2-Dichloropropane ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 20 of 48 Project: NPU, Oakdale CET # : 6110624 Client Sample ID 44 4-6ft Lab ID: 6110624-12 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Dibromomethane ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L Bromodichloromethane ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L Methyl Isobutyl Ketone ND 1.87 B6K2842 11/28/2016 11/28/2016 20:4631EPA 5035A-L cis-1,3-Dichloropropene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L Toluene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L trans-1,3-Dichloropropene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L 2-Hexanone ND 1.87 B6K2842 11/28/2016 11/28/2016 20:4631EPA 5035A-L 1,1,2-Trichloroethane ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L Tetrachloroethene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L 1,3-Dichloropropane ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L Dibromochloromethane ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L 1,2-Dibromoethane ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L trans-1,4-Dichloro-2-Butene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:4631EPA 5035A-L Chlorobenzene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L 1,1,1,2-Tetrachloroethane ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L Ethylbenzene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L m+p Xylenes ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L o-Xylene 11 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L Styrene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L Bromoform ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L Isopropylbenzene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L 1,1,2,2-Tetrachloroethane ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L Bromobenzene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L 1,2,3-Trichloropropane ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L n-Propylbenzene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L 2-Chlorotoluene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L 4-Chlorotoluene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L 1,3,5-Trimethylbenzene 29 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L tert-Butylbenzene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L 1,2,4-Trimethylbenzene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L sec-Butylbenzene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L 1,3-Dichlorobenzene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L 4-Isopropyltoluene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L 1,4-Dichlorobenzene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L 1,2-Dichlorobenzene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L n-Butylbenzene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L 1,2-Dibromo-3-Chloropropane ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L 1,2,4-Trichlorobenzene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L Hexachlorobutadiene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 21 of 48 Project: NPU, Oakdale CET # : 6110624 Client Sample ID 44 4-6ft Lab ID: 6110624-12 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Naphthalene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L 1,2,3-Trichlorobenzene ND 1.87 B6K2842 11/28/2016 11/28/2016 20:466.2 EPA 5035A-L Surrogate: 1,2-Dichloroethane-d4 108 %11/28/2016 11/28/2016 20:46B6K284270 - 130 Surrogate: Toluene-d8 101 %11/28/2016 11/28/2016 20:46B6K284270 - 130 Surrogate: 4-Bromofluorobenzene 91.9 %11/28/2016 11/28/2016 20:46B6K284270 - 130 Client Sample ID 45 0-3ft Lab ID: 6110624-13 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6K2606 11/26/2016 12/01/2016 11:0461EPA 3550C *F1 Surrogate: Octacosane 91.8 %11/26/2016 12/01/2016 11:04B6K260650 - 150 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 22 of 48 Project: NPU, Oakdale CET # : 6110624 Client Sample ID 46 1-3ft Lab ID: 6110624-14 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6K2606 11/26/2016 11/28/2016 00:5463EPA 3550C *F1 Surrogate: Octacosane 73.5 %11/26/2016 11/28/2016 00:54B6K260650 - 150 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Methyl-t-Butyl Ether (MTBE)ND 1.92 B6K2842 11/28/2016 11/28/2016 21:086.1 EPA 5035A-L Benzene ND 1.92 B6K2842 11/28/2016 11/28/2016 21:086.1 EPA 5035A-L Toluene ND 1.92 B6K2842 11/28/2016 11/28/2016 21:086.1 EPA 5035A-L Chlorobenzene ND 1.92 B6K2842 11/28/2016 11/28/2016 21:086.1 EPA 5035A-L Ethylbenzene ND 1.92 B6K2842 11/28/2016 11/28/2016 21:086.1 EPA 5035A-L m+p Xylenes ND 1.92 B6K2842 11/28/2016 11/28/2016 21:086.1 EPA 5035A-L o-Xylene ND 1.92 B6K2842 11/28/2016 11/28/2016 21:086.1 EPA 5035A-L Styrene ND 1.92 B6K2842 11/28/2016 11/28/2016 21:086.1 EPA 5035A-L Isopropylbenzene ND 1.92 B6K2842 11/28/2016 11/28/2016 21:086.1 EPA 5035A-L Bromobenzene ND 1.92 B6K2842 11/28/2016 11/28/2016 21:086.1 EPA 5035A-L n-Propylbenzene ND 1.92 B6K2842 11/28/2016 11/28/2016 21:086.1 EPA 5035A-L 2-Chlorotoluene ND 1.92 B6K2842 11/28/2016 11/28/2016 21:086.1 EPA 5035A-L 4-Chlorotoluene ND 1.92 B6K2842 11/28/2016 11/28/2016 21:086.1 EPA 5035A-L 1,3,5-Trimethylbenzene ND 1.92 B6K2842 11/28/2016 11/28/2016 21:086.1 EPA 5035A-L tert-Butylbenzene ND 1.92 B6K2842 11/28/2016 11/28/2016 21:086.1 EPA 5035A-L 1,2,4-Trimethylbenzene ND 1.92 B6K2842 11/28/2016 11/28/2016 21:086.1 EPA 5035A-L sec-Butylbenzene ND 1.92 B6K2842 11/28/2016 11/28/2016 21:086.1 EPA 5035A-L 1,3-Dichlorobenzene ND 1.92 B6K2842 11/28/2016 11/28/2016 21:086.1 EPA 5035A-L 4-Isopropyltoluene ND 1.92 B6K2842 11/28/2016 11/28/2016 21:086.1 EPA 5035A-L 1,4-Dichlorobenzene ND 1.92 B6K2842 11/28/2016 11/28/2016 21:086.1 EPA 5035A-L 1,2-Dichlorobenzene ND 1.92 B6K2842 11/28/2016 11/28/2016 21:086.1 EPA 5035A-L n-Butylbenzene ND 1.92 B6K2842 11/28/2016 11/28/2016 21:086.1 EPA 5035A-L 1,2,4-Trichlorobenzene ND 1.92 B6K2842 11/28/2016 11/28/2016 21:086.1 EPA 5035A-L Hexachlorobutadiene ND 1.92 B6K2842 11/28/2016 11/28/2016 21:086.1 EPA 5035A-L Naphthalene ND 1.92 B6K2842 11/28/2016 11/28/2016 21:086.1 EPA 5035A-L 1,2,3-Trichlorobenzene ND 1.92 B6K2842 11/28/2016 11/28/2016 21:086.1 EPA 5035A-L 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 23 of 48 Project: NPU, Oakdale CET # : 6110624 Client Sample ID 46 1-3ft Lab ID: 6110624-14 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg) Result (ug/kg)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Surrogate: 1,2-Dichloroethane-d4 108 %11/28/2016 11/28/2016 21:08B6K284270 - 130 Surrogate: Toluene-d8 101 %11/28/2016 11/28/2016 21:08B6K284270 - 130 Surrogate: 4-Bromofluorobenzene 92.8 %11/28/2016 11/28/2016 21:08B6K284270 - 130 Client Sample ID 47 4-6ft Lab ID: 6110624-15 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6K2606 11/26/2016 11/28/2016 01:1865EPA 3550C *F1 Surrogate: Octacosane 76.7 %11/26/2016 11/28/2016 01:18B6K260650 - 150 Client Sample ID 48 4-6ft Lab ID: 6110624-16 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6K2606 11/26/2016 11/28/2016 01:4163EPA 3550C *F1 Surrogate: Octacosane 77.4 %11/26/2016 11/28/2016 01:41B6K260650 - 150 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 24 of 48 Project: NPU, Oakdale CET # : 6110624 Client Sample ID 43/44A 4-6ft Lab ID: 6110624-17 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH 4300 1 B6K2606 11/26/2016 12/01/2016 11:2865EPA 3550C 2*F1 Surrogate: Octacosane 92.4 %11/26/2016 12/01/2016 11:28B6K260650 - 150 2 C9-C28 Fuel Oil Range 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 25 of 48 Project: NPU, Oakdale CET # : 6110624 Client Sample ID 50 6ft Lab ID: 6110624-18 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6K2606 11/26/2016 11/28/2016 02:2966EPA 3550C *F1 Surrogate: Octacosane 77.8 %11/26/2016 11/28/2016 02:29B6K260650 - 150 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Methyl-t-Butyl Ether (MTBE)ND 1.97 B6K2842 11/28/2016 11/28/2016 21:296.5 EPA 5035A-L Benzene ND 1.97 B6K2842 11/28/2016 11/28/2016 21:296.5 EPA 5035A-L Toluene ND 1.97 B6K2842 11/28/2016 11/28/2016 21:296.5 EPA 5035A-L Chlorobenzene ND 1.97 B6K2842 11/28/2016 11/28/2016 21:296.5 EPA 5035A-L Ethylbenzene ND 1.97 B6K2842 11/28/2016 11/28/2016 21:296.5 EPA 5035A-L m+p Xylenes 8.7 1.97 B6K2842 11/28/2016 11/28/2016 21:296.5 EPA 5035A-L o-Xylene 21 1.97 B6K2842 11/28/2016 11/28/2016 21:296.5 EPA 5035A-L Styrene ND 1.97 B6K2842 11/28/2016 11/28/2016 21:296.5 EPA 5035A-L Isopropylbenzene ND 1.97 B6K2842 11/28/2016 11/28/2016 21:296.5 EPA 5035A-L Bromobenzene ND 1.97 B6K2842 11/28/2016 11/28/2016 21:296.5 EPA 5035A-L n-Propylbenzene ND 1.97 B6K2842 11/28/2016 11/28/2016 21:296.5 EPA 5035A-L 2-Chlorotoluene ND 1.97 B6K2842 11/28/2016 11/28/2016 21:296.5 EPA 5035A-L 4-Chlorotoluene ND 1.97 B6K2842 11/28/2016 11/28/2016 21:296.5 EPA 5035A-L 1,3,5-Trimethylbenzene 56 1.97 B6K2842 11/28/2016 11/28/2016 21:296.5 EPA 5035A-L tert-Butylbenzene ND 1.97 B6K2842 11/28/2016 11/28/2016 21:296.5 EPA 5035A-L 1,2,4-Trimethylbenzene ND 1.97 B6K2842 11/28/2016 11/28/2016 21:296.5 EPA 5035A-L sec-Butylbenzene ND 1.97 B6K2842 11/28/2016 11/28/2016 21:296.5 EPA 5035A-L 1,3-Dichlorobenzene ND 1.97 B6K2842 11/28/2016 11/28/2016 21:296.5 EPA 5035A-L 4-Isopropyltoluene ND 1.97 B6K2842 11/28/2016 11/28/2016 21:296.5 EPA 5035A-L 1,4-Dichlorobenzene ND 1.97 B6K2842 11/28/2016 11/28/2016 21:296.5 EPA 5035A-L 1,2-Dichlorobenzene ND 1.97 B6K2842 11/28/2016 11/28/2016 21:296.5 EPA 5035A-L n-Butylbenzene ND 1.97 B6K2842 11/28/2016 11/28/2016 21:296.5 EPA 5035A-L 1,2,4-Trichlorobenzene ND 1.97 B6K2842 11/28/2016 11/28/2016 21:296.5 EPA 5035A-L Hexachlorobutadiene ND 1.97 B6K2842 11/28/2016 11/28/2016 21:296.5 EPA 5035A-L Naphthalene ND 1.97 B6K2842 11/28/2016 11/28/2016 21:296.5 EPA 5035A-L 1,2,3-Trichlorobenzene ND 1.97 B6K2842 11/28/2016 11/28/2016 21:296.5 EPA 5035A-L 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 26 of 48 Project: NPU, Oakdale CET # : 6110624 Client Sample ID 50 6ft Lab ID: 6110624-18 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg) Result (ug/kg)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Surrogate: 1,2-Dichloroethane-d4 109 %11/28/2016 11/28/2016 21:29B6K284270 - 130 Surrogate: Toluene-d8 101 %11/28/2016 11/28/2016 21:29B6K284270 - 130 Surrogate: 4-Bromofluorobenzene 93.9 %11/28/2016 11/28/2016 21:29B6K284270 - 130 Client Sample ID 51 5ft Lab ID: 6110624-19 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH 130 1 B6K2606 11/26/2016 11/28/2016 02:5264EPA 3550C 2*F1 Surrogate: Octacosane 77.4 %11/26/2016 11/28/2016 02:52B6K260650 - 150 2 C9-C28 Fuel Oil Range 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 27 of 48 Project: NPU, Oakdale CET # : 6110624 QUALITY CONTROL SECTION Batch B6K2605 - CT-ETPH Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(mg/kg) (mg/kg)Notes Blank (B6K2605-BLK1)Prepared: 11/26/2016 Analyzed: 11/27/2016 ETPH 50ND 81.5 50 - 150Surrogate: Octacosane LCS (B6K2605-BS1)Prepared: 11/26/2016 Analyzed: 11/27/2016 ETPH 50 60 - 1201190 L 69.3 50 - 150Surrogate: Octacosane 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 28 of 48 Project: NPU, Oakdale CET # : 6110624 Batch B6K2606 - CT-ETPH Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(mg/kg) (mg/kg)Notes Blank (B6K2606-BLK1)Prepared: 11/26/2016 Analyzed: 11/27/2016 ETPH 50ND 84.2 50 - 150Surrogate: Octacosane LCS (B6K2606-BS1)Prepared: 11/26/2016 Analyzed: 11/27/2016 ETPH 50 60 - 1201220 L 84.7 50 - 150Surrogate: Octacosane Duplicate (B6K2606-DUP1)Source: 6110624-05 Prepared: 11/26/2016 Analyzed: 11/27/2016 ETPH 66 ND 30ND 83.5 50 - 150Surrogate: Octacosane Matrix Spike (B6K2606-MS1)Source: 6110624-05 Prepared: 11/26/2016 Analyzed: 11/27/2016 ETPH 66 ND 50 - 1501690 L 55.9 50 - 150Surrogate: Octacosane Matrix Spike Dup (B6K2606-MSD1)Source: 6110624-05 Prepared: 11/26/2016 Analyzed: 11/27/2016 ETPH 66 ND 50 - 150 0.105 301690 L 80.8 50 - 150Surrogate: Octacosane 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 29 of 48 Project: NPU, Oakdale CET # : 6110624 Batch B6K2842 - EPA 8260C Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes Blank (B6K2842-BLK1)Prepared: 11/28/2016 Analyzed: 11/28/2016 Dichlorodifluoromethane 7.5ND Chloromethane 5.0ND Vinyl Chloride 2.5ND Bromomethane 5.0ND Chloroethane 5.0ND Trichlorofluoromethane 20ND Acetone 75ND Acrylonitrile 4.0ND Trichlorotrifluoroethane 20ND 1,1-Dichloroethene 2.5ND Methylene Chloride 25ND Carbon Disulfide 5.0ND Methyl-t-Butyl Ether (MTBE)2.5ND trans-1,2-Dichloroethene 2.5ND 1,1-Dichloroethane 2.5ND 2-Butanone (MEK)13ND 2,2-Dichloropropane 2.5ND cis-1,2-Dichloroethene 2.5ND Chloroform 2.5ND Tetrahydrofuran 13ND 1,1,1-Trichloroethane 2.5ND Carbon Tetrachloride 2.5ND 1,1-Dichloropropene 2.5ND Benzene 2.5ND 1,2-Dichloroethane 2.5ND Trichloroethene 2.5ND 1,2-Dichloropropane 2.5ND Dibromomethane 2.5ND Bromodichloromethane 2.5ND Methyl Isobutyl Ketone 13ND cis-1,3-Dichloropropene 2.5ND Toluene 2.5ND trans-1,3-Dichloropropene 2.5ND 2-Hexanone 13ND 1,1,2-Trichloroethane 2.5ND Tetrachloroethene 2.5ND 1,3-Dichloropropane 2.5ND Dibromochloromethane 2.5ND 1,2-Dibromoethane 2.5ND trans-1,4-Dichloro-2-Butene 13ND Chlorobenzene 2.5ND 1,1,1,2-Tetrachloroethane 2.5ND Ethylbenzene 2.5ND m+p Xylenes 2.5ND o-Xylene 2.5ND Styrene 2.5ND Bromoform 2.5ND Isopropylbenzene 2.5ND 1,1,2,2-Tetrachloroethane 2.5ND Bromobenzene 2.5ND 1,2,3-Trichloropropane 2.5ND n-Propylbenzene 2.5ND 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 30 of 48 Project: NPU, Oakdale CET # : 6110624 Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes Blank (B6K2842-BLK1) - Continued Prepared: 11/28/2016 Analyzed: 11/28/2016 2-Chlorotoluene 2.5ND 4-Chlorotoluene 2.5ND 1,3,5-Trimethylbenzene 2.5ND tert-Butylbenzene 2.5ND 1,2,4-Trimethylbenzene 2.5ND sec-Butylbenzene 2.5ND 1,3-Dichlorobenzene 2.5ND 4-Isopropyltoluene 2.5ND 1,4-Dichlorobenzene 2.5ND 1,2-Dichlorobenzene 2.5ND n-Butylbenzene 2.5ND 1,2-Dibromo-3-Chloropropane 2.5ND 1,2,4-Trichlorobenzene 2.5ND Hexachlorobutadiene 2.5ND Naphthalene 2.5ND 1,2,3-Trichlorobenzene 2.5ND 99.6 70 - 130Surrogate: 1,2-Dichloroethane-d4 95.3 70 - 130Surrogate: Toluene-d8 111 70 - 130Surrogate: 4-Bromofluorobenzene LCS (B6K2842-BS1)Prepared: 11/28/2016 Analyzed: 11/28/2016 Dichlorodifluoromethane 7.5 92.4 70 - 13046.2 50.000 Chloromethane 5.0 91.0 70 - 13045.5 50.000 Vinyl Chloride 2.5 91.8 70 - 13045.9 50.000 Bromomethane 5.0 104 70 - 13052.1 50.000 Chloroethane 5.0 93.6 70 - 13046.8 50.000 Trichlorofluoromethane 20 93.3 70 - 13046.7 50.000 Acetone 75 85.4 70 - 13085.4 100.000 Acrylonitrile 4.0 97.8 70 - 13048.9 50.000 Trichlorotrifluoroethane 20 97.8 70 - 13048.9 50.000 1,1-Dichloroethene 2.5 97.7 70 - 13048.8 50.000 Methylene Chloride 25 65.3 70 - 13032.7 L 50.000 Carbon Disulfide 5.0 102 70 - 13050.8 50.000 Methyl-t-Butyl Ether (MTBE)2.5 96.3 70 - 13048.1 50.000 trans-1,2-Dichloroethene 2.5 96.8 70 - 13048.4 50.000 1,1-Dichloroethane 2.5 98.3 70 - 13049.1 50.000 2-Butanone (MEK)13 99.7 70 - 13099.7 100.000 2,2-Dichloropropane 2.5 102 70 - 13051.1 50.000 cis-1,2-Dichloroethene 2.5 96.6 70 - 13048.3 50.000 Chloroform 2.5 97.6 70 - 13048.8 50.000 Tetrahydrofuran 13 94.8 70 - 13047.4 50.000 1,1,1-Trichloroethane 2.5 101 70 - 13050.3 50.000 Carbon Tetrachloride 2.5 102 70 - 13051.0 50.000 1,1-Dichloropropene 2.5 98.7 70 - 13049.4 50.000 Benzene 2.5 97.4 70 - 13048.7 50.000 1,2-Dichloroethane 2.5 94.4 70 - 13047.2 50.000 Trichloroethene 2.5 98.4 70 - 13049.2 50.000 1,2-Dichloropropane 2.5 96.7 70 - 13048.3 50.000 Dibromomethane 2.5 99.0 70 - 13049.5 50.000 Bromodichloromethane 2.5 99.8 70 - 13049.9 50.000 Methyl Isobutyl Ketone 13 100 70 - 130100 100.000 cis-1,3-Dichloropropene 2.5 101 70 - 13050.5 50.000 Toluene 2.5 94.3 70 - 13047.1 50.000 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 31 of 48 Project: NPU, Oakdale CET # : 6110624 Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes LCS (B6K2842-BS1) - Continued Prepared: 11/28/2016 Analyzed: 11/28/2016 trans-1,3-Dichloropropene 2.5 101 70 - 13050.3 50.000 2-Hexanone 13 97.1 70 - 13097.1 100.000 1,1,2-Trichloroethane 2.5 97.7 70 - 13048.9 50.000 Tetrachloroethene 2.5 92.2 70 - 13046.1 50.000 1,3-Dichloropropane 2.5 95.8 70 - 13047.9 50.000 Dibromochloromethane 2.5 102 70 - 13050.8 50.000 1,2-Dibromoethane 2.5 96.8 70 - 13048.4 50.000 trans-1,4-Dichloro-2-Butene 13 97.3 70 - 13048.6 50.000 Chlorobenzene 2.5 96.7 70 - 13048.3 50.000 1,1,1,2-Tetrachloroethane 2.5 99.7 70 - 13049.8 50.000 Ethylbenzene 2.5 98.1 70 - 13049.0 50.000 m+p Xylenes 2.5 97.8 70 - 13097.8 100.000 o-Xylene 2.5 98.1 70 - 13049.0 50.000 Styrene 2.5 97.1 70 - 13048.6 50.000 Bromoform 2.5 97.0 70 - 13048.5 50.000 Isopropylbenzene 2.5 98.8 70 - 13049.4 50.000 1,1,2,2-Tetrachloroethane 2.5 96.4 70 - 13048.2 50.000 Bromobenzene 2.5 101 70 - 13050.4 50.000 1,2,3-Trichloropropane 2.5 97.3 70 - 13048.6 50.000 n-Propylbenzene 2.5 103 70 - 13051.3 50.000 2-Chlorotoluene 2.5 102 70 - 13050.9 50.000 4-Chlorotoluene 2.5 101 70 - 13050.5 50.000 1,3,5-Trimethylbenzene 2.5 101 70 - 13050.5 50.000 tert-Butylbenzene 2.5 103 70 - 13051.3 50.000 1,2,4-Trimethylbenzene 2.5 101 70 - 13050.3 50.000 sec-Butylbenzene 2.5 105 70 - 13052.6 50.000 1,3-Dichlorobenzene 2.5 94.0 70 - 13047.0 50.000 4-Isopropyltoluene 2.5 101 70 - 13050.7 50.000 1,4-Dichlorobenzene 2.5 97.2 70 - 13048.6 50.000 1,2-Dichlorobenzene 2.5 102 70 - 13051.1 50.000 n-Butylbenzene 2.5 102 70 - 13051.2 50.000 1,2-Dibromo-3-Chloropropane 2.5 103 70 - 13051.3 50.000 1,2,4-Trichlorobenzene 2.5 98.0 70 - 13049.0 50.000 Hexachlorobutadiene 2.5 99.0 70 - 13049.5 50.000 Naphthalene 2.5 101 70 - 13050.4 50.000 1,2,3-Trichlorobenzene 2.5 101 70 - 13050.3 50.000 102 70 - 130Surrogate: 1,2-Dichloroethane-d4 99.5 70 - 130Surrogate: Toluene-d8 97.5 70 - 130Surrogate: 4-Bromofluorobenzene 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 32 of 48 Project: NPU, Oakdale CET # : 6110624 Batch B6K3044 - EPA 8260C Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes Blank (B6K3044-BLK1)Prepared: 11/30/2016 Analyzed: 11/30/2016 Dichlorodifluoromethane 7.5ND Chloromethane 5.0ND Vinyl Chloride 2.5ND Bromomethane 5.0ND Chloroethane 5.0ND Trichlorofluoromethane 20ND Acetone 75ND Acrylonitrile 4.0ND Trichlorotrifluoroethane 20ND 1,1-Dichloroethene 2.5ND Methylene Chloride 25ND Carbon Disulfide 5.0ND Methyl-t-Butyl Ether (MTBE)2.5ND trans-1,2-Dichloroethene 2.5ND 1,1-Dichloroethane 2.5ND 2-Butanone (MEK)13ND 2,2-Dichloropropane 2.5ND cis-1,2-Dichloroethene 2.5ND Chloroform 2.5ND Tetrahydrofuran 13ND 1,1,1-Trichloroethane 2.5ND Carbon Tetrachloride 2.5ND 1,1-Dichloropropene 2.5ND Benzene 2.5ND 1,2-Dichloroethane 2.5ND Trichloroethene 2.5ND 1,2-Dichloropropane 2.5ND Dibromomethane 2.5ND Bromodichloromethane 2.5ND Methyl Isobutyl Ketone 13ND cis-1,3-Dichloropropene 2.5ND Toluene 2.5ND trans-1,3-Dichloropropene 2.5ND 2-Hexanone 13ND 1,1,2-Trichloroethane 2.5ND Tetrachloroethene 2.5ND 1,3-Dichloropropane 2.5ND Dibromochloromethane 2.5ND 1,2-Dibromoethane 2.5ND trans-1,4-Dichloro-2-Butene 13ND Chlorobenzene 2.5ND 1,1,1,2-Tetrachloroethane 2.5ND Ethylbenzene 2.5ND m+p Xylenes 2.5ND o-Xylene 2.5ND Styrene 2.5ND Bromoform 2.5ND Isopropylbenzene 2.5ND 1,1,2,2-Tetrachloroethane 2.5ND Bromobenzene 2.5ND 1,2,3-Trichloropropane 2.5ND n-Propylbenzene 2.5ND 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 33 of 48 Project: NPU, Oakdale CET # : 6110624 Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes Blank (B6K3044-BLK1) - Continued Prepared: 11/30/2016 Analyzed: 11/30/2016 2-Chlorotoluene 2.5ND 4-Chlorotoluene 2.5ND 1,3,5-Trimethylbenzene 2.5ND tert-Butylbenzene 2.5ND 1,2,4-Trimethylbenzene 2.5ND sec-Butylbenzene 2.5ND 1,3-Dichlorobenzene 2.5ND 4-Isopropyltoluene 2.5ND 1,4-Dichlorobenzene 2.5ND 1,2-Dichlorobenzene 2.5ND n-Butylbenzene 2.5ND 1,2-Dibromo-3-Chloropropane 2.5ND 1,2,4-Trichlorobenzene 2.5ND Hexachlorobutadiene 2.5ND Naphthalene 2.5ND 1,2,3-Trichlorobenzene 2.5ND 106 70 - 130Surrogate: 1,2-Dichloroethane-d4 101 70 - 130Surrogate: Toluene-d8 100 70 - 130Surrogate: 4-Bromofluorobenzene LCS (B6K3044-BS1)Prepared: 11/30/2016 Analyzed: 11/30/2016 Dichlorodifluoromethane 7.5 110 70 - 13055.0 50.000 Chloromethane 5.0 99.3 70 - 13049.7 50.000 Vinyl Chloride 2.5 98.5 70 - 13049.3 50.000 Bromomethane 5.0 108 70 - 13054.1 50.000 Chloroethane 5.0 94.8 70 - 13047.4 50.000 Trichlorofluoromethane 20 90.1 70 - 13045.0 50.000 Acetone 75 90.5 70 - 13090.5 100.000 Acrylonitrile 4.0 105 70 - 13052.3 50.000 Trichlorotrifluoroethane 20 83.9 70 - 13042.0 50.000 1,1-Dichloroethene 2.5 83.6 70 - 13041.8 50.000 Methylene Chloride 25 77.8 70 - 13038.9 50.000 Carbon Disulfide 5.0 90.9 70 - 13045.4 50.000 Methyl-t-Butyl Ether (MTBE)2.5 91.0 70 - 13045.5 50.000 trans-1,2-Dichloroethene 2.5 88.3 70 - 13044.2 50.000 1,1-Dichloroethane 2.5 89.3 70 - 13044.7 50.000 2-Butanone (MEK)13 101 70 - 130101 100.000 2,2-Dichloropropane 2.5 84.6 70 - 13042.3 50.000 cis-1,2-Dichloroethene 2.5 90.4 70 - 13045.2 50.000 Chloroform 2.5 90.3 70 - 13045.1 50.000 Tetrahydrofuran 13 101 70 - 13050.5 50.000 1,1,1-Trichloroethane 2.5 84.1 70 - 13042.0 50.000 Carbon Tetrachloride 2.5 77.5 70 - 13038.8 50.000 1,1-Dichloropropene 2.5 83.5 70 - 13041.7 50.000 Benzene 2.5 87.9 70 - 13044.0 50.000 1,2-Dichloroethane 2.5 96.3 70 - 13048.2 50.000 Trichloroethene 2.5 84.9 70 - 13042.5 50.000 1,2-Dichloropropane 2.5 92.1 70 - 13046.1 50.000 Dibromomethane 2.5 95.0 70 - 13047.5 50.000 Bromodichloromethane 2.5 93.0 70 - 13046.5 50.000 Methyl Isobutyl Ketone 13 101 70 - 130101 100.000 cis-1,3-Dichloropropene 2.5 93.7 70 - 13046.8 50.000 Toluene 2.5 85.9 70 - 13042.9 50.000 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 34 of 48 Project: NPU, Oakdale CET # : 6110624 Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes LCS (B6K3044-BS1) - Continued Prepared: 11/30/2016 Analyzed: 11/30/2016 trans-1,3-Dichloropropene 2.5 95.0 70 - 13047.5 50.000 2-Hexanone 13 102 70 - 130102 100.000 1,1,2-Trichloroethane 2.5 95.9 70 - 13047.9 50.000 Tetrachloroethene 2.5 78.2 70 - 13039.1 50.000 1,3-Dichloropropane 2.5 96.5 70 - 13048.3 50.000 Dibromochloromethane 2.5 97.5 70 - 13048.7 50.000 1,2-Dibromoethane 2.5 97.7 70 - 13048.9 50.000 trans-1,4-Dichloro-2-Butene 13 102 70 - 13050.8 50.000 Chlorobenzene 2.5 88.0 70 - 13044.0 50.000 1,1,1,2-Tetrachloroethane 2.5 92.4 70 - 13046.2 50.000 Ethylbenzene 2.5 85.2 70 - 13042.6 50.000 m+p Xylenes 2.5 85.4 70 - 13085.4 100.000 o-Xylene 2.5 87.8 70 - 13043.9 50.000 Styrene 2.5 92.1 70 - 13046.1 50.000 Bromoform 2.5 98.5 70 - 13049.2 50.000 Isopropylbenzene 2.5 85.3 70 - 13042.6 50.000 1,1,2,2-Tetrachloroethane 2.5 102 70 - 13050.9 50.000 Bromobenzene 2.5 94.0 70 - 13047.0 50.000 1,2,3-Trichloropropane 2.5 103 70 - 13051.3 50.000 n-Propylbenzene 2.5 88.7 70 - 13044.4 50.000 2-Chlorotoluene 2.5 91.1 70 - 13045.6 50.000 4-Chlorotoluene 2.5 93.0 70 - 13046.5 50.000 1,3,5-Trimethylbenzene 2.5 89.0 70 - 13044.5 50.000 tert-Butylbenzene 2.5 86.0 70 - 13043.0 50.000 1,2,4-Trimethylbenzene 2.5 91.0 70 - 13045.5 50.000 sec-Butylbenzene 2.5 88.0 70 - 13044.0 50.000 1,3-Dichlorobenzene 2.5 93.0 70 - 13046.5 50.000 4-Isopropyltoluene 2.5 88.8 70 - 13044.4 50.000 1,4-Dichlorobenzene 2.5 93.3 70 - 13046.7 50.000 1,2-Dichlorobenzene 2.5 96.9 70 - 13048.5 50.000 n-Butylbenzene 2.5 91.6 70 - 13045.8 50.000 1,2-Dibromo-3-Chloropropane 2.5 102 70 - 13051.2 50.000 1,2,4-Trichlorobenzene 2.5 95.3 70 - 13047.6 50.000 Hexachlorobutadiene 2.5 86.5 70 - 13043.3 50.000 Naphthalene 2.5 102 70 - 13051.0 50.000 1,2,3-Trichlorobenzene 2.5 97.8 70 - 13048.9 50.000 105 70 - 130Surrogate: 1,2-Dichloroethane-d4 101 70 - 130Surrogate: Toluene-d8 99.4 70 - 130Surrogate: 4-Bromofluorobenzene 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 35 of 48 Project: NPU, Oakdale CET # : 6110624 Batch B6K3045 - EPA 8260C Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes Blank (B6K3045-BLK1)Prepared: 11/30/2016 Analyzed: 11/30/2016 Dichlorodifluoromethane 7.5ND Chloromethane 5.0ND Vinyl Chloride 2.5ND Bromomethane 5.0ND Chloroethane 5.0ND Trichlorofluoromethane 20ND Acetone 75ND Acrylonitrile 4.0ND Trichlorotrifluoroethane 20ND 1,1-Dichloroethene 2.5ND Methylene Chloride 25ND Carbon Disulfide 5.0ND Methyl-t-Butyl Ether (MTBE)2.5ND trans-1,2-Dichloroethene 2.5ND 1,1-Dichloroethane 2.5ND 2-Butanone (MEK)13ND 2,2-Dichloropropane 2.5ND cis-1,2-Dichloroethene 2.5ND Chloroform 2.5ND Tetrahydrofuran 13ND 1,1,1-Trichloroethane 2.5ND Carbon Tetrachloride 2.5ND 1,1-Dichloropropene 2.5ND Benzene 2.5ND 1,2-Dichloroethane 2.5ND Trichloroethene 2.5ND 1,2-Dichloropropane 2.5ND Dibromomethane 2.5ND Bromodichloromethane 2.5ND Methyl Isobutyl Ketone 13ND cis-1,3-Dichloropropene 2.5ND Toluene 2.5ND trans-1,3-Dichloropropene 2.5ND 2-Hexanone 13ND 1,1,2-Trichloroethane 2.5ND Tetrachloroethene 2.5ND 1,3-Dichloropropane 2.5ND Dibromochloromethane 2.5ND 1,2-Dibromoethane 2.5ND trans-1,4-Dichloro-2-Butene 13ND Chlorobenzene 2.5ND 1,1,1,2-Tetrachloroethane 2.5ND Ethylbenzene 2.5ND m+p Xylenes 2.5ND o-Xylene 2.5ND Styrene 2.5ND Bromoform 2.5ND Isopropylbenzene 2.5ND 1,1,2,2-Tetrachloroethane 2.5ND Bromobenzene 2.5ND 1,2,3-Trichloropropane 2.5ND n-Propylbenzene 2.5ND 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 36 of 48 Project: NPU, Oakdale CET # : 6110624 Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes Blank (B6K3045-BLK1) - Continued Prepared: 11/30/2016 Analyzed: 11/30/2016 2-Chlorotoluene 2.5ND 4-Chlorotoluene 2.5ND 1,3,5-Trimethylbenzene 2.5ND tert-Butylbenzene 2.5ND 1,2,4-Trimethylbenzene 2.5ND sec-Butylbenzene 2.5ND 1,3-Dichlorobenzene 2.5ND 4-Isopropyltoluene 2.5ND 1,4-Dichlorobenzene 2.5ND 1,2-Dichlorobenzene 2.5ND n-Butylbenzene 2.5ND 1,2-Dibromo-3-Chloropropane 2.5ND 1,2,4-Trichlorobenzene 2.5ND Hexachlorobutadiene 2.5ND Naphthalene 2.5ND 1,2,3-Trichlorobenzene 2.5ND 106 70 - 130Surrogate: 1,2-Dichloroethane-d4 101 70 - 130Surrogate: Toluene-d8 100 70 - 130Surrogate: 4-Bromofluorobenzene LCS (B6K3045-BS1)Prepared: 11/30/2016 Analyzed: 11/30/2016 Dichlorodifluoromethane 7.5 110 70 - 13055.0 50.000 Chloromethane 5.0 99.3 70 - 13049.7 50.000 Vinyl Chloride 2.5 98.5 70 - 13049.3 50.000 Bromomethane 5.0 108 70 - 13054.1 50.000 Chloroethane 5.0 94.8 70 - 13047.4 50.000 Trichlorofluoromethane 20 90.1 70 - 13045.0 50.000 Acetone 75 90.5 70 - 13090.5 100.000 Acrylonitrile 4.0 105 70 - 13052.3 50.000 Trichlorotrifluoroethane 20 83.9 70 - 13042.0 50.000 1,1-Dichloroethene 2.5 83.6 70 - 13041.8 50.000 Methylene Chloride 25 77.8 70 - 13038.9 50.000 Carbon Disulfide 5.0 90.9 70 - 13045.4 50.000 Methyl-t-Butyl Ether (MTBE)2.5 91.0 70 - 13045.5 50.000 trans-1,2-Dichloroethene 2.5 88.3 70 - 13044.2 50.000 1,1-Dichloroethane 2.5 89.3 70 - 13044.7 50.000 2-Butanone (MEK)13 101 70 - 130101 100.000 2,2-Dichloropropane 2.5 84.6 70 - 13042.3 50.000 cis-1,2-Dichloroethene 2.5 90.4 70 - 13045.2 50.000 Chloroform 2.5 90.3 70 - 13045.1 50.000 Tetrahydrofuran 13 101 70 - 13050.5 50.000 1,1,1-Trichloroethane 2.5 84.1 70 - 13042.0 50.000 Carbon Tetrachloride 2.5 77.5 70 - 13038.8 50.000 1,1-Dichloropropene 2.5 83.5 70 - 13041.7 50.000 Benzene 2.5 87.9 70 - 13044.0 50.000 1,2-Dichloroethane 2.5 96.3 70 - 13048.2 50.000 Trichloroethene 2.5 84.9 70 - 13042.5 50.000 1,2-Dichloropropane 2.5 92.1 70 - 13046.1 50.000 Dibromomethane 2.5 95.0 70 - 13047.5 50.000 Bromodichloromethane 2.5 93.0 70 - 13046.5 50.000 Methyl Isobutyl Ketone 13 101 70 - 130101 100.000 cis-1,3-Dichloropropene 2.5 93.7 70 - 13046.8 50.000 Toluene 2.5 85.9 70 - 13042.9 50.000 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 37 of 48 Project: NPU, Oakdale CET # : 6110624 Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes LCS (B6K3045-BS1) - Continued Prepared: 11/30/2016 Analyzed: 11/30/2016 trans-1,3-Dichloropropene 2.5 95.0 70 - 13047.5 50.000 2-Hexanone 13 102 70 - 130102 100.000 1,1,2-Trichloroethane 2.5 95.9 70 - 13047.9 50.000 Tetrachloroethene 2.5 78.2 70 - 13039.1 50.000 1,3-Dichloropropane 2.5 96.5 70 - 13048.3 50.000 Dibromochloromethane 2.5 97.5 70 - 13048.7 50.000 1,2-Dibromoethane 2.5 97.7 70 - 13048.9 50.000 trans-1,4-Dichloro-2-Butene 13 102 70 - 13050.8 50.000 Chlorobenzene 2.5 88.0 70 - 13044.0 50.000 1,1,1,2-Tetrachloroethane 2.5 92.4 70 - 13046.2 50.000 Ethylbenzene 2.5 85.2 70 - 13042.6 50.000 m+p Xylenes 2.5 85.4 70 - 13085.4 100.000 o-Xylene 2.5 87.8 70 - 13043.9 50.000 Styrene 2.5 92.1 70 - 13046.1 50.000 Bromoform 2.5 98.5 70 - 13049.2 50.000 Isopropylbenzene 2.5 85.3 70 - 13042.6 50.000 1,1,2,2-Tetrachloroethane 2.5 102 70 - 13050.9 50.000 Bromobenzene 2.5 94.0 70 - 13047.0 50.000 1,2,3-Trichloropropane 2.5 103 70 - 13051.3 50.000 n-Propylbenzene 2.5 88.7 70 - 13044.4 50.000 2-Chlorotoluene 2.5 91.1 70 - 13045.6 50.000 4-Chlorotoluene 2.5 93.0 70 - 13046.5 50.000 1,3,5-Trimethylbenzene 2.5 89.0 70 - 13044.5 50.000 tert-Butylbenzene 2.5 86.0 70 - 13043.0 50.000 1,2,4-Trimethylbenzene 2.5 91.0 70 - 13045.5 50.000 sec-Butylbenzene 2.5 88.0 70 - 13044.0 50.000 1,3-Dichlorobenzene 2.5 93.0 70 - 13046.5 50.000 4-Isopropyltoluene 2.5 88.8 70 - 13044.4 50.000 1,4-Dichlorobenzene 2.5 93.3 70 - 13046.7 50.000 1,2-Dichlorobenzene 2.5 96.9 70 - 13048.5 50.000 n-Butylbenzene 2.5 91.6 70 - 13045.8 50.000 1,2-Dibromo-3-Chloropropane 2.5 102 70 - 13051.2 50.000 1,2,4-Trichlorobenzene 2.5 95.3 70 - 13047.6 50.000 Hexachlorobutadiene 2.5 86.5 70 - 13043.3 50.000 Naphthalene 2.5 102 70 - 13051.0 50.000 1,2,3-Trichlorobenzene 2.5 97.8 70 - 13048.9 50.000 105 70 - 130Surrogate: 1,2-Dichloroethane-d4 101 70 - 130Surrogate: Toluene-d8 99.4 70 - 130Surrogate: 4-Bromofluorobenzene 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 38 of 48 Project: NPU, Oakdale CET # : 6110624 Report Comments: Questions related to this report should be directed to David Ditta, Timothy Fusco, or Robert Blake at 203-377-9984. Sincerely, David Ditta Laboratory Director Sample Result Flags: E- The result is estimated, above the calibration range. H- The surrogate recovery is above the control limits. L- The surrogate recovery is below the control limits. B- The compound was detected in the laboratory blank. P- The Relative Percent Difference (RPD) of dual column analyses exceeds 40%. D- The RPD between the sample and the sample duplicate is high. Sample homogeneity may be a problem. +- The Surrogate was diluted out. *C1- The Continuing Calibration did not meet method specifications and was biased low for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased low. *C2- The Continuing Calibration did not meet method specifications and was biased high for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased high. *F1- The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the low side. *F2- The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the high side. I- The Analyte exceeds %RSD limits for the Initial Calibration. This is a non-directional bias. All results met standard operating procedures unless indicated by a data qualifier next to a sample result, or a narration in the QC report. Complete Environmental Testing is only responsible for the certified testing and is not directly responsible for the integrity of the sample before laboratory receipt. ND is None Detected at the specified detection limit All analyses were performed in house unless a Reference Laboratory is listed. Samples will be disposed of 30 days after the report date. 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 39 of 48 Project: NPU, Oakdale CET # : 6110624 Quality Control Definitions and Abbreviations 80 Lupes Drive Stratford, CT 06615 Internal Standard (IS)An Analyte added to each sample or sample extract. An internal standard is used to monitor retention time, calculate relative response, and quantify analytes of interest. Surrogate Recovery The % recovery for non-target organic compounds that are spiked into all samples. Used to determine method performance. Continuing Calibration An analytical standard analyzed with each set of samples to verify initial calibration of the system. Batch Samples that are analyzed together with the same method, sequence and lot of reagents within the same time period. ND Not detected RL Reporting Limit Dilution Multiplier added to detection levels (MDL) and/or sample results due to interferences and/or high concentration of target compounds. Duplicate Result from the duplicate analysis of a sample. Result Amount of analyte found in a sample. Spike Level Amount of analyte added to a sample Matrix Spike Result Amount of analyte found including amount that was spiked. Matrix Spike Dup Amount of analyte found in duplicate spikes including amount that was spike. Matrix Spike % Recovery % Recovery of spiked amount in sample. Matrix Spike Dup % Recovery % Recovery of spiked duplicate amount in sample. RPD Relative percent difference between Matrix Spike and Matrix Spike Duplicate. Blank Method Blank that has been taken through all steps of the analysis. LCS % Recovery Laboratory Control Sample percent recovery. The amount of analyte recovered from a fortified sample. Recovery Limits A range within which specified measurements results must fall to be compliant. CC Calibration Verification Flags: H-Recovery is above the control limits L-Recovery is below the control limits B-Compound detected in the Blank P-RPD of dual column results exceeds 40% #-Sample result too high for accurate spike recovery. Connecticut Laboratory Certification PH0116 New York Certification 11982 Massachussets Laboratory Certification M-CT903 Rhode Island Certification 199 Tel: (203) 377-9984 Fax: (203) 377-9952 email: cet1@cetlabs.com 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 40 of 48 REASONABLE CONFIDENCE PROTOCOL LABORATORY ANALYSIS QA/QC CERTIFICATION FORM Laboratory Name:Complete Environmental Testing, Inc.Soil & Environmental ServiceClient: Project Number:Project Location: Laboratory Sample ID(s): List RCP Methods Used:6110624 Sample Date(s): 6110624-01 thru 6110624-19 11/18/2016, 11/19/2016 CT-ETPH, EPA 8260C NPU, Oakdale CET #: ü 1 Yes NoFor each analytical method referenced in this laboratory report package, were all specified QA/QC performance criteria followed, including the requirement to explain any criteria falling outside of acceptable guidelines, as specified in the CTDEP method-specific Reasonable Confidence Protocol documents? ü 1A Yes NoWere the method specified preservation and holding time requirements met? ü 1B Yes No N/A VPH and EPH Methods only: Was the VPH and EPH method conducted without significant modifications (see Section 11.3 of respective RCP methods)? ü 2 Yes NoWere all samples received by the laboratory in a condition consistent with that described on the associated chain-of-custody document(s)? ü 3 Yes No N/A Were samples received at an appropriate temperature (< 6 degrees C.)? ü4Yes NoWere all QA/QC performance criteria specified in the CT DEP Reasonable Confidence Protocol documents achieved? ü 5a Yes Noa) Were reporting limits specified or referenced on the chain-of-custody? ü 5b Yes Nob) Were these reporting limits met? ü6Yes NoFor each analytical method referenced in this laboratory report package, were results reported for all consituents identified in the method-specific analyte lists presented in the Reasonable Confidence Protocol documents? ü 7 Yes NoAre project specific matrix spikes and laboratory duplicates included with this data set? Notes: For all questions to which the response was "No" (with the exception of question #7), additional information must be provided in an attached narrative. If the answer to question #1, #1A, or #1B is "No", the data package does not meet the requirements for "Reasonable Confidence." This form may not be altered and all questions must be answered. This certification form is to be used for RCP methods only. I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report, such information is accurate and complete. Authorized Signature: Position: Laboratory Director Printed Name: David Ditta Date: 12/01/2016 Name of Laboratory: Complete Environmental Testing, Inc. CTDEP RCP Laboratory Analysis QA/QC Certification Form - November 2007 Laboratory Quality Assurance and Quality Control Guidance Reasonable Confidence Protocols Page 1 of 3Page 41 of 48 RCP Case Narrative 4- See Exceptions Report Below 6- The client requested a subset of the CT8260 list. Analyte Exception Result Recovery QC Type Sample IDRPD(%) 4- Exceptions Report Batch/Sequence Methylene Chloride Low B6K284232.7 65.3LCS Methylene Chloride Low S6K290329.3 58.7CC Tetrahydrofuran High S6K290361.3 123CC 2-Butanone (MEK)High S6L0109155 124CC 2-Hexanone High S6L0109152 122CC Tetrachloroethene High S6L010967.1 134CC Tetrahydrofuran High S6L010971.9 144CC 2-Butanone (MEK)High S6L0110155 124CC 2-Hexanone High S6L0110152 122CC Tetrachloroethene High S6L011067.1 134CC Tetrahydrofuran High S6L011071.9 144CC CTDEP RCP Laboratory Analysis QA/QC Certification Form - November 2007 Laboratory Quality Assurance and Quality Control Guidance Reasonable Confidence Protocols Page 2 of 3Page 42 of 48 Batch Sample ID Specific MethodCET ID Collection Date QC Batch/Sequence Report MatrixSequence B6K2605 6110624-01 52 5-6ft CT-ETPH Soil 11/19/2016 B6K2605 6110624-02 53 2-5ft CT-ETPH Soil 11/19/2016 B6K2605 6110624-03 54 1-5ft CT-ETPH Soil 11/19/2016 B6K2606 6110624-04 55 1-4.5ft CT-ETPH Soil 11/19/2016 B6K2606 6110624-05 56 5-7ft CT-ETPH Soil 11/19/2016 B6K2606 6110624-06 57 1-5ft CT-ETPH Soil 11/19/2016 B6K2606 6110624-07 58 4-7ft CT-ETPH Soil 11/19/2016 B6K2606 6110624-08 60 4-7ft CT-ETPH Soil 11/19/2016 B6K2606 6110624-09 61 0-3ft CT-ETPH Soil 11/19/2016 B6K2606 6110624-10 62 0.5-2ft CT-ETPH Soil 11/19/2016 B6K2606 6110624-11 43 4-6ft CT-ETPH Soil 11/18/2016 B6K2606 6110624-12 44 4-6ft CT-ETPH Soil 11/18/2016 B6K2606 6110624-13 45 0-3ft CT-ETPH Soil 11/18/2016 B6K2606 6110624-14 46 1-3ft CT-ETPH Soil 11/18/2016 B6K2606 6110624-15 47 4-6ft CT-ETPH Soil 11/18/2016 B6K2606 6110624-16 48 4-6ft CT-ETPH Soil 11/18/2016 B6K2606 6110624-17 43/44A 4-6ft CT-ETPH Soil 11/18/2016 B6K2606 6110624-18 50 6ft CT-ETPH Soil 11/19/2016 B6K2606 6110624-19 51 5ft CT-ETPH Soil 11/19/2016 B6K2842 6110624-01 52 5-6ft EPA 8260C Soil 11/19/2016S6K2903 B6K2842 6110624-04 55 1-4.5ft EPA 8260C Soil 11/19/2016S6K2903 B6K2842 6110624-08 60 4-7ft EPA 8260C Soil 11/19/2016S6K2903 B6K2842 6110624-12 44 4-6ft EPA 8260C Soil 11/18/2016S6K2903 B6K2842 6110624-14 46 1-3ft EPA 8260C Soil 11/18/2016S6K2903 B6K2842 6110624-18 50 6ft EPA 8260C Soil 11/19/2016S6K2903 B6K3044 6110624-11 43 4-6ft EPA 8260C Soil 11/18/2016S6L0109 B6K3045 6110624-04RE1 55 1-4.5ft EPA 8260C Soil 11/19/2016S6L0110 B6K3045 6110624-11RE1 43 4-6ft EPA 8260C Soil 11/18/2016S6L0110 CTDEP RCP Laboratory Analysis QA/QC Certification Form - November 2007 Laboratory Quality Assurance and Quality Control Guidance Reasonable Confidence Protocols Page 3 of 3Page 43 of 48 CertificationsAnalyte CERTIFICATIONS Certified Analyses included in this Report CT-ETPH in Soil CTETPH EPA 8260C in Soil CT,NYDichlorodifluoromethane CT,NYChloromethane CT,NYVinyl Chloride CT,NYBromomethane CT,NYChloroethane CT,NYTrichlorofluoromethane CT,NYAcetone CT,NYAcrylonitrile CT,NYTrichlorotrifluoroethane CT,NY1,1-Dichloroethene CT,NYMethylene Chloride CT,NYCarbon Disulfide CT,NYMethyl-t-Butyl Ether (MTBE) CT,NYMethyl-t-Butyl Ether (MTBE) CT,NYtrans-1,2-Dichloroethene CT,NY1,1-Dichloroethane CT,NY2-Butanone (MEK) CT,NY2,2-Dichloropropane CT,NYcis-1,2-Dichloroethene CT,NYChloroform CTTetrahydrofuran CT,NY1,1,1-Trichloroethane CT,NYCarbon Tetrachloride CT,NY1,1-Dichloropropene CT,NYBenzene CT,NYBenzene CT,NY1,2-Dichloroethane CT,NYTrichloroethene CT,NY1,2-Dichloropropane CT,NYDibromomethane CT,NYBromodichloromethane CT,NYMethyl Isobutyl Ketone CT,NYcis-1,3-Dichloropropene CT,NYToluene CT,NYToluene CT,NYtrans-1,3-Dichloropropene CT,NY2-Hexanone CT,NY1,1,2-Trichloroethane CT,NYTetrachloroethene CT,NY1,3-Dichloropropane CT,NYDibromochloromethane CT,NY1,2-Dibromoethane CT,NYtrans-1,4-Dichloro-2-Butene CT,NYChlorobenzene CT,NYChlorobenzene CT,NY1,1,1,2-Tetrachloroethane CT,NYEthylbenzene Page 44 of 48 CertificationsAnalyte CERTIFICATIONS Certified Analyses included in this Report EPA 8260C in Soil CT,NYEthylbenzene CT,NYm+p Xylenes CT,NYm+p Xylenes CT,NYo-Xylene CT,NYo-Xylene CT,NYStyrene CT,NYStyrene CT,NYBromoform CT,NYIsopropylbenzene CT,NYIsopropylbenzene CT,NY1,1,2,2-Tetrachloroethane CT,NYBromobenzene CT,NYBromobenzene CT,NY1,2,3-Trichloropropane CT,NYn-Propylbenzene CT,NYn-Propylbenzene CT,NY2-Chlorotoluene CT,NY2-Chlorotoluene CT,NY4-Chlorotoluene CT,NY4-Chlorotoluene CT,NY1,3,5-Trimethylbenzene CT,NY1,3,5-Trimethylbenzene CT,NYtert-Butylbenzene CT,NYtert-Butylbenzene CT,NY1,2,4-Trimethylbenzene CT,NY1,2,4-Trimethylbenzene CT,NYsec-Butylbenzene CT,NYsec-Butylbenzene CT,NY1,3-Dichlorobenzene CT,NY1,3-Dichlorobenzene CT,NY4-Isopropyltoluene CT,NY4-Isopropyltoluene CT,NY1,4-Dichlorobenzene CT,NY1,4-Dichlorobenzene CT,NY1,2-Dichlorobenzene CT,NY1,2-Dichlorobenzene CT,NYn-Butylbenzene CT,NYn-Butylbenzene CT,NY1,2-Dibromo-3-Chloropropane CT,NY1,2,4-Trichlorobenzene CT,NY1,2,4-Trichlorobenzene CT,NYHexachlorobutadiene CT,NYHexachlorobutadiene CT,NYNaphthalene CT,NYNaphthalene CT1,2,3-Trichlorobenzene CT1,2,3-Trichlorobenzene Page 45 of 48 Complete Environmental Testing operates under the following certifications and accreditations: Code Description Number Expires Connecticut Public Health 09/30/2018CTPH0116 New York Certification (NELAC)04/01/2017NY11982 Page 46 of 48 Page 47 of 48 Page 48 of 48 80 Lupes Drive Stratford, CT 06615 Tel: (203) 377-9984 Fax: (203) 377-9952 e-mail: cet1@cetlabs.com Client:Mr. Don Fortunato Soil & Environmental Service 61 Plants Dam Road East Lyme, CT 06333 Analytical Report CET# 6110625R Report Date:December 02, 2016 Project: NPU, Oakdale Rhode Island Certification: 199Massachusetts laboratory Certificate: M-CT903 Connecticut Laboratory Certificate: PH 0116 New York NELAP Accreditation: 11982 Page 1 of 33 Project: NPU, Oakdale CET # : 6110625 Sample ID Laboratory ID Matrix Collection Date/Time Receipt Date SAMPLE SUMMARY The sample(s) were received at 4.9 C. This report contains analytical data associated with following samples only. 63 5-9in 6110625-01 Soil 11/22/201611/21/2016 64 5-9in 6110625-02 Soil 11/22/201611/21/2016 65 0-12in 6110625-03 Soil 11/22/201611/21/2016 12A 0-12in 6110625-04 Soil 11/22/201611/21/2016 12B 0-12in 6110625-05 Soil 11/22/201611/21/2016 SW 2 6110625-06 Water 11/22/201611/21/2016 1 Root 4-6ft 6110625-07 Solid 11/22/201611/19/2016 Notes Date/Time AnalyzedPreparedBatchDilutionRLResultLaboratory ID Client Sample ID Units Analyst: ALM Matrix: Soil Analyte: Percent Solids [SM 2540 G] 90 11/29/2016 11/29/2016 09:146110625-01 %63 5-9in 1.0 1 B6K2907 91 11/29/2016 11/29/2016 09:146110625-02 %64 5-9in 1.0 1 B6K2907 78 11/29/2016 11/29/2016 09:146110625-03 %65 0-12in 1.0 1 B6K2907 82 11/29/2016 11/29/2016 12:306110625-04 %12A 0-12in 1.0 1 B6K2908 81 11/29/2016 11/29/2016 12:306110625-05 %12B 0-12in 1.0 1 B6K2908 Notes Date/Time AnalyzedPreparedBatchDilutionRLResultLaboratory ID Client Sample ID Units Analyst: ALM Matrix: Solid Analyte: Percent Solids [SM 2540 G] 69 11/29/2016 11/29/2016 13:186110625-07 %1 Root 4-6ft 1.0 1 B6K2922 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 2 of 33 Project: NPU, Oakdale CET # : 6110625 Client Sample ID 63 5-9in Lab ID: 6110625-01 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6K2606 11/26/2016 11/28/2016 03:1655EPA 3550C *F1 Surrogate: Octacosane 76.3 %11/26/2016 11/28/2016 03:16B6K260650 - 150 Client Sample ID 64 5-9in Lab ID: 6110625-02 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6K2606 11/26/2016 11/28/2016 03:4055EPA 3550C *F1 Surrogate: Octacosane 77.1 %11/26/2016 11/28/2016 03:40B6K260650 - 150 Client Sample ID 65 0-12in Lab ID: 6110625-03 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH 490 1 B6K2606 11/26/2016 11/28/2016 04:0464EPA 3550C 2*F1 Surrogate: Octacosane 80.3 %11/26/2016 11/28/2016 04:04B6K260650 - 150 2 C9-C28 Fuel Oil Range 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 3 of 33 Project: NPU, Oakdale CET # : 6110625 Client Sample ID 12A 0-12in Lab ID: 6110625-04 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6K2606 11/26/2016 12/01/2016 11:5261EPA 3550C *F1 Surrogate: Octacosane 90.7 %11/26/2016 12/01/2016 11:52B6K260650 - 150 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 4 of 33 Project: NPU, Oakdale CET # : 6110625 Client Sample ID 12B 0-12in Lab ID: 6110625-05 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6K2607 11/26/2016 11/28/2016 06:2662EPA 3550C *F1 Surrogate: Octacosane 85.3 %11/26/2016 11/28/2016 06:26B6K260750 - 150 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Methyl-t-Butyl Ether (MTBE)ND 1.73 B6K2842 11/28/2016 11/28/2016 21:515.4 EPA 5035A-L Benzene ND 1.73 B6K2842 11/28/2016 11/28/2016 21:515.4 EPA 5035A-L Toluene ND 1.73 B6K2842 11/28/2016 11/28/2016 21:515.4 EPA 5035A-L Chlorobenzene ND 1.73 B6K2842 11/28/2016 11/28/2016 21:515.4 EPA 5035A-L Ethylbenzene ND 1.73 B6K2842 11/28/2016 11/28/2016 21:515.4 EPA 5035A-L m+p Xylenes ND 1.73 B6K2842 11/28/2016 11/28/2016 21:515.4 EPA 5035A-L o-Xylene ND 1.73 B6K2842 11/28/2016 11/28/2016 21:515.4 EPA 5035A-L Styrene ND 1.73 B6K2842 11/28/2016 11/28/2016 21:515.4 EPA 5035A-L Isopropylbenzene ND 1.73 B6K2842 11/28/2016 11/28/2016 21:515.4 EPA 5035A-L Bromobenzene ND 1.73 B6K2842 11/28/2016 11/28/2016 21:515.4 EPA 5035A-L n-Propylbenzene ND 1.73 B6K2842 11/28/2016 11/28/2016 21:515.4 EPA 5035A-L 2-Chlorotoluene ND 1.73 B6K2842 11/28/2016 11/28/2016 21:515.4 EPA 5035A-L 4-Chlorotoluene ND 1.73 B6K2842 11/28/2016 11/28/2016 21:515.4 EPA 5035A-L 1,3,5-Trimethylbenzene ND 1.73 B6K2842 11/28/2016 11/28/2016 21:515.4 EPA 5035A-L tert-Butylbenzene ND 1.73 B6K2842 11/28/2016 11/28/2016 21:515.4 EPA 5035A-L 1,2,4-Trimethylbenzene ND 1.73 B6K2842 11/28/2016 11/28/2016 21:515.4 EPA 5035A-L sec-Butylbenzene ND 1.73 B6K2842 11/28/2016 11/28/2016 21:515.4 EPA 5035A-L 1,3-Dichlorobenzene ND 1.73 B6K2842 11/28/2016 11/28/2016 21:515.4 EPA 5035A-L 4-Isopropyltoluene ND 1.73 B6K2842 11/28/2016 11/28/2016 21:515.4 EPA 5035A-L 1,4-Dichlorobenzene ND 1.73 B6K2842 11/28/2016 11/28/2016 21:515.4 EPA 5035A-L 1,2-Dichlorobenzene ND 1.73 B6K2842 11/28/2016 11/28/2016 21:515.4 EPA 5035A-L n-Butylbenzene ND 1.73 B6K2842 11/28/2016 11/28/2016 21:515.4 EPA 5035A-L 1,2,4-Trichlorobenzene ND 1.73 B6K2842 11/28/2016 11/28/2016 21:515.4 EPA 5035A-L Hexachlorobutadiene ND 1.73 B6K2842 11/28/2016 11/28/2016 21:515.4 EPA 5035A-L Naphthalene ND 1.73 B6K2842 11/28/2016 11/28/2016 21:515.4 EPA 5035A-L 1,2,3-Trichlorobenzene ND 1.73 B6K2842 11/28/2016 11/28/2016 21:515.4 EPA 5035A-L Surrogate: 1,2-Dichloroethane-d4 107 %11/28/2016 11/28/2016 21:51B6K284270 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 5 of 33 Project: NPU, Oakdale CET # : 6110625 Client Sample ID 12B 0-12in Lab ID: 6110625-05 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg) Result (ug/kg)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Surrogate: Toluene-d8 101 %11/28/2016 11/28/2016 21:51B6K284270 - 130 Surrogate: 4-Bromofluorobenzene 91.0 %11/28/2016 11/28/2016 21:51B6K284270 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 6 of 33 Project: NPU, Oakdale CET # : 6110625 Client Sample ID SW 2 Lab ID: 6110625-06 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/L) Result (mg/L)Analyte Prep Method Method: CT-ETPH Matrix: Water Analyst: MHConn. Extractable TPH ETPH ND 1 B6K2824 11/28/2016 11/28/2016 16:440.10 EPA 3510C Surrogate: Octacosane 92.5 %11/28/2016 11/28/2016 16:44B6K282450 - 150 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/L) Result (ug/L)Analyte Prep Method Method: EPA 8260C Matrix: Water Analyst: TWFVolatile Organics Methyl-t-Butyl Ether (MTBE)ND 1 B6K2532 11/25/2016 11/25/2016 19:415.0 EPA 5030C Benzene ND 1 B6K2532 11/25/2016 11/25/2016 19:411.0 EPA 5030C Toluene ND 1 B6K2532 11/25/2016 11/25/2016 19:411.0 EPA 5030C Chlorobenzene ND 1 B6K2532 11/25/2016 11/25/2016 19:411.0 EPA 5030C Ethylbenzene ND 1 B6K2532 11/25/2016 11/25/2016 19:411.0 EPA 5030C m+p Xylenes ND 1 B6K2532 11/25/2016 11/25/2016 19:411.0 EPA 5030C o-Xylene ND 1 B6K2532 11/25/2016 11/25/2016 19:411.0 EPA 5030C Styrene ND 1 B6K2532 11/25/2016 11/25/2016 19:411.0 EPA 5030C Isopropylbenzene ND 1 B6K2532 11/25/2016 11/25/2016 19:411.0 EPA 5030C Bromobenzene ND 1 B6K2532 11/25/2016 11/25/2016 19:411.0 EPA 5030C n-Propylbenzene ND 1 B6K2532 11/25/2016 11/25/2016 19:411.0 EPA 5030C 2-Chlorotoluene ND 1 B6K2532 11/25/2016 11/25/2016 19:411.0 EPA 5030C 4-Chlorotoluene ND 1 B6K2532 11/25/2016 11/25/2016 19:411.0 EPA 5030C 1,3,5-Trimethylbenzene ND 1 B6K2532 11/25/2016 11/25/2016 19:411.0 EPA 5030C tert-Butylbenzene ND 1 B6K2532 11/25/2016 11/25/2016 19:411.0 EPA 5030C 1,2,4-Trimethylbenzene ND 1 B6K2532 11/25/2016 11/25/2016 19:411.0 EPA 5030C sec-Butylbenzene ND 1 B6K2532 11/25/2016 11/25/2016 19:411.0 EPA 5030C 1,3-Dichlorobenzene ND 1 B6K2532 11/25/2016 11/25/2016 19:411.0 EPA 5030C 4-Isopropyltoluene ND 1 B6K2532 11/25/2016 11/25/2016 19:411.0 EPA 5030C 1,4-Dichlorobenzene ND 1 B6K2532 11/25/2016 11/25/2016 19:411.0 EPA 5030C 1,2-Dichlorobenzene ND 1 B6K2532 11/25/2016 11/25/2016 19:411.0 EPA 5030C n-Butylbenzene ND 1 B6K2532 11/25/2016 11/25/2016 19:411.0 EPA 5030C 1,2,4-Trichlorobenzene ND 1 B6K2532 11/25/2016 11/25/2016 19:411.0 EPA 5030C Hexachlorobutadiene ND 1 B6K2532 11/25/2016 11/25/2016 19:410.45 EPA 5030C Naphthalene ND 1 B6K2532 11/25/2016 11/25/2016 19:411.0 EPA 5030C 1,2,3-Trichlorobenzene ND 1 B6K2532 11/25/2016 11/25/2016 19:411.0 EPA 5030C Surrogate: 1,2-Dichloroethane-d4 95.7 %11/25/2016 11/25/2016 19:41B6K253270 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 7 of 33 Project: NPU, Oakdale CET # : 6110625 Client Sample ID SW 2 Lab ID: 6110625-06 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/L) Result (ug/L)Analyte Prep Method Method: EPA 8260C Matrix: Water Analyst: TWFVolatile Organics Surrogate: Toluene-d8 94.0 %11/25/2016 11/25/2016 19:41B6K253270 - 130 Surrogate: 4-Bromofluorobenzene 93.4 %11/25/2016 11/25/2016 19:41B6K253270 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 8 of 33 Project: NPU, Oakdale CET # : 6110625 Client Sample ID 1 Root 4-6ft Lab ID: 6110625-07 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Solid Analyst: MHConn. Extractable TPH ETPH 5000 1 B6K2607 11/26/2016 11/28/2016 08:0172EPA 3550C 2*F1 Surrogate: Octacosane 85.9 %11/26/2016 11/28/2016 08:01B6K260750 - 150 2 C9-C28 Fuel Oil Range Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Solid Analyst: DAHVolatile Organics Dichlorodifluoromethane ND 1.98 B6K3017 11/29/2016 11/29/2016 16:2922EPA 5035A-L Chloromethane ND 1.98 B6K3017 11/29/2016 11/29/2016 16:2914EPA 5035A-L Vinyl Chloride ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L Bromomethane ND 1.98 B6K3017 11/29/2016 11/29/2016 16:2914EPA 5035A-L Chloroethane ND 1.98 B6K3017 11/29/2016 11/29/2016 16:2914EPA 5035A-L Trichlorofluoromethane ND 1.98 B6K3017 11/29/2016 11/29/2016 16:2958EPA 5035A-L Acetone ND 1.98 B6K3017 11/29/2016 11/29/2016 16:29220EPA 5035A-L Acrylonitrile ND 1.98 B6K3017 11/29/2016 11/29/2016 16:2912EPA 5035A-L Trichlorotrifluoroethane ND 1.98 B6K3017 11/29/2016 11/29/2016 16:2958EPA 5035A-L 1,1-Dichloroethene ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L Methylene Chloride ND 1.98 B6K3017 11/29/2016 11/29/2016 16:2972EPA 5035A-L *C1 Carbon Disulfide ND 1.98 B6K3017 11/29/2016 11/29/2016 16:2914EPA 5035A-L Methyl-t-Butyl Ether (MTBE)ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L trans-1,2-Dichloroethene ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L 1,1-Dichloroethane ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L 2-Butanone (MEK)ND 1.98 B6K3017 11/29/2016 11/29/2016 16:2936EPA 5035A-L 2,2-Dichloropropane ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L cis-1,2-Dichloroethene ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L Chloroform ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L Tetrahydrofuran ND 1.98 B6K3017 11/29/2016 11/29/2016 16:2936EPA 5035A-L *C2 1,1,1-Trichloroethane ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L Carbon Tetrachloride ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L 1,1-Dichloropropene ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L Benzene ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L 1,2-Dichloroethane ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L Trichloroethene ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L 1,2-Dichloropropane ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L Dibromomethane ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 9 of 33 Project: NPU, Oakdale CET # : 6110625 Client Sample ID 1 Root 4-6ft Lab ID: 6110625-07 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Solid Analyst: DAHVolatile Organics Bromodichloromethane ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L Methyl Isobutyl Ketone ND 1.98 B6K3017 11/29/2016 11/29/2016 16:2936EPA 5035A-L cis-1,3-Dichloropropene ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L Toluene ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L trans-1,3-Dichloropropene ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L 2-Hexanone ND 1.98 B6K3017 11/29/2016 11/29/2016 16:2936EPA 5035A-L 1,1,2-Trichloroethane ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L Tetrachloroethene ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L *C2 1,3-Dichloropropane ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L Dibromochloromethane ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L 1,2-Dibromoethane ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L trans-1,4-Dichloro-2-Butene ND 1.98 B6K3017 11/29/2016 11/29/2016 16:2936EPA 5035A-L Chlorobenzene ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L 1,1,1,2-Tetrachloroethane ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L Ethylbenzene ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L m+p Xylenes 8.5 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L o-Xylene 110 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L Styrene ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L Bromoform ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L Isopropylbenzene 20 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L 1,1,2,2-Tetrachloroethane ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L Bromobenzene ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L 1,2,3-Trichloropropane ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L n-Propylbenzene 63 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L 2-Chlorotoluene ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L 4-Chlorotoluene ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L 1,3,5-Trimethylbenzene 640 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L E tert-Butylbenzene ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L *C2 1,2,4-Trimethylbenzene 100 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L sec-Butylbenzene 170 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L 1,3-Dichlorobenzene ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L 4-Isopropyltoluene 120 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L 1,4-Dichlorobenzene ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L 1,2-Dichlorobenzene ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L n-Butylbenzene 210 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L 1,2-Dibromo-3-Chloropropane ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L 1,2,4-Trichlorobenzene ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L Hexachlorobutadiene ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L Naphthalene ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L 1,2,3-Trichlorobenzene ND 1.98 B6K3017 11/29/2016 11/29/2016 16:297.2 EPA 5035A-L 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 10 of 33 Project: NPU, Oakdale CET # : 6110625 Client Sample ID 1 Root 4-6ft Lab ID: 6110625-07 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg) Result (ug/kg)Analyte Prep Method Method: EPA 8260C Matrix: Solid Analyst: DAHVolatile Organics Surrogate: 1,2-Dichloroethane-d4 104 %11/29/2016 11/29/2016 16:29B6K301770 - 130 Surrogate: Toluene-d8 95.7 %11/29/2016 11/29/2016 16:29B6K301770 - 130 Surrogate: 4-Bromofluorobenzene 93.7 %11/29/2016 11/29/2016 16:29B6K301770 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 11 of 33 Project: NPU, Oakdale CET # : 6110625 Client Sample ID 1 Root 4-6ft Lab ID: 6110625-07RE1(Dilution) Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Solid Analyst: DAHVolatile Organics Dichlorodifluoromethane ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57540EPA 5035A-H Chloromethane ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57360EPA 5035A-H Vinyl Chloride ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H Bromomethane ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57360EPA 5035A-H Chloroethane ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57360EPA 5035A-H Trichlorofluoromethane ND 49.16 B6K3018 11/29/2016 11/29/2016 20:571400EPA 5035A-H Acetone ND 49.16 B6K3018 11/29/2016 11/29/2016 20:575400EPA 5035A-H Acrylonitrile ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57290EPA 5035A-H Trichlorotrifluoroethane ND 49.16 B6K3018 11/29/2016 11/29/2016 20:571400EPA 5035A-H 1,1-Dichloroethene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H Methylene Chloride ND 49.16 B6K3018 11/29/2016 11/29/2016 20:571800EPA 5035A-H *C1 Carbon Disulfide ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57360EPA 5035A-H Methyl-t-Butyl Ether (MTBE)ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H trans-1,2-Dichloroethene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H 1,1-Dichloroethane ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H 2-Butanone (MEK)ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57890EPA 5035A-H 2,2-Dichloropropane ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H cis-1,2-Dichloroethene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H Chloroform ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H Tetrahydrofuran ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57890EPA 5035A-H *C2 1,1,1-Trichloroethane ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H Carbon Tetrachloride ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H 1,1-Dichloropropene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H Benzene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H 1,2-Dichloroethane ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H Trichloroethene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H 1,2-Dichloropropane ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H Dibromomethane ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H Bromodichloromethane ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H Methyl Isobutyl Ketone ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57890EPA 5035A-H cis-1,3-Dichloropropene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H Toluene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H trans-1,3-Dichloropropene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H 2-Hexanone ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57890EPA 5035A-H 1,1,2-Trichloroethane ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H Tetrachloroethene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H *C2 1,3-Dichloropropane ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H Dibromochloromethane ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H 1,2-Dibromoethane ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H trans-1,4-Dichloro-2-Butene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57890EPA 5035A-H Chlorobenzene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 12 of 33 Project: NPU, Oakdale CET # : 6110625 Client Sample ID 1 Root 4-6ft Lab ID: 6110625-07RE1(Dilution) Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Solid Analyst: DAHVolatile Organics 1,1,1,2-Tetrachloroethane ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H Ethylbenzene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H m+p Xylenes ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H o-Xylene 270 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H Styrene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H Bromoform ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H Isopropylbenzene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H 1,1,2,2-Tetrachloroethane ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H Bromobenzene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H 1,2,3-Trichloropropane ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H n-Propylbenzene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H 2-Chlorotoluene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H 4-Chlorotoluene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H 1,3,5-Trimethylbenzene 1100 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H tert-Butylbenzene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H *C2 1,2,4-Trimethylbenzene 370 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H sec-Butylbenzene 410 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H 1,3-Dichlorobenzene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H 4-Isopropyltoluene 270 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H 1,4-Dichlorobenzene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H 1,2-Dichlorobenzene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H n-Butylbenzene 730 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H 1,2-Dibromo-3-Chloropropane ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H 1,2,4-Trichlorobenzene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H Hexachlorobutadiene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H Naphthalene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H 1,2,3-Trichlorobenzene ND 49.16 B6K3018 11/29/2016 11/29/2016 20:57180EPA 5035A-H Surrogate: 1,2-Dichloroethane-d4 93.9 %11/29/2016 11/29/2016 20:57B6K301870 - 130 Surrogate: Toluene-d8 102 %11/29/2016 11/29/2016 20:57B6K301870 - 130 Surrogate: 4-Bromofluorobenzene 99.9 %11/29/2016 11/29/2016 20:57B6K301870 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 13 of 33 Project: NPU, Oakdale CET # : 6110625 QUALITY CONTROL SECTION Batch B6K2532 - EPA 8260C Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/L) (ug/L)Notes Blank (B6K2532-BLK1)Prepared: 11/25/2016 Analyzed: 11/25/2016 Methyl-t-Butyl Ether (MTBE)5.0ND Benzene 1.0ND Toluene 1.0ND Chlorobenzene 1.0ND Ethylbenzene 1.0ND m+p Xylenes 1.0ND o-Xylene 1.0ND Styrene 1.0ND Isopropylbenzene 1.0ND Bromobenzene 1.0ND n-Propylbenzene 1.0ND 2-Chlorotoluene 1.0ND 4-Chlorotoluene 1.0ND 1,3,5-Trimethylbenzene 1.0ND tert-Butylbenzene 1.0ND 1,2,4-Trimethylbenzene 1.0ND sec-Butylbenzene 1.0ND 1,3-Dichlorobenzene 1.0ND 4-Isopropyltoluene 1.0ND 1,4-Dichlorobenzene 1.0ND 1,2-Dichlorobenzene 1.0ND n-Butylbenzene 1.0ND 1,2,4-Trichlorobenzene 1.0ND Hexachlorobutadiene 0.45ND Naphthalene 1.0ND 1,2,3-Trichlorobenzene 1.0ND 103 70 - 130Surrogate: 1,2-Dichloroethane-d4 96.1 70 - 130Surrogate: Toluene-d8 99.8 70 - 130Surrogate: 4-Bromofluorobenzene LCS (B6K2532-BS1)Prepared: 11/25/2016 Analyzed: 11/25/2016 Methyl-t-Butyl Ether (MTBE)5.0 93.7 70 - 13046.8 50.000 Benzene 1.0 97.7 70 - 13048.8 50.000 Toluene 1.0 97.0 70 - 13048.5 50.000 Chlorobenzene 1.0 94.5 70 - 13047.2 50.000 Ethylbenzene 1.0 95.6 70 - 13047.8 50.000 m+p Xylenes 1.0 100 70 - 130100 100.000 o-Xylene 1.0 98.4 70 - 13049.2 50.000 Styrene 1.0 101 70 - 13050.3 50.000 Isopropylbenzene 1.0 100 70 - 13050.0 50.000 Bromobenzene 1.0 92.2 70 - 13046.1 50.000 n-Propylbenzene 1.0 92.9 70 - 13046.5 50.000 2-Chlorotoluene 1.0 95.1 70 - 13047.6 50.000 4-Chlorotoluene 1.0 95.7 70 - 13047.9 50.000 1,3,5-Trimethylbenzene 1.0 100 70 - 13050.2 50.000 tert-Butylbenzene 1.0 100 70 - 13050.1 50.000 1,2,4-Trimethylbenzene 1.0 103 70 - 13051.6 50.000 sec-Butylbenzene 1.0 95.9 70 - 13048.0 50.000 1,3-Dichlorobenzene 1.0 95.5 70 - 13047.8 50.000 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 14 of 33 Project: NPU, Oakdale CET # : 6110625 Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/L) (ug/L)Notes LCS (B6K2532-BS1) - Continued Prepared: 11/25/2016 Analyzed: 11/25/2016 4-Isopropyltoluene 1.0 100 70 - 13050.1 50.000 1,4-Dichlorobenzene 1.0 94.8 70 - 13047.4 50.000 1,2-Dichlorobenzene 1.0 97.1 70 - 13048.6 50.000 n-Butylbenzene 1.0 97.8 70 - 13048.9 50.000 1,2,4-Trichlorobenzene 1.0 98.7 70 - 13049.4 50.000 Hexachlorobutadiene 0.45 98.0 70 - 13049.0 50.000 Naphthalene 1.0 92.2 70 - 13046.1 50.000 1,2,3-Trichlorobenzene 1.0 84.0 70 - 13042.0 50.000 95.7 70 - 130Surrogate: 1,2-Dichloroethane-d4 98.5 70 - 130Surrogate: Toluene-d8 97.2 70 - 130Surrogate: 4-Bromofluorobenzene 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 15 of 33 Project: NPU, Oakdale CET # : 6110625 Batch B6K2606 - CT-ETPH Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(mg/kg) (mg/kg)Notes Blank (B6K2606-BLK1)Prepared: 11/26/2016 Analyzed: 11/27/2016 ETPH 50ND 84.2 50 - 150Surrogate: Octacosane LCS (B6K2606-BS1)Prepared: 11/26/2016 Analyzed: 11/27/2016 ETPH 50 60 - 1201220 L 84.7 50 - 150Surrogate: Octacosane 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 16 of 33 Project: NPU, Oakdale CET # : 6110625 Batch B6K2607 - CT-ETPH Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(mg/kg) (mg/kg)Notes Blank (B6K2607-BLK1)Prepared: 11/26/2016 Analyzed: 11/28/2016 ETPH 50ND 61.2 50 - 150Surrogate: Octacosane LCS (B6K2607-BS1)Prepared: 11/26/2016 Analyzed: 11/28/2016 ETPH 50 60 - 1201200 L 90.5 50 - 150Surrogate: Octacosane Duplicate (B6K2607-DUP1)Source: 6110625-05 Prepared: 11/26/2016 Analyzed: 11/28/2016 ETPH 62 ND 30ND 91.0 50 - 150Surrogate: Octacosane Matrix Spike (B6K2607-MS1)Source: 6110625-05 Prepared: 11/26/2016 Analyzed: 11/28/2016 ETPH 62 ND 50 - 1501510 L 85.0 50 - 150Surrogate: Octacosane Matrix Spike Dup (B6K2607-MSD1)Source: 6110625-05 Prepared: 11/26/2016 Analyzed: 11/28/2016 ETPH 62 ND 50 - 150 0.565 301500 L 91.5 50 - 150Surrogate: Octacosane 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 17 of 33 Project: NPU, Oakdale CET # : 6110625 Batch B6K2824 - CT-ETPH Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(mg/L) (mg/L)Notes Blank (B6K2824-BLK1)Prepared: 11/28/2016 Analyzed: 11/28/2016 ETPH 0.10ND 81.8 50 - 150Surrogate: Octacosane LCS (B6K2824-BS1)Prepared: 11/28/2016 Analyzed: 11/28/2016 ETPH 0.10 79.0 60 - 1203.95 5.000 91.4 50 - 150Surrogate: Octacosane 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 18 of 33 Project: NPU, Oakdale CET # : 6110625 Batch B6K2842 - EPA 8260C Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes Blank (B6K2842-BLK1)Prepared: 11/28/2016 Analyzed: 11/28/2016 Methyl-t-Butyl Ether (MTBE)2.5ND Benzene 2.5ND Toluene 2.5ND Chlorobenzene 2.5ND Ethylbenzene 2.5ND m+p Xylenes 2.5ND o-Xylene 2.5ND Styrene 2.5ND Isopropylbenzene 2.5ND Bromobenzene 2.5ND n-Propylbenzene 2.5ND 2-Chlorotoluene 2.5ND 4-Chlorotoluene 2.5ND 1,3,5-Trimethylbenzene 2.5ND tert-Butylbenzene 2.5ND 1,2,4-Trimethylbenzene 2.5ND sec-Butylbenzene 2.5ND 1,3-Dichlorobenzene 2.5ND 4-Isopropyltoluene 2.5ND 1,4-Dichlorobenzene 2.5ND 1,2-Dichlorobenzene 2.5ND n-Butylbenzene 2.5ND 1,2,4-Trichlorobenzene 2.5ND Hexachlorobutadiene 2.5ND Naphthalene 2.5ND 1,2,3-Trichlorobenzene 2.5ND 99.6 70 - 130Surrogate: 1,2-Dichloroethane-d4 95.3 70 - 130Surrogate: Toluene-d8 111 70 - 130Surrogate: 4-Bromofluorobenzene LCS (B6K2842-BS1)Prepared: 11/28/2016 Analyzed: 11/28/2016 Methyl-t-Butyl Ether (MTBE)2.5 96.3 70 - 13048.1 50.000 Benzene 2.5 97.4 70 - 13048.7 50.000 Toluene 2.5 94.3 70 - 13047.1 50.000 Chlorobenzene 2.5 96.7 70 - 13048.3 50.000 Ethylbenzene 2.5 98.1 70 - 13049.0 50.000 m+p Xylenes 2.5 97.8 70 - 13097.8 100.000 o-Xylene 2.5 98.1 70 - 13049.0 50.000 Styrene 2.5 97.1 70 - 13048.6 50.000 Isopropylbenzene 2.5 98.8 70 - 13049.4 50.000 Bromobenzene 2.5 101 70 - 13050.4 50.000 n-Propylbenzene 2.5 103 70 - 13051.3 50.000 2-Chlorotoluene 2.5 102 70 - 13050.9 50.000 4-Chlorotoluene 2.5 101 70 - 13050.5 50.000 1,3,5-Trimethylbenzene 2.5 101 70 - 13050.5 50.000 tert-Butylbenzene 2.5 103 70 - 13051.3 50.000 1,2,4-Trimethylbenzene 2.5 101 70 - 13050.3 50.000 sec-Butylbenzene 2.5 105 70 - 13052.6 50.000 1,3-Dichlorobenzene 2.5 94.0 70 - 13047.0 50.000 4-Isopropyltoluene 2.5 101 70 - 13050.7 50.000 1,4-Dichlorobenzene 2.5 97.2 70 - 13048.6 50.000 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 19 of 33 Project: NPU, Oakdale CET # : 6110625 Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes LCS (B6K2842-BS1) - Continued Prepared: 11/28/2016 Analyzed: 11/28/2016 1,2-Dichlorobenzene 2.5 102 70 - 13051.1 50.000 n-Butylbenzene 2.5 102 70 - 13051.2 50.000 1,2,4-Trichlorobenzene 2.5 98.0 70 - 13049.0 50.000 Hexachlorobutadiene 2.5 99.0 70 - 13049.5 50.000 Naphthalene 2.5 101 70 - 13050.4 50.000 1,2,3-Trichlorobenzene 2.5 101 70 - 13050.3 50.000 102 70 - 130Surrogate: 1,2-Dichloroethane-d4 99.5 70 - 130Surrogate: Toluene-d8 97.5 70 - 130Surrogate: 4-Bromofluorobenzene 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 20 of 33 Project: NPU, Oakdale CET # : 6110625 Batch B6K2907 - SM 2540 G Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(%) (%)Notes Duplicate (B6K2907-DUP1)Source: 6110625-03 Prepared: 11/29/2016 Analyzed: 11/29/2016 Percent Solids 1.0 78 0.869 579 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 21 of 33 Project: NPU, Oakdale CET # : 6110625 Batch B6K3017 - EPA 8260C Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes Blank (B6K3017-BLK1)Prepared: 11/29/2016 Analyzed: 11/29/2016 Dichlorodifluoromethane 7.5ND Chloromethane 5.0ND Vinyl Chloride 2.5ND Bromomethane 5.0ND Chloroethane 5.0ND Trichlorofluoromethane 20ND Acetone 75ND Acrylonitrile 4.0ND Trichlorotrifluoroethane 20ND 1,1-Dichloroethene 2.5ND Methylene Chloride 25ND Carbon Disulfide 5.0ND Methyl-t-Butyl Ether (MTBE)2.5ND trans-1,2-Dichloroethene 2.5ND 1,1-Dichloroethane 2.5ND 2-Butanone (MEK)13ND 2,2-Dichloropropane 2.5ND cis-1,2-Dichloroethene 2.5ND Chloroform 2.5ND Tetrahydrofuran 13ND 1,1,1-Trichloroethane 2.5ND Carbon Tetrachloride 2.5ND 1,1-Dichloropropene 2.5ND Benzene 2.5ND 1,2-Dichloroethane 2.5ND Trichloroethene 2.5ND 1,2-Dichloropropane 2.5ND Dibromomethane 2.5ND Bromodichloromethane 2.5ND Methyl Isobutyl Ketone 13ND cis-1,3-Dichloropropene 2.5ND Toluene 2.5ND trans-1,3-Dichloropropene 2.5ND 2-Hexanone 13ND 1,1,2-Trichloroethane 2.5ND Tetrachloroethene 2.5ND 1,3-Dichloropropane 2.5ND Dibromochloromethane 2.5ND 1,2-Dibromoethane 2.5ND trans-1,4-Dichloro-2-Butene 13ND Chlorobenzene 2.5ND 1,1,1,2-Tetrachloroethane 2.5ND Ethylbenzene 2.5ND m+p Xylenes 2.5ND o-Xylene 2.5ND Styrene 2.5ND Bromoform 2.5ND Isopropylbenzene 2.5ND 1,1,2,2-Tetrachloroethane 2.5ND Bromobenzene 2.5ND 1,2,3-Trichloropropane 2.5ND n-Propylbenzene 2.5ND 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 22 of 33 Project: NPU, Oakdale CET # : 6110625 Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes Blank (B6K3017-BLK1) - Continued Prepared: 11/29/2016 Analyzed: 11/29/2016 2-Chlorotoluene 2.5ND 4-Chlorotoluene 2.5ND 1,3,5-Trimethylbenzene 2.5ND tert-Butylbenzene 2.5ND 1,2,4-Trimethylbenzene 2.5ND sec-Butylbenzene 2.5ND 1,3-Dichlorobenzene 2.5ND 4-Isopropyltoluene 2.5ND 1,4-Dichlorobenzene 2.5ND 1,2-Dichlorobenzene 2.5ND n-Butylbenzene 2.5ND 1,2-Dibromo-3-Chloropropane 2.5ND 1,2,4-Trichlorobenzene 2.5ND Hexachlorobutadiene 2.5ND Naphthalene 2.5ND 1,2,3-Trichlorobenzene 2.5ND 109 70 - 130Surrogate: 1,2-Dichloroethane-d4 101 70 - 130Surrogate: Toluene-d8 104 70 - 130Surrogate: 4-Bromofluorobenzene LCS (B6K3017-BS1)Prepared: 11/29/2016 Analyzed: 11/29/2016 Dichlorodifluoromethane 7.5 109 70 - 13054.5 50.000 Chloromethane 5.0 99.3 70 - 13049.7 50.000 Vinyl Chloride 2.5 103 70 - 13051.3 50.000 Bromomethane 5.0 111 70 - 13055.4 50.000 Chloroethane 5.0 101 70 - 13050.4 50.000 Trichlorofluoromethane 20 102 70 - 13051.1 50.000 Acetone 75 81.1 70 - 13081.1 100.000 Acrylonitrile 4.0 101 70 - 13050.3 50.000 Trichlorotrifluoroethane 20 103 70 - 13051.3 50.000 1,1-Dichloroethene 2.5 99.0 70 - 13049.5 50.000 Methylene Chloride 25 73.8 70 - 13036.9 50.000 Carbon Disulfide 5.0 100 70 - 13050.0 50.000 Methyl-t-Butyl Ether (MTBE)2.5 94.9 70 - 13047.4 50.000 trans-1,2-Dichloroethene 2.5 100 70 - 13050.2 50.000 1,1-Dichloroethane 2.5 99.9 70 - 13050.0 50.000 2-Butanone (MEK)13 99.9 70 - 13099.9 100.000 2,2-Dichloropropane 2.5 99.6 70 - 13049.8 50.000 cis-1,2-Dichloroethene 2.5 99.8 70 - 13049.9 50.000 Chloroform 2.5 99.4 70 - 13049.7 50.000 Tetrahydrofuran 13 98.8 70 - 13049.4 50.000 1,1,1-Trichloroethane 2.5 103 70 - 13051.4 50.000 Carbon Tetrachloride 2.5 97.2 70 - 13048.6 50.000 1,1-Dichloropropene 2.5 102 70 - 13050.8 50.000 Benzene 2.5 100 70 - 13050.2 50.000 1,2-Dichloroethane 2.5 100 70 - 13050.2 50.000 Trichloroethene 2.5 99.7 70 - 13049.8 50.000 1,2-Dichloropropane 2.5 99.8 70 - 13049.9 50.000 Dibromomethane 2.5 100 70 - 13050.1 50.000 Bromodichloromethane 2.5 101 70 - 13050.4 50.000 Methyl Isobutyl Ketone 13 102 70 - 130102 100.000 cis-1,3-Dichloropropene 2.5 101 70 - 13050.4 50.000 Toluene 2.5 100 70 - 13050.0 50.000 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 23 of 33 Project: NPU, Oakdale CET # : 6110625 Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes LCS (B6K3017-BS1) - Continued Prepared: 11/29/2016 Analyzed: 11/29/2016 trans-1,3-Dichloropropene 2.5 101 70 - 13050.3 50.000 2-Hexanone 13 99.2 70 - 13099.2 100.000 1,1,2-Trichloroethane 2.5 99.5 70 - 13049.8 50.000 Tetrachloroethene 2.5 99.5 70 - 13049.8 50.000 1,3-Dichloropropane 2.5 99.9 70 - 13049.9 50.000 Dibromochloromethane 2.5 102 70 - 13050.9 50.000 1,2-Dibromoethane 2.5 100 70 - 13050.1 50.000 trans-1,4-Dichloro-2-Butene 13 103 70 - 13051.3 50.000 Chlorobenzene 2.5 99.7 70 - 13049.8 50.000 1,1,1,2-Tetrachloroethane 2.5 101 70 - 13050.6 50.000 Ethylbenzene 2.5 101 70 - 13050.6 50.000 m+p Xylenes 2.5 103 70 - 130103 100.000 o-Xylene 2.5 102 70 - 13050.9 50.000 Styrene 2.5 103 70 - 13051.4 50.000 Bromoform 2.5 102 70 - 13050.8 50.000 Isopropylbenzene 2.5 102 70 - 13051.1 50.000 1,1,2,2-Tetrachloroethane 2.5 102 70 - 13051.0 50.000 Bromobenzene 2.5 100 70 - 13050.1 50.000 1,2,3-Trichloropropane 2.5 99.9 70 - 13049.9 50.000 n-Propylbenzene 2.5 103 70 - 13051.5 50.000 2-Chlorotoluene 2.5 101 70 - 13050.5 50.000 4-Chlorotoluene 2.5 102 70 - 13051.0 50.000 1,3,5-Trimethylbenzene 2.5 102 70 - 13051.1 50.000 tert-Butylbenzene 2.5 101 70 - 13050.7 50.000 1,2,4-Trimethylbenzene 2.5 102 70 - 13050.9 50.000 sec-Butylbenzene 2.5 102 70 - 13051.2 50.000 1,3-Dichlorobenzene 2.5 101 70 - 13050.4 50.000 4-Isopropyltoluene 2.5 103 70 - 13051.7 50.000 1,4-Dichlorobenzene 2.5 99.7 70 - 13049.8 50.000 1,2-Dichlorobenzene 2.5 100 70 - 13050.2 50.000 n-Butylbenzene 2.5 103 70 - 13051.6 50.000 1,2-Dibromo-3-Chloropropane 2.5 101 70 - 13050.6 50.000 1,2,4-Trichlorobenzene 2.5 101 70 - 13050.7 50.000 Hexachlorobutadiene 2.5 99.9 70 - 13049.9 50.000 Naphthalene 2.5 104 70 - 13051.9 50.000 1,2,3-Trichlorobenzene 2.5 102 70 - 13050.9 50.000 98.0 70 - 130Surrogate: 1,2-Dichloroethane-d4 100 70 - 130Surrogate: Toluene-d8 100 70 - 130Surrogate: 4-Bromofluorobenzene 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 24 of 33 Project: NPU, Oakdale CET # : 6110625 Batch B6K3018 - EPA 8260C Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes Blank (B6K3018-BLK1)Prepared: 11/29/2016 Analyzed: 11/29/2016 Dichlorodifluoromethane 7.5ND Chloromethane 5.0ND Vinyl Chloride 2.5ND Bromomethane 5.0ND Chloroethane 5.0ND Trichlorofluoromethane 20ND Acetone 75ND Acrylonitrile 4.0ND Trichlorotrifluoroethane 20ND 1,1-Dichloroethene 2.5ND Methylene Chloride 25ND Carbon Disulfide 5.0ND Methyl-t-Butyl Ether (MTBE)2.5ND trans-1,2-Dichloroethene 2.5ND 1,1-Dichloroethane 2.5ND 2-Butanone (MEK)13ND 2,2-Dichloropropane 2.5ND cis-1,2-Dichloroethene 2.5ND Chloroform 2.5ND Tetrahydrofuran 13ND 1,1,1-Trichloroethane 2.5ND Carbon Tetrachloride 2.5ND 1,1-Dichloropropene 2.5ND Benzene 2.5ND 1,2-Dichloroethane 2.5ND Trichloroethene 2.5ND 1,2-Dichloropropane 2.5ND Dibromomethane 2.5ND Bromodichloromethane 2.5ND Methyl Isobutyl Ketone 13ND cis-1,3-Dichloropropene 2.5ND Toluene 2.5ND trans-1,3-Dichloropropene 2.5ND 2-Hexanone 13ND 1,1,2-Trichloroethane 2.5ND Tetrachloroethene 2.5ND 1,3-Dichloropropane 2.5ND Dibromochloromethane 2.5ND 1,2-Dibromoethane 2.5ND trans-1,4-Dichloro-2-Butene 13ND Chlorobenzene 2.5ND 1,1,1,2-Tetrachloroethane 2.5ND Ethylbenzene 2.5ND m+p Xylenes 2.5ND o-Xylene 2.5ND Styrene 2.5ND Bromoform 2.5ND Isopropylbenzene 2.5ND 1,1,2,2-Tetrachloroethane 2.5ND Bromobenzene 2.5ND 1,2,3-Trichloropropane 2.5ND n-Propylbenzene 2.5ND 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 25 of 33 Project: NPU, Oakdale CET # : 6110625 Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes Blank (B6K3018-BLK1) - Continued Prepared: 11/29/2016 Analyzed: 11/29/2016 2-Chlorotoluene 2.5ND 4-Chlorotoluene 2.5ND 1,3,5-Trimethylbenzene 2.5ND tert-Butylbenzene 2.5ND 1,2,4-Trimethylbenzene 2.5ND sec-Butylbenzene 2.5ND 1,3-Dichlorobenzene 2.5ND 4-Isopropyltoluene 2.5ND 1,4-Dichlorobenzene 2.5ND 1,2-Dichlorobenzene 2.5ND n-Butylbenzene 2.5ND 1,2-Dibromo-3-Chloropropane 2.5ND 1,2,4-Trichlorobenzene 2.5ND Hexachlorobutadiene 2.5ND Naphthalene 2.5ND 1,2,3-Trichlorobenzene 2.5ND 109 70 - 130Surrogate: 1,2-Dichloroethane-d4 101 70 - 130Surrogate: Toluene-d8 104 70 - 130Surrogate: 4-Bromofluorobenzene LCS (B6K3018-BS1)Prepared: 11/29/2016 Analyzed: 11/29/2016 Dichlorodifluoromethane 7.5 109 70 - 13054.5 50.000 Chloromethane 5.0 99.3 70 - 13049.7 50.000 Vinyl Chloride 2.5 103 70 - 13051.3 50.000 Bromomethane 5.0 111 70 - 13055.4 50.000 Chloroethane 5.0 101 70 - 13050.4 50.000 Trichlorofluoromethane 20 102 70 - 13051.1 50.000 Acetone 75 81.1 70 - 13081.1 100.000 Acrylonitrile 4.0 101 70 - 13050.3 50.000 Trichlorotrifluoroethane 20 103 70 - 13051.3 50.000 1,1-Dichloroethene 2.5 99.0 70 - 13049.5 50.000 Methylene Chloride 25 73.8 70 - 13036.9 50.000 Carbon Disulfide 5.0 100 70 - 13050.0 50.000 Methyl-t-Butyl Ether (MTBE)2.5 94.9 70 - 13047.4 50.000 trans-1,2-Dichloroethene 2.5 100 70 - 13050.2 50.000 1,1-Dichloroethane 2.5 99.9 70 - 13050.0 50.000 2-Butanone (MEK)13 99.9 70 - 13099.9 100.000 2,2-Dichloropropane 2.5 99.6 70 - 13049.8 50.000 cis-1,2-Dichloroethene 2.5 99.8 70 - 13049.9 50.000 Chloroform 2.5 99.4 70 - 13049.7 50.000 Tetrahydrofuran 13 98.8 70 - 13049.4 50.000 1,1,1-Trichloroethane 2.5 103 70 - 13051.4 50.000 Carbon Tetrachloride 2.5 97.2 70 - 13048.6 50.000 1,1-Dichloropropene 2.5 102 70 - 13050.8 50.000 Benzene 2.5 100 70 - 13050.2 50.000 1,2-Dichloroethane 2.5 100 70 - 13050.2 50.000 Trichloroethene 2.5 99.7 70 - 13049.8 50.000 1,2-Dichloropropane 2.5 99.8 70 - 13049.9 50.000 Dibromomethane 2.5 100 70 - 13050.1 50.000 Bromodichloromethane 2.5 101 70 - 13050.4 50.000 Methyl Isobutyl Ketone 13 102 70 - 130102 100.000 cis-1,3-Dichloropropene 2.5 101 70 - 13050.4 50.000 Toluene 2.5 100 70 - 13050.0 50.000 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 26 of 33 Project: NPU, Oakdale CET # : 6110625 Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes LCS (B6K3018-BS1) - Continued Prepared: 11/29/2016 Analyzed: 11/29/2016 trans-1,3-Dichloropropene 2.5 101 70 - 13050.3 50.000 2-Hexanone 13 99.2 70 - 13099.2 100.000 1,1,2-Trichloroethane 2.5 99.5 70 - 13049.8 50.000 Tetrachloroethene 2.5 99.5 70 - 13049.8 50.000 1,3-Dichloropropane 2.5 99.9 70 - 13049.9 50.000 Dibromochloromethane 2.5 102 70 - 13050.9 50.000 1,2-Dibromoethane 2.5 100 70 - 13050.1 50.000 trans-1,4-Dichloro-2-Butene 13 103 70 - 13051.3 50.000 Chlorobenzene 2.5 99.7 70 - 13049.8 50.000 1,1,1,2-Tetrachloroethane 2.5 101 70 - 13050.6 50.000 Ethylbenzene 2.5 101 70 - 13050.6 50.000 m+p Xylenes 2.5 103 70 - 130103 100.000 o-Xylene 2.5 102 70 - 13050.9 50.000 Styrene 2.5 103 70 - 13051.4 50.000 Bromoform 2.5 102 70 - 13050.8 50.000 Isopropylbenzene 2.5 102 70 - 13051.1 50.000 1,1,2,2-Tetrachloroethane 2.5 102 70 - 13051.0 50.000 Bromobenzene 2.5 100 70 - 13050.1 50.000 1,2,3-Trichloropropane 2.5 99.9 70 - 13049.9 50.000 n-Propylbenzene 2.5 103 70 - 13051.5 50.000 2-Chlorotoluene 2.5 101 70 - 13050.5 50.000 4-Chlorotoluene 2.5 102 70 - 13051.0 50.000 1,3,5-Trimethylbenzene 2.5 102 70 - 13051.1 50.000 tert-Butylbenzene 2.5 101 70 - 13050.7 50.000 1,2,4-Trimethylbenzene 2.5 102 70 - 13050.9 50.000 sec-Butylbenzene 2.5 102 70 - 13051.2 50.000 1,3-Dichlorobenzene 2.5 101 70 - 13050.4 50.000 4-Isopropyltoluene 2.5 103 70 - 13051.7 50.000 1,4-Dichlorobenzene 2.5 99.7 70 - 13049.8 50.000 1,2-Dichlorobenzene 2.5 100 70 - 13050.2 50.000 n-Butylbenzene 2.5 103 70 - 13051.6 50.000 1,2-Dibromo-3-Chloropropane 2.5 101 70 - 13050.6 50.000 1,2,4-Trichlorobenzene 2.5 101 70 - 13050.7 50.000 Hexachlorobutadiene 2.5 99.9 70 - 13049.9 50.000 Naphthalene 2.5 104 70 - 13051.9 50.000 1,2,3-Trichlorobenzene 2.5 102 70 - 13050.9 50.000 98.0 70 - 130Surrogate: 1,2-Dichloroethane-d4 100 70 - 130Surrogate: Toluene-d8 100 70 - 130Surrogate: 4-Bromofluorobenzene 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 27 of 33 Project: NPU, Oakdale CET # : 6110625 Quality Control Definitions and Abbreviations 80 Lupes Drive Stratford, CT 06615 Internal Standard (IS)An Analyte added to each sample or sample extract. An internal standard is used to monitor retention time, calculate relative response, and quantify analytes of interest. Surrogate Recovery The % recovery for non-target organic compounds that are spiked into all samples. Used to determine method performance. Continuing Calibration An analytical standard analyzed with each set of samples to verify initial calibration of the system. Batch Samples that are analyzed together with the same method, sequence and lot of reagents within the same time period. ND Not detected RL Reporting Limit Dilution Multiplier added to detection levels (MDL) and/or sample results due to interferences and/or high concentration of target compounds. Duplicate Result from the duplicate analysis of a sample. Result Amount of analyte found in a sample. Spike Level Amount of analyte added to a sample Matrix Spike Result Amount of analyte found including amount that was spiked. Matrix Spike Dup Amount of analyte found in duplicate spikes including amount that was spike. Matrix Spike % Recovery % Recovery of spiked amount in sample. Matrix Spike Dup % Recovery % Recovery of spiked duplicate amount in sample. RPD Relative percent difference between Matrix Spike and Matrix Spike Duplicate. Blank Method Blank that has been taken through all steps of the analysis. LCS % Recovery Laboratory Control Sample percent recovery. The amount of analyte recovered from a fortified sample. Recovery Limits A range within which specified measurements results must fall to be compliant. CC Calibration Verification Flags: H-Recovery is above the control limits L-Recovery is below the control limits B-Compound detected in the Blank P-RPD of dual column results exceeds 40% #-Sample result too high for accurate spike recovery. Connecticut Laboratory Certification PH0116 New York Certification 11982 Massachussets Laboratory Certification M-CT903 Rhode Island Certification 199 Tel: (203) 377-9984 Fax: (203) 377-9952 email: cet1@cetlabs.com 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 28 of 33 Project: NPU, Oakdale CET # : 6110625 Revision: Original report dated 12/01/2016, changed sample depths from ft to inches for Sample 6110625-01 and 625-02 due to reporting error. CASE NARRATIVE 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 29 of 33 Project: NPU, Oakdale CET # : 6110625 Report Comments: Questions related to this report should be directed to David Ditta, Timothy Fusco, or Robert Blake at 203-377-9984. Sincerely, David Ditta Laboratory Director Sample Result Flags: E- The result is estimated, above the calibration range. H- The surrogate recovery is above the control limits. L- The surrogate recovery is below the control limits. B- The compound was detected in the laboratory blank. P- The Relative Percent Difference (RPD) of dual column analyses exceeds 40%. D- The RPD between the sample and the sample duplicate is high. Sample homogeneity may be a problem. +- The Surrogate was diluted out. *C1- The Continuing Calibration did not meet method specifications and was biased low for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased low. *C2- The Continuing Calibration did not meet method specifications and was biased high for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased high. *F1- The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the low side. *F2- The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the high side. I- The Analyte exceeds %RSD limits for the Initial Calibration. This is a non-directional bias. All results met standard operating procedures unless indicated by a data qualifier next to a sample result, or a narration in the QC report. Complete Environmental Testing is only responsible for the certified testing and is not directly responsible for the integrity of the sample before laboratory receipt. ND is None Detected at the specified detection limit All analyses were performed in house unless a Reference Laboratory is listed. Samples will be disposed of 30 days after the report date. 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 30 of 33 Project: NPU, Oakdale CET # : 6110625 CertificationsAnalyte CERTIFICATIONS Certified Analyses included in this Report CT-ETPH in Soil CTETPH CT-ETPH in Water CTETPH EPA 8260C in Soil CT,NYMethyl-t-Butyl Ether (MTBE) CT,NYBenzene CT,NYToluene CT,NYChlorobenzene CT,NYEthylbenzene CT,NYm+p Xylenes CT,NYo-Xylene CT,NYStyrene CT,NYIsopropylbenzene CT,NYBromobenzene CT,NYn-Propylbenzene CT,NY2-Chlorotoluene CT,NY4-Chlorotoluene CT,NY1,3,5-Trimethylbenzene CT,NYtert-Butylbenzene CT,NY1,2,4-Trimethylbenzene CT,NYsec-Butylbenzene CT,NY1,3-Dichlorobenzene CT,NY4-Isopropyltoluene CT,NY1,4-Dichlorobenzene CT,NY1,2-Dichlorobenzene CT,NYn-Butylbenzene CT,NY1,2,4-Trichlorobenzene CT,NYHexachlorobutadiene CT,NYNaphthalene CT1,2,3-Trichlorobenzene EPA 8260C in Water CT,NYMethyl-t-Butyl Ether (MTBE) CT,NYBenzene CT,NYToluene CT,NYChlorobenzene CT,NYEthylbenzene CT,NYm+p Xylenes CT,NYo-Xylene CT,NYStyrene CT,NYIsopropylbenzene CTBromobenzene CT,NYn-Propylbenzene CT,NY2-Chlorotoluene 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 31 of 33 Project: NPU, Oakdale CET # : 6110625 CertificationsAnalyte CERTIFICATIONS Certified Analyses included in this Report EPA 8260C in Water CT,NY4-Chlorotoluene CT,NY1,3,5-Trimethylbenzene CT,NYtert-Butylbenzene CT,NY1,2,4-Trimethylbenzene CT,NYsec-Butylbenzene CT,NY1,3-Dichlorobenzene CT,NY4-Isopropyltoluene CT,NY1,4-Dichlorobenzene CT,NY1,2-Dichlorobenzene CT,NYn-Butylbenzene CT,NY1,2,4-Trichlorobenzene CT,NYHexachlorobutadiene CT,NYNaphthalene CT1,2,3-Trichlorobenzene Complete Environmental Testing operates under the following certifications and accreditations: Code Description Number Expires Connecticut Public Health 09/30/2018CTPH0116 New York Certification (NELAC)04/01/2017NY11982 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 32 of 33 Page 33 of 33 Soil Disposal Information Ron SwaneyNPU; Generators On Demand 260 Cherry Lane Oakdale CT 06370 860 662 4090 Same SES Inc Donald Fortunato 61 Plants Dam Rd 860 739 6691 East Lyme CT 06333 250 180 Commercial Construction Group & Generators On Demand Ron Swaney 61-1 Buttonball Rd Old Lyme CT 06371 860 662 4090 VI.DESCRIPTION OF THE PCS: ______Sand _______ Gravel _______ Fill ______ Clay _________ Other Physical description of the PCS – In addition please indicate the presence of any construction debris, veg. matter, ash, etc. Specify type of contamination: ________Gasoline _________Diesel _________#2 __________#4 _________#6 ________Lub. Oil _________Waste Oil __________Jet Fuel _________Kerosene __________Other:___________________ VII.SITE HISTORY: Please include at a minimum the following information: Current & Former usage of site, description of release (known dates, source), sampling method used (grab, composite, etc.), analytical parameters selected and any other pertinent information. ** Sufficient information must be provided in the Site History to justify the limiting of the analytical requirements necessary for recycling.** VIII.Please forward a diagram which includes the following information: At least one street reference, any adjacent structures, excavation area, stockpile location, location where samples were taken from, name of individual preparing diagram, reference the site name and location and any other pertinent information. IX.GENERATOR / LSP / QEP STATEMENTS: a.I, the generator/LSP/QEP, using due diligence have determined that there is no reason to Suspect or believe the PCS has been impacted by any release of oil or hazardous materials other than that of the known source or I have identified the additional oil and hazardous materials that are suspected or known to be present in the PCS, in addition to those associated with the known release including any anthropogenetic contaminates. b.I, the generator/LSP/QEP, realize that due diligence shall consist of a search of information and records reasonably available to the generator of the PCS sufficient to make the determination. Such records and information may include, but are not limited to, those of the generator, location of the generation (Facility if not the generator) the Department Bureau of Waste Site Cleanup, and the municipality (Board of Health, Fire Department) within which the site is located. msr.doc.doc • 11/01 Material Shipping Record and Log • Page 2 of 6 Massachusetts Department of Environmental Protection Bureau of Waste PreventionMaterial Shipping Record & Log For the shipment of contaminated soil, urban fill, and dredgematerials not subject to management under section 310 CMR 40.0035nor manifesting under 310 CMR 30.000 Tracking Number D. Transporter/Common Carrier Information 1. Provide the following information: Transporter/Common carrier name Hazardous waste license number (if applicable)Licensing state (if applicable) Contact person Title Street City/Town State Zip code Telephone number Ext. E. Receiving Facility Information 1. Provide the following information on the receiving facility: Operator/Facility name Contact person Title Street City/Town State Zip code Telephone number Ext. 2. Type of facility: asphalt batch/cold mix asphalt batch/hot mix landfill/disposal landfill/ daily cover thermal processing landfill/structural fill other(specify): 3. Permit number: Ondrick Materials and Recycling, LLC David S. Costanzo Operations and Sales Manager 58 Industry Road Chicopee MA 01020 413592-2566 X258844 "~-.flG /"" o ff 0 4\o (\ey::;::6,-6 ,',I 257,8bINV. o<0 ""I .---. \ \ \ !---- .,.,>'>----~ R PADRM[NSFO URE'ETE TRA ENCLOS PAD OUTDOO~ONCR[7EVSET ON 4400 -~ G-rr#~--- 1-AI/) 2- -AI])s _AID if -tIJ) 5" .-/If]) t -jV7J '7 -#7) '6"-/II]) 7 -#7) L-a7~ ,v t;l# ",--- / -:t--~I.i.J (:)/'. ~ 18"RCP1nv=255.40 \ IJ~O'RIPRAP SPLA'sH PAD (DEPTH=f'Z. FLARED END UNIT INV 260.0 1, ~86lf-T8"RCP S=f.OX 10 -/tf']) )/-AI]) l~-/5t/jJl'· i p-/tiP )'-/- /II]) 15-;VlJ / \\>tt? /.1° ~_----.--1..•''V - \'?a·~~~~~-in'~~~~_..__1 \~.~\\ £PTH=I.S,) I v -,~:: &l'-' 84LF-18"R . 5=7.5 /~ ------~I I!U;)~ ~ ~ \ o\ <:)<:) <, 65'x /00'BUiLDING FF£=262.00 /1'£=25/.00 FF ~ Elev=260A <, o ETPH 80 Lupes Drive Stratford, CT 06615 Tel: (203) 377-9984 Fax: (203) 377-9952 e-mail: cet1@cetlabs.com Client:Mr. Don Fortunato Soil & Environmental Service 61 Plants Dam Road East Lyme, CT 06333 Analytical Report CET# 6100211 Report Date:October 12, 2016 Project: NPU Stony Brook, Montville Rhode Island Certification: 199Massachusetts laboratory Certificate: M-CT903 Connecticut Laboratory Certificate: PH 0116 New York Certification: 11982 Page 1 of 12 Project: NPU Stony Brook, Montville CET # : 6100211 Sample ID Laboratory ID Matrix Collection Date/Time Receipt Date SAMPLE SUMMARY The sample(s) were received at 2.5 C. This report contains analytical data associated with following samples only. 25 B 6100211-01 Soil 10/10/201610/07/2016 26 B 6100211-02 Soil 10/10/201610/07/2016 29 B 6100211-03 Soil 10/10/201610/07/2016 30 B 6100211-04 Soil 10/10/201610/07/2016 31 B 6100211-05 Soil 10/10/201610/07/2016 Notes Date/Time AnalyzedPreparedBatchDilutionRLResultLaboratory ID Client Sample ID Units Analyst: PB Matrix: Soil Analyte: Total Solids [EPA 160.3 modified] 78 10/11/2016 10/11/2016 14:466100211-01 %25 B 1.0 1 B6J1109 75 10/11/2016 10/11/2016 14:466100211-02 %26 B 1.0 1 B6J1109 91 10/11/2016 10/11/2016 14:466100211-03 %29 B 1.0 1 B6J1109 74 10/11/2016 10/11/2016 14:466100211-04 %30 B 1.0 1 B6J1109 93 10/11/2016 10/11/2016 14:466100211-05 %31 B 1.0 1 B6J1109 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 2 of 12 Project: NPU Stony Brook, Montville CET # : 6100211 Client Sample ID 25 B Lab ID: 6100211-01 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH ND 1 B6J1127 10/11/2016 10/12/2016 01:2664EPA 3550C *F1 Surrogate: Octacosane 82.9 %10/11/2016 10/12/2016 01:26B6J112750 - 150 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8270D Matrix: Soil Analyst: ALBSemivolatile Organics Naphthalene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A 2-Methyl Naphthalene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Acenaphthylene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Acenaphthene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Fluorene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Phenanthrene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Anthracene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Fluoranthene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Pyrene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Benzo[a]anthracene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Chrysene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Benzo[b]fluoranthene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Benzo[k]fluoranthene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Benzo[a]pyrene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Indeno[1,2,3-cd]pyrene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Dibenz[a,h]anthracene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Benzo[g,h,i]perylene ND 0.968 B6J1121 10/11/2016 10/12/2016 10:50370EPA 3545A Surrogate: Nitrobenzene-d5 38.9 %10/11/2016 10/12/2016 10:50B6J112130 - 130 Surrogate: 2-Fluorobiphenyl 36.1 %10/11/2016 10/12/2016 10:50B6J112130 - 130 Surrogate: Terphenyl-d14 52.3 %10/11/2016 10/12/2016 10:50B6J112130 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 3 of 12 Project: NPU Stony Brook, Montville CET # : 6100211 Client Sample ID 26 B Lab ID: 6100211-02 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH 5400 1 B6J1127 10/11/2016 10/12/2016 03:0166EPA 3550C 2*F1 Surrogate: Octacosane 84.5 %10/11/2016 10/12/2016 03:01B6J112750 - 150 2 C9-C28 Fuel Oil Range Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8270D Matrix: Soil Analyst: ALBSemivolatile Organics Naphthalene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A 2-Methyl Naphthalene 7300 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Acenaphthylene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Acenaphthene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Fluorene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Phenanthrene 1000 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Anthracene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Fluoranthene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Pyrene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Benzo[a]anthracene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Chrysene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Benzo[b]fluoranthene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Benzo[k]fluoranthene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Benzo[a]pyrene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Indeno[1,2,3-cd]pyrene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Dibenz[a,h]anthracene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Benzo[g,h,i]perylene ND 0.977 B6J1121 10/11/2016 10/12/2016 15:07390EPA 3545A Surrogate: Nitrobenzene-d5 64.9 %10/11/2016 10/12/2016 15:07B6J112130 - 130 Surrogate: 2-Fluorobiphenyl 86.4 %10/11/2016 10/12/2016 15:07B6J112130 - 130 Surrogate: Terphenyl-d14 88.0 %10/11/2016 10/12/2016 15:07B6J112130 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 4 of 12 Project: NPU Stony Brook, Montville CET # : 6100211 Client Sample ID 29 B Lab ID: 6100211-03 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH 760 1 B6J1127 10/11/2016 10/12/2016 03:2555EPA 3550C 2*F1 Surrogate: Octacosane 88.4 %10/11/2016 10/12/2016 03:25B6J112750 - 150 2 C9-C28 Fuel Oil Range Client Sample ID 30 B Lab ID: 6100211-04 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH 3100 1 B6J1127 10/11/2016 10/12/2016 03:4867EPA 3550C 2*F1 Surrogate: Octacosane 80.3 %10/11/2016 10/12/2016 03:48B6J112750 - 150 2 C9-C28 Fuel Oil Range 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 5 of 12 Project: NPU Stony Brook, Montville CET # : 6100211 Client Sample ID 31 B Lab ID: 6100211-05 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH 18000 1 B6J1127 10/11/2016 10/12/2016 04:1254EPA 3550C 2*F1 Surrogate: Octacosane 85.5 %10/11/2016 10/12/2016 04:12B6J112750 - 150 2 C9-C28 Fuel Oil Range 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 6 of 12 Project: NPU Stony Brook, Montville CET # : 6100211 QUALITY CONTROL SECTION Batch B6J1121 - EPA 8270D Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg)(ug/kg)Notes Blank (B6J1121-BLK1)Prepared: 10/11/2016 Analyzed: 10/12/2016 Naphthalene 300ND 2-Methyl Naphthalene 300ND Acenaphthylene 300ND Acenaphthene 300ND Fluorene 300ND Phenanthrene 300ND Anthracene 300ND Fluoranthene 300ND Pyrene 300ND Benzo[a]anthracene 300ND Chrysene 300ND Benzo[b]fluoranthene 300ND Benzo[k]fluoranthene 300ND Benzo[a]pyrene 300ND Indeno[1,2,3-cd]pyrene 300ND Dibenz[a,h]anthracene 300ND Benzo[g,h,i]perylene 300ND 60.2 30 - 130Surrogate: Nitrobenzene-d5 65.1 30 - 130Surrogate: 2-Fluorobiphenyl 82.7 30 - 130Surrogate: Terphenyl-d14 LCS (B6J1121-BS1)Prepared: 10/11/2016 Analyzed: 10/12/2016 Naphthalene 300 63.1 40 - 1402530 4,000.000 2-Methyl Naphthalene 300 63.4 40 - 1402540 4,000.000 Acenaphthylene 300 62.6 40 - 1402500 4,000.000 Acenaphthene 300 68.9 40 - 1402760 4,000.000 Fluorene 300 71.2 40 - 1402850 4,000.000 Phenanthrene 300 76.0 40 - 1403040 4,000.000 Anthracene 300 76.1 40 - 1403040 4,000.000 Fluoranthene 300 74.9 40 - 1403000 4,000.000 Pyrene 300 75.4 40 - 1403020 4,000.000 Benzo[a]anthracene 300 81.5 40 - 1403260 4,000.000 Chrysene 300 80.3 40 - 1403210 4,000.000 Benzo[b]fluoranthene 300 92.0 40 - 1403680 4,000.000 Benzo[k]fluoranthene 300 105 40 - 1404200 4,000.000 Benzo[a]pyrene 300 101 40 - 1404050 4,000.000 Indeno[1,2,3-cd]pyrene 300 105 40 - 1404220 4,000.000 Dibenz[a,h]anthracene 300 113 40 - 1404540 4,000.000 Benzo[g,h,i]perylene 300 93.8 40 - 1403750 4,000.000 62.7 30 - 130Surrogate: Nitrobenzene-d5 67.6 30 - 130Surrogate: 2-Fluorobiphenyl 81.3 30 - 130Surrogate: Terphenyl-d14 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 7 of 12 Project: NPU Stony Brook, Montville CET # : 6100211 Report Comments: Questions related to this report should be directed to David Ditta, Timothy Fusco, or Robert Blake at 203-377-9984. Sincerely, David Ditta Laboratory Director Sample Result Flags: E- The result is estimated, above the calibration range. H- The surrogate recovery is above the control limits. L- The surrogate recovery is below the control limits. B- The compound was detected in the laboratory blank. P-The Relative Percent Difference (RPD) of dual column analyses exceeds 40%. D- The RPD between the sample and the sample duplicate is high. Sample homogeneity may be a problem. +- The Surrogate was diluted out. *C1- The Continuing Calibration did not meet method specifications and was biased low for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased low. *C2- The Continuing Calibration did not meet method specifications and was biased high for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased high. *F1- The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the low side. *F2- The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the high side. I-The Analyte exceeds %RSD limits for the Initial Calibration. This is a non-directional bias. All results met standard operating procedures unless indicated by a data qualifier next to a sample result, or a narration in the QC report. Complete Environmental Testing is only responsible for the certified testing and is not directly responsible for the integrity of the sample before laboratory receipt. ND is None Detected at the specified detection limit All analyses were performed in house unless a Reference Laboratory is listed. Samples will be disposed of 30 days after the report date. 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 10 of 12 Page 12 of 12 80 Lupes Drive Stratford, CT 06615 Tel: (203) 377-9984 Fax: (203) 377-9952 e-mail: cet1@cetlabs.com Client:Mr. Don Fortunato Soil & Environmental Service 61 Plants Dam Road East Lyme, CT 06333 Analytical Report CET# 6100217 Report Date:October 18, 2016 Project: NPU Stony Brook, Montville Rhode Island Certification: 199Massachusetts laboratory Certificate: M-CT903 Connecticut Laboratory Certificate: PH 0116 New York Certification: 11982 Page 1 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Sample ID Laboratory ID Matrix Collection Date/Time Receipt Date SAMPLE SUMMARY The sample(s) were received at 2.5 C. This report contains analytical data associated with following samples only. Waste 1 6100217-01 Soil 10/10/201616:0010/07/2016 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 2 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Notes Date/Time AnalyzedPreparedBatchDilutionRLResultLaboratory ID Client Sample ID Units Analyst: MRH Matrix: Soil Analyte: Percent Solids [SM 2540 G] 79 10/12/2016 10/14/2016 10:006100217-01 %Waste 1 1.0 1 B6J1205 Notes Date/Time AnalyzedPreparedBatchDilutionRLResultLaboratory ID Client Sample ID Units Analyst: JF Matrix: Soil Analyte: Flashpoint [EPA 1010A] >200 F 10/13/2016 10/13/2016 10:226100217-01 FWaste 1 NA 1 B6J1309 Notes Date/Time AnalyzedPreparedBatchDilutionRLResultLaboratory ID Client Sample ID Units Analyst: JZ Matrix: Soil Analyte: Reactive Sulfide [SW 846 Ch. 7] ND 10/17/2016 10/17/2016 09:466100217-01 mg/kg dryWaste 1 25 1 B6J1706 Notes Date/Time AnalyzedPreparedBatchDilutionRLResultLaboratory ID Client Sample ID Units Analyst: JZ Matrix: Soil Analyte: Reactive Cyanide [SW 846 Ch. 7] ND 10/17/2016 10/17/2016 09:466100217-01 mg/kg dryWaste 1 6.3 1 B6J1706 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 3 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Notes Date/Time AnalyzedPreparedBatchDilutionRLResultLaboratory ID Client Sample ID Units Analyst: KP Matrix: Soil Analyte: pH [EPA 9045D] 6.32 10/11/2016 10/11/2016 16:386100217-01 pH UnitsWaste 1 NA 1 B6J1124 Notes Date/Time AnalyzedPreparedBatchDilutionRLResultLaboratory ID Client Sample ID Units Analyst: KP Matrix: Soil Analyte: Mercury [EPA 7471B] ND 10/12/2016 10/17/2016 15:476100217-01 mg/kg dryWaste 1 0.25 1 B6J1212 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 4 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Client Sample ID Waste 1 Lab ID: 6100217-01 Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: EPA 6010C Matrix: Soil Analyst: SSTotal Metals Lead 6.3 1 B6J1404 10/14/2016 10/17/2016 16:302.5 EPA 3050B Selenium ND 1 B6J1404 10/14/2016 10/17/2016 16:301.3 EPA 3050B Cadmium ND 1 B6J1404 10/14/2016 10/17/2016 16:300.63 EPA 3050B Chromium 17 1 B6J1404 10/14/2016 10/17/2016 16:302.5 EPA 3050B Arsenic 7.0 1 B6J1404 10/14/2016 10/17/2016 16:301.3 EPA 3050B Barium 49 1 B6J1404 10/14/2016 10/17/2016 16:302.5 EPA 3050B Silver ND 1 B6J1404 10/14/2016 10/17/2016 16:302.5 EPA 3050B Notes Date/Time AnalyzedPreparedBatchDilution RL (mg/kg dry) Result (mg/kg dry)Analyte Prep Method Method: CT-ETPH Matrix: Soil Analyst: MHConn. Extractable TPH ETPH 5200 1 B6J1342 10/13/2016 10/14/2016 01:3363EPA 3550C 2*F1 Surrogate: Octacosane 93.2 %10/13/2016 10/14/2016 01:33B6J134250 - 150 2 C9-C28 Fuel Oil Range Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8270D Matrix: Soil Analyst: ALBSemivolatile Organics Phenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 1,3-Dichlorobenzene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A n-Nitroso-di-n-propylamine ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Pyridine ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A *C2 n-Nitroso-dimethylamine ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A bis(2-Chloroethyl)ether ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 5 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Client Sample ID Waste 1 Lab ID: 6100217-01 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8270D Matrix: Soil Analyst: ALBSemivolatile Organics Aniline ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2-Chlorophenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 1,4-Dichlorobenzene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Benzyl Alcohol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 1,2-Dichlorobenzene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A bis(2-Chloroisopropyl)ether ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Hexachloroethane ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2-Methyl Phenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 3+4 Methyl Phenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Naphthalene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2-Nitrophenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2,4-Dichlorophenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Hexachlorobutadiene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 4-Chloro-3-methylphenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Nitrobenzene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Isophorone ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2,4-Dimethylphenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A bis(2-Chloroethoxy)methane ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Benzoic Acid ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 1,2,4-Trichlorobenzene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2,6-Dichlorophenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 4-Chloroaniline ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 1,2,4,5-Tetrachlorobenzene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2-Methyl Naphthalene 9700 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Acenaphthylene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Acenaphthene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Dibenzofuran ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Fluorene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Hexachlorocyclopentadiene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A *F1*C1 2,4,6-Trichlorophenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2,4,5-Trichlorophenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2,4-Dinitrophenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A *F1*C1 4-Nitrophenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2-Chloronaphthalene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2-Nitroaniline ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Dimethylphthalate ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2,6-Dinitrotoluene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 4-Nitroaniline ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2,4-Dinitrotoluene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 2,3,4,6-Tetrachlorophenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 4-Chlorophenyl-phenylether ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 6 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Client Sample ID Waste 1 Lab ID: 6100217-01 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8270D Matrix: Soil Analyst: ALBSemivolatile Organics Diethylphthalate ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Phenanthrene 1400 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Anthracene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Carbazole ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Fluoranthene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Pyrene 540 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A n-Nitrosodiphenylamine ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Pentachlorophenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 3-Nitroaniline ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 4,6-Dinitro-2-methylphenol ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A *C1 1,2-Diphenylhydrazine ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 4-Bromophenyl-phenylether ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Hexachlorobenzene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Di-n-butylphthalate ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Pentachloronitrobenzene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Benzo[a]anthracene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Chrysene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Butylbenzylphthalate ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A 3,3-Dichlorobenzidine ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A *F1 bis(2-Ethylhexyl)phthalate ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Di-n-octylphthalate ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Benzo[b]fluoranthene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Benzo[k]fluoranthene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Benzo[a]pyrene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Indeno[1,2,3-cd]pyrene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Dibenz[a,h]anthracene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Benzo[g,h,i]perylene ND 0.931 B6J1121 10/11/2016 10/12/2016 20:05350EPA 3545A Surrogate: 2-Fluorophenol 59.6 %10/11/2016 10/12/2016 20:05B6J112130 - 130 Surrogate: Phenol-d6 60.9 %10/11/2016 10/12/2016 20:05B6J112130 - 130 Surrogate: Nitrobenzene-d5 61.4 %10/11/2016 10/12/2016 20:05B6J112130 - 130 Surrogate: 2-Fluorobiphenyl 108 %10/11/2016 10/12/2016 20:05B6J112130 - 130 Surrogate: 2,4,6-Tribromophenol 86.0 %10/11/2016 10/12/2016 20:05B6J112130 - 130 Surrogate: Terphenyl-d14 110 %10/11/2016 10/12/2016 20:05B6J112130 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 7 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Client Sample ID Waste 1 Lab ID: 6100217-01 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics Dichlorodifluoromethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:543600EPA 5035A-H *C1 Chloromethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:542400EPA 5035A-H *C1 Vinyl Chloride ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H *C1 Bromomethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:542400EPA 5035A-H Chloroethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:542400EPA 5035A-H Trichlorofluoromethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:549600EPA 5035A-H Acetone ND 379.51 B6J1719 10/17/2016 10/17/2016 14:5436000EPA 5035A-H Acrylonitrile ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541900EPA 5035A-H Trichlorotrifluoroethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:549600EPA 5035A-H 1,1-Dichloroethene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H *C2 Methylene Chloride ND 379.51 B6J1719 10/17/2016 10/17/2016 14:5412000EPA 5035A-H Carbon Disulfide ND 379.51 B6J1719 10/17/2016 10/17/2016 14:542400EPA 5035A-H *C2 Methyl-t-Butyl Ether (MTBE)ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H trans-1,2-Dichloroethene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,1-Dichloroethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 2-Butanone (MEK)ND 379.51 B6J1719 10/17/2016 10/17/2016 14:546000EPA 5035A-H 2,2-Dichloropropane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H cis-1,2-Dichloroethene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Chloroform ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Tetrahydrofuran ND 379.51 B6J1719 10/17/2016 10/17/2016 14:546000EPA 5035A-H 1,1,1-Trichloroethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Carbon Tetrachloride ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H *C2 1,1-Dichloropropene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Benzene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,2-Dichloroethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Trichloroethene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,2-Dichloropropane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Dibromomethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Bromodichloromethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Methyl Isobutyl Ketone ND 379.51 B6J1719 10/17/2016 10/17/2016 14:546000EPA 5035A-H cis-1,3-Dichloropropene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Toluene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H trans-1,3-Dichloropropene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 2-Hexanone ND 379.51 B6J1719 10/17/2016 10/17/2016 14:546000EPA 5035A-H 1,1,2-Trichloroethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Tetrachloroethene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,3-Dichloropropane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Dibromochloromethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,2-Dibromoethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H trans-1,4-Dichloro-2-Butene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:546000EPA 5035A-H Chlorobenzene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 8 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Client Sample ID Waste 1 Lab ID: 6100217-01 Notes Date/Time AnalyzedPreparedBatchDilution RL (ug/kg dry) Result (ug/kg dry)Analyte Prep Method Method: EPA 8260C Matrix: Soil Analyst: DAHVolatile Organics 1,1,1,2-Tetrachloroethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Ethylbenzene 3500 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H m+p Xylenes 16000 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H o-Xylene 13000 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Styrene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Bromoform ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Isopropylbenzene 1700 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,1,2,2-Tetrachloroethane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Bromobenzene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,2,3-Trichloropropane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H n-Propylbenzene 6000 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 2-Chlorotoluene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 4-Chlorotoluene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,3,5-Trimethylbenzene 18000 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H tert-Butylbenzene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,2,4-Trimethylbenzene 38000 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H sec-Butylbenzene 3500 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,3-Dichlorobenzene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 4-Isopropyltoluene 2400 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,4-Dichlorobenzene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,2-Dichlorobenzene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H n-Butylbenzene 7100 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,2-Dibromo-3-Chloropropane ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,2,4-Trichlorobenzene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Hexachlorobutadiene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Naphthalene 4400 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H 1,2,3-Trichlorobenzene ND 379.51 B6J1719 10/17/2016 10/17/2016 14:541200EPA 5035A-H Surrogate: 1,2-Dichloroethane-d4 109 %10/17/2016 10/17/2016 14:54B6J171970 - 130 Surrogate: Toluene-d8 101 %10/17/2016 10/17/2016 14:54B6J171970 - 130 Surrogate: 4-Bromofluorobenzene 99.5 %10/17/2016 10/17/2016 14:54B6J171970 - 130 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 9 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 QUALITY CONTROL SECTION Batch B6J1121 - EPA 8270D Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes Blank (B6J1121-BLK1)Prepared: 10/11/2016 Analyzed: 10/12/2016 Phenol 300ND 1,3-Dichlorobenzene 300ND n-Nitroso-di-n-propylamine 300ND Pyridine 300ND n-Nitroso-dimethylamine 300ND bis(2-Chloroethyl)ether 300ND Aniline 300ND 2-Chlorophenol 300ND 1,4-Dichlorobenzene 300ND Benzyl Alcohol 300ND 1,2-Dichlorobenzene 300ND bis(2-Chloroisopropyl)ether 300ND Hexachloroethane 300ND 2-Methyl Phenol 300ND 3+4 Methyl Phenol 300ND Naphthalene 300ND 2-Nitrophenol 300ND 2,4-Dichlorophenol 300ND Hexachlorobutadiene 300ND 4-Chloro-3-methylphenol 300ND Nitrobenzene 300ND Isophorone 300ND 2,4-Dimethylphenol 300ND bis(2-Chloroethoxy)methane 300ND Benzoic Acid 300ND 1,2,4-Trichlorobenzene 300ND 2,6-Dichlorophenol 300ND 4-Chloroaniline 300ND 1,2,4,5-Tetrachlorobenzene 300ND 2-Methyl Naphthalene 300ND Acenaphthylene 300ND Acenaphthene 300ND Dibenzofuran 300ND Fluorene 300ND Hexachlorocyclopentadiene 300ND 2,4,6-Trichlorophenol 300ND 2,4,5-Trichlorophenol 300ND 2,4-Dinitrophenol 300ND 4-Nitrophenol 300ND 2-Chloronaphthalene 300ND 2-Nitroaniline 300ND Dimethylphthalate 300ND 2,6-Dinitrotoluene 300ND 4-Nitroaniline 300ND 2,4-Dinitrotoluene 300ND 2,3,4,6-Tetrachlorophenol 300ND 4-Chlorophenyl-phenylether 300ND Diethylphthalate 300ND Phenanthrene 300ND 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 10 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes Blank (B6J1121-BLK1) - Continued Prepared: 10/11/2016 Analyzed: 10/12/2016 Anthracene 300ND Carbazole 300ND Fluoranthene 300ND Pyrene 300ND n-Nitrosodiphenylamine 300ND Pentachlorophenol 300ND 3-Nitroaniline 300ND 4,6-Dinitro-2-methylphenol 300ND 1,2-Diphenylhydrazine 300ND 4-Bromophenyl-phenylether 300ND Hexachlorobenzene 300ND Di-n-butylphthalate 300ND Pentachloronitrobenzene 300ND Benzo[a]anthracene 300ND Chrysene 300ND Butylbenzylphthalate 300ND 3,3-Dichlorobenzidine 300ND bis(2-Ethylhexyl)phthalate 300ND Di-n-octylphthalate 300ND Benzo[b]fluoranthene 300ND Benzo[k]fluoranthene 300ND Benzo[a]pyrene 300ND Indeno[1,2,3-cd]pyrene 300ND Dibenz[a,h]anthracene 300ND Benzo[g,h,i]perylene 300ND 63.3 30 - 130Surrogate: 2-Fluorophenol 62.1 30 - 130Surrogate: Phenol-d6 60.2 30 - 130Surrogate: Nitrobenzene-d5 65.1 30 - 130Surrogate: 2-Fluorobiphenyl 70.7 30 - 130Surrogate: 2,4,6-Tribromophenol 82.7 30 - 130Surrogate: Terphenyl-d14 LCS (B6J1121-BS1)Prepared: 10/11/2016 Analyzed: 10/12/2016 Phenol 300 69.0 30 - 1302760 4,000.000 1,3-Dichlorobenzene 300 53.4 40 - 1402140 4,000.000 n-Nitroso-di-n-propylamine 300 60.8 40 - 1402430 4,000.000 Pyridine 300 44.6 40 - 1401780 4,000.000 n-Nitroso-dimethylamine 300 58.3 40 - 1402330 4,000.000 bis(2-Chloroethyl)ether 300 57.9 40 - 1402320 4,000.000 Aniline 300 47.3 40 - 1401890 4,000.000 2-Chlorophenol 300 62.5 30 - 1302500 4,000.000 1,4-Dichlorobenzene 300 54.7 40 - 1402190 4,000.000 Benzyl Alcohol 300 50.3 30 - 1302010 4,000.000 1,2-Dichlorobenzene 300 54.9 40 - 1402200 4,000.000 bis(2-Chloroisopropyl)ether 300 49.0 40 - 1401960 4,000.000 Hexachloroethane 300 47.1 40 - 1401890 4,000.000 2-Methyl Phenol 300 70.7 30 - 1302830 4,000.000 3+4 Methyl Phenol 300 66.2 30 - 1302650 4,000.000 Naphthalene 300 63.1 40 - 1402530 4,000.000 2-Nitrophenol 300 57.9 30 - 1302310 4,000.000 2,4-Dichlorophenol 300 64.3 30 - 1302570 4,000.000 Hexachlorobutadiene 300 57.9 40 - 1402320 4,000.000 4-Chloro-3-methylphenol 300 68.0 30 - 1302720 4,000.000 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 11 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Analyte Result RL Spike Level Source Result % Rec % Rec Limits RPD RPD Limit(ug/kg) (ug/kg)Notes LCS (B6J1121-BS1) - Continued Prepared: 10/11/2016 Analyzed: 10/12/2016 Nitrobenzene 300 60.6 40 - 1402420 4,000.000 Isophorone 300 63.2 40 - 1402530 4,000.000 2,4-Dimethylphenol 300 65.7 30 - 1302630 4,000.000 bis(2-Chloroethoxy)methane 300 63.7 40 - 1402550 4,000.000 Benzoic Acid 300 41.7 30 - 1301670 4,000.000 1,2,4-Trichlorobenzene 300 58.1 40 - 1402320 4,000.000 2,6-Dichlorophenol 300 59.6 30 - 1302380 4,000.000 4-Chloroaniline 300 42.0 40 - 1401680 4,000.000 1,2,4,5-Tetrachlorobenzene 300 62.2 40 - 1402490 4,000.000 2-Methyl Naphthalene 300 63.4 40 - 1402540 4,000.000 Acenaphthylene 300 62.6 40 - 1402500 4,000.000 Acenaphthene 300 68.9 40 - 1402760 4,000.000 Dibenzofuran 300 70.7 40 - 1402830 4,000.000 Fluorene 300 71.2 40 - 1402850 4,000.000 Hexachlorocyclopentadiene 300 36.2 40 - 1401450 L 4,000.000 2,4,6-Trichlorophenol 300 67.0 30 - 1302680 4,000.000 2,4,5-Trichlorophenol 300 72.9 30 - 1302920 4,000.000 2,4-Dinitrophenol 300 27.9 30 - 1301120 L 4,000.000 4-Nitrophenol 300 64.3 30 - 1302570 4,000.000 2-Chloronaphthalene 300 62.6 40 - 1402510 4,000.000 2-Nitroaniline 300 71.9 40 - 1402880 4,000.000 Dimethylphthalate 300 72.3 40 - 1402890 4,000.000 2,6-Dinitrotoluene 300 69.0 40 - 1402760 4,000.000 4-Nitroaniline 300 70.4 40 - 1402810 4,000.000 2,4-Dinitrotoluene 300 70.5 40 - 1402820 4,000.000 2,3,4,6-Tetrachlorophenol 300 71.4 30 - 1302860 4,000.000 4-Chlorophenyl-phenylether 300 71.3 40 - 1402850 4,000.000 Diethylphthalate 300 74.0 40 - 1402960 4,000.000 Phenanthrene 300 76.0 40 - 1403040 4,000.000 Anthracene 300 76.1 40 - 1403040 4,000.000 Carbazole 300 95.3 40 - 1403810 4,000.000 Fluoranthene 300 74.9 40 - 1403000 4,000.000 Pyrene 300 75.4 40 - 1403020 4,000.000 n-Nitrosodiphenylamine 300 93.3 40 - 1403730 4,000.000 Pentachlorophenol 300 63.0 30 - 1302520 4,000.000 3-Nitroaniline 300 66.9 40 - 1402670 4,000.000 4,6-Dinitro-2-methylphenol 300 30.7 30 - 1301230 4,000.000 1,2-Diphenylhydrazine 300 70.4 40 - 1402820 4,000.000 4-Bromophenyl-phenylether 300 69.8 40 - 1402790 4,000.000 Hexachlorobenzene 300 69.6 40 - 1402790 4,000.000 Di-n-butylphthalate 300 75.5 40 - 1403020 4,000.000 Pentachloronitrobenzene 300 78.9 40 - 1403160 4,000.000 Benzo[a]anthracene 300 81.5 40 - 1403260 4,000.000 Chrysene 300 80.3 40 - 1403210 4,000.000 Butylbenzylphthalate 300 80.5 40 - 1403220 4,000.000 3,3-Dichlorobenzidine 300 40 - 1404280 L bis(2-Ethylhexyl)phthalate 300 75.5 40 - 1403020 4,000.000 Di-n-octylphthalate 300 85.3 40 - 1403410 4,000.000 Benzo[b]fluoranthene 300 92.0 40 - 1403680 4,000.000 Benzo[k]fluoranthene 300 105 40 - 1404200 4,000.000 Benzo[a]pyrene 300 101 40 - 1404050 4,000.000 Indeno[1,2,3-cd]pyrene 300 105 40 - 1404220 4,000.000 Dibenz[a,h]anthracene 300 113 40 - 1404540 4,000.000 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 12 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 Report Comments: Questions related to this report should be directed to David Ditta, Timothy Fusco, or Robert Blake at 203-377-9984. Sincerely, David Ditta Laboratory Director Sample Result Flags: E- The result is estimated, above the calibration range. H- The surrogate recovery is above the control limits. L- The surrogate recovery is below the control limits. B- The compound was detected in the laboratory blank. P- The Relative Percent Difference (RPD) of dual column analyses exceeds 40%. D- The RPD between the sample and the sample duplicate is high. Sample homogeneity may be a problem. +- The Surrogate was diluted out. *C1- The Continuing Calibration did not meet method specifications and was biased low for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased low. *C2- The Continuing Calibration did not meet method specifications and was biased high for this analyte. Increased uncertainty is associated with the reported value which is likely to be biased high. *F1- The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the low side. *F2- The Laboratory Control Sample recovery is outside of control limits. Reported value for this analyte is likely to be biased on the high side. I- The Analyte exceeds %RSD limits for the Initial Calibration. This is a non-directional bias. All results met standard operating procedures unless indicated by a data qualifier next to a sample result, or a narration in the QC report. Complete Environmental Testing is only responsible for the certified testing and is not directly responsible for the integrity of the sample before laboratory receipt. ND is None Detected at the specified detection limit All analyses were performed in house unless a Reference Laboratory is listed. Samples will be disposed of 30 days after the report date. 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 25 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 CertificationsAnalyte CERTIFICATIONS Certified Analyses included in this Report CT-ETPH in Soil CTETPH EPA 1010A in Soil CT,NYFlashpoint EPA 6010C in Soil CT,NYLead CT,NYSelenium CT,NYCadmium CT,NYChromium CT,NYArsenic CT,NYBarium CT,NYSilver EPA 7471B in Soil CT,NYMercury EPA 8260C in Soil CT,NYDichlorodifluoromethane CT,NYChloromethane CT,NYVinyl Chloride CT,NYBromomethane CT,NYChloroethane CT,NYTrichlorofluoromethane CT,NYAcetone CT,NYAcrylonitrile CT,NYTrichlorotrifluoroethane CT,NY1,1-Dichloroethene CT,NYMethylene Chloride CT,NYCarbon Disulfide CT,NYMethyl-t-Butyl Ether (MTBE) CT,NYtrans-1,2-Dichloroethene CT,NY1,1-Dichloroethane CT,NY2-Butanone (MEK) CT,NY2,2-Dichloropropane CT,NYcis-1,2-Dichloroethene CT,NYChloroform CTTetrahydrofuran CT,NY1,1,1-Trichloroethane CT,NYCarbon Tetrachloride CT,NY1,1-Dichloropropene CT,NYBenzene CT,NY1,2-Dichloroethane CT,NYTrichloroethene CT,NY1,2-Dichloropropane CT,NYDibromomethane CT,NYBromodichloromethane 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 26 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 CertificationsAnalyte CERTIFICATIONS Certified Analyses included in this Report EPA 8260C in Soil CT,NYMethyl Isobutyl Ketone CT,NYcis-1,3-Dichloropropene CT,NYToluene CT,NYtrans-1,3-Dichloropropene CT,NY2-Hexanone CT,NY1,1,2-Trichloroethane CT,NYTetrachloroethene CT,NY1,3-Dichloropropane CT,NYDibromochloromethane CT,NY1,2-Dibromoethane CT,NYtrans-1,4-Dichloro-2-Butene CT,NYChlorobenzene CT,NY1,1,1,2-Tetrachloroethane CT,NYEthylbenzene CT,NYm+p Xylenes CT,NYo-Xylene CT,NYStyrene CT,NYBromoform CT,NYIsopropylbenzene CT,NY1,1,2,2-Tetrachloroethane CT,NYBromobenzene CT,NY1,2,3-Trichloropropane CT,NYn-Propylbenzene CT,NY2-Chlorotoluene CT,NY4-Chlorotoluene CT,NY1,3,5-Trimethylbenzene CT,NYtert-Butylbenzene CT,NY1,2,4-Trimethylbenzene CT,NYsec-Butylbenzene CT,NY1,3-Dichlorobenzene CT,NY4-Isopropyltoluene CT,NY1,4-Dichlorobenzene CT,NY1,2-Dichlorobenzene CT,NYn-Butylbenzene CT,NY1,2-Dibromo-3-Chloropropane CT,NY1,2,4-Trichlorobenzene CT,NYHexachlorobutadiene CT,NYNaphthalene CT1,2,3-Trichlorobenzene EPA 8270D in Soil CT,NYPhenol CT,NY1,3-Dichlorobenzene CT,NYn-Nitroso-di-n-propylamine CT,NYPyridine 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 27 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 CertificationsAnalyte CERTIFICATIONS Certified Analyses included in this Report EPA 8270D in Soil CT,NYn-Nitroso-dimethylamine CT,NYbis(2-Chloroethyl)ether CT,NYAniline CT,NY2-Chlorophenol CT,NY1,4-Dichlorobenzene CT,NYBenzyl Alcohol CT,NY1,2-Dichlorobenzene CT,NYbis(2-Chloroisopropyl)ether CT,NYHexachloroethane CT,NY2-Methyl Phenol CT,NY3+4 Methyl Phenol CT,NYNaphthalene CT,NY2-Nitrophenol CT,NY2,4-Dichlorophenol CT,NYHexachlorobutadiene CT,NY4-Chloro-3-methylphenol CT,NYNitrobenzene CT,NYIsophorone CT,NY2,4-Dimethylphenol CT,NYbis(2-Chloroethoxy)methane CT,NYBenzoic Acid CT,NY1,2,4-Trichlorobenzene CT,NY2,6-Dichlorophenol CT,NY4-Chloroaniline CT,NY1,2,4,5-Tetrachlorobenzene CT,NY2-Methyl Naphthalene CT,NYAcenaphthylene CT,NYAcenaphthene CT,NYDibenzofuran CT,NYFluorene CT,NYHexachlorocyclopentadiene CT,NY2,4,6-Trichlorophenol CT,NY2,4,5-Trichlorophenol CT,NY2,4-Dinitrophenol CT,NY4-Nitrophenol CT,NY2-Chloronaphthalene CT,NY2-Nitroaniline CT,NYDimethylphthalate CT,NY2,6-Dinitrotoluene CT,NY4-Nitroaniline CT,NY2,4-Dinitrotoluene CT,NY2,3,4,6-Tetrachlorophenol CT,NY4-Chlorophenyl-phenylether CT,NYDiethylphthalate CT,NYPhenanthrene 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 28 of 30 Project: NPU Stony Brook, Montville CET # : 6100217 CertificationsAnalyte CERTIFICATIONS Certified Analyses included in this Report EPA 8270D in Soil CT,NYAnthracene CT,NYCarbazole CT,NYFluoranthene CT,NYPyrene CT,NYn-Nitrosodiphenylamine CT,NYPentachlorophenol CT,NY3-Nitroaniline CT,NY4,6-Dinitro-2-methylphenol CT1,2-Diphenylhydrazine CT,NY4-Bromophenyl-phenylether CT,NYHexachlorobenzene CT,NYDi-n-butylphthalate CT,NYPentachloronitrobenzene CT,NYBenzo[a]anthracene CT,NYChrysene CT,NYButylbenzylphthalate CT,NY3,3-Dichlorobenzidine CT,NYbis(2-Ethylhexyl)phthalate CT,NYDi-n-octylphthalate CT,NYBenzo[b]fluoranthene CT,NYBenzo[k]fluoranthene CT,NYBenzo[a]pyrene CT,NYIndeno[1,2,3-cd]pyrene CT,NYDibenz[a,h]anthracene CT,NYBenzo[g,h,i]perylene EPA 9045D in Soil CTpH SW 846 Ch. 7 in Soil CTReactive Cyanide CTReactive Sulfide Complete Environmental Testing operates under the following certifications and accreditations: Code Description Number Expires Connecticut Public Health 09/30/2016CTPH0116 New York Certification (NELAC)04/01/2017NY11982 80 Lupes Drive, Stratford, CT 06615 Tel: 203-377-9984 Fax: 203-377-9952 www.cetlabs.com Complete Environmental Testing, Inc. Page 29 of 30 Page 30 of 30 Source: CLA EngineersSource: CLA Engineers NTSflow